JP2019210220A5 - - Google Patents
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- Publication number
- JP2019210220A5 JP2019210220A5 JP2018105283A JP2018105283A JP2019210220A5 JP 2019210220 A5 JP2019210220 A5 JP 2019210220A5 JP 2018105283 A JP2018105283 A JP 2018105283A JP 2018105283 A JP2018105283 A JP 2018105283A JP 2019210220 A5 JP2019210220 A5 JP 2019210220A5
- Authority
- JP
- Japan
- Prior art keywords
- added
- mmol
- iodosobenzene
- purity
- stirring
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- JYJVVHFRSFVEJM-UHFFFAOYSA-N iodosobenzene Chemical compound O=IC1=CC=CC=C1 JYJVVHFRSFVEJM-UHFFFAOYSA-N 0.000 description 3
- NLKNQRATVPKPDG-UHFFFAOYSA-M potassium iodide Chemical compound [K+].[I-] NLKNQRATVPKPDG-UHFFFAOYSA-M 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- PQLVXDKIJBQVDF-UHFFFAOYSA-N acetic acid;hydrate Chemical compound O.CC(O)=O PQLVXDKIJBQVDF-UHFFFAOYSA-N 0.000 description 1
- YCOXTKKNXUZSKD-UHFFFAOYSA-N as-o-xylenol Natural products CC1=CC=C(O)C=C1C YCOXTKKNXUZSKD-UHFFFAOYSA-N 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- SNHMUERNLJLMHN-UHFFFAOYSA-N iodobenzene Chemical compound IC1=CC=CC=C1 SNHMUERNLJLMHN-UHFFFAOYSA-N 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- AKHNMLFCWUSKQB-UHFFFAOYSA-L sodium thiosulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=S AKHNMLFCWUSKQB-UHFFFAOYSA-L 0.000 description 1
- 235000019345 sodium thiosulphate Nutrition 0.000 description 1
- FHKLOBNGYGFRSF-UHFFFAOYSA-N sodium;hypochlorite;pentahydrate Chemical compound O.O.O.O.O.[Na+].Cl[O-] FHKLOBNGYGFRSF-UHFFFAOYSA-N 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2018105283A JP7035815B2 (ja) | 2018-05-31 | 2018-05-31 | 次亜塩素酸塩を用いた三価超原子価ヨウ素化合物の製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2018105283A JP7035815B2 (ja) | 2018-05-31 | 2018-05-31 | 次亜塩素酸塩を用いた三価超原子価ヨウ素化合物の製造方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2019210220A JP2019210220A (ja) | 2019-12-12 |
| JP2019210220A5 true JP2019210220A5 (enExample) | 2020-12-17 |
| JP7035815B2 JP7035815B2 (ja) | 2022-03-15 |
Family
ID=68845728
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2018105283A Active JP7035815B2 (ja) | 2018-05-31 | 2018-05-31 | 次亜塩素酸塩を用いた三価超原子価ヨウ素化合物の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP7035815B2 (enExample) |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4552611B2 (ja) | 2003-11-18 | 2010-09-29 | 和光純薬工業株式会社 | 低分子リサイクル型超原子価ヨウ素試薬 |
| JP5797539B2 (ja) | 2011-12-08 | 2015-10-21 | 株式会社合同資源 | 三配位超原子価ヨウ素化合物の製造方法 |
-
2018
- 2018-05-31 JP JP2018105283A patent/JP7035815B2/ja active Active
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