JP2017517644A - ミネラルウールのためのバインダ組成物 - Google Patents
ミネラルウールのためのバインダ組成物 Download PDFInfo
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- JP2017517644A JP2017517644A JP2016569052A JP2016569052A JP2017517644A JP 2017517644 A JP2017517644 A JP 2017517644A JP 2016569052 A JP2016569052 A JP 2016569052A JP 2016569052 A JP2016569052 A JP 2016569052A JP 2017517644 A JP2017517644 A JP 2017517644A
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- 239000000203 mixture Substances 0.000 title claims abstract description 69
- 239000011490 mineral wool Substances 0.000 title claims abstract description 18
- 239000011230 binding agent Substances 0.000 title description 16
- 235000000346 sugar Nutrition 0.000 claims abstract description 55
- 238000004513 sizing Methods 0.000 claims abstract description 41
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 claims abstract description 30
- 239000002253 acid Substances 0.000 claims abstract description 25
- 150000008163 sugars Chemical class 0.000 claims abstract description 25
- 150000001720 carbohydrates Chemical class 0.000 claims abstract description 19
- 235000014633 carbohydrates Nutrition 0.000 claims abstract description 16
- 238000009413 insulation Methods 0.000 claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 238000005192 partition Methods 0.000 claims abstract description 13
- 125000000524 functional group Chemical group 0.000 claims abstract description 8
- 125000001931 aliphatic group Chemical group 0.000 claims abstract description 5
- 125000003118 aryl group Chemical group 0.000 claims abstract description 4
- 150000003839 salts Chemical class 0.000 claims abstract description 4
- 125000002723 alicyclic group Chemical group 0.000 claims abstract 2
- 239000000047 product Substances 0.000 claims description 33
- 239000000835 fiber Substances 0.000 claims description 14
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 12
- 229920002472 Starch Polymers 0.000 claims description 10
- 239000008107 starch Substances 0.000 claims description 10
- 235000019698 starch Nutrition 0.000 claims description 10
- 150000004676 glycans Chemical class 0.000 claims description 7
- 229920001282 polysaccharide Polymers 0.000 claims description 7
- 239000005017 polysaccharide Substances 0.000 claims description 7
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 6
- 239000000178 monomer Substances 0.000 claims description 5
- 150000002772 monosaccharides Chemical class 0.000 claims description 5
- 150000002016 disaccharides Chemical class 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 229920001542 oligosaccharide Polymers 0.000 claims description 4
- 150000002482 oligosaccharides Chemical class 0.000 claims description 4
- 150000008065 acid anhydrides Chemical class 0.000 claims description 3
- 229960005323 phenoxyethanol Drugs 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 238000001704 evaporation Methods 0.000 claims description 2
- 239000000413 hydrolysate Substances 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims description 2
- 229920001187 thermosetting polymer Polymers 0.000 claims description 2
- 150000007513 acids Chemical class 0.000 abstract description 4
- 150000008064 anhydrides Chemical class 0.000 abstract description 3
- 239000003054 catalyst Substances 0.000 description 9
- -1 isotrehalose Chemical compound 0.000 description 9
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 8
- 238000011084 recovery Methods 0.000 description 8
- 230000002209 hydrophobic effect Effects 0.000 description 7
- 229920001296 polysiloxane Polymers 0.000 description 7
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 6
- 150000001875 compounds Chemical class 0.000 description 6
- 239000000523 sample Substances 0.000 description 6
- MSXVEPNJUHWQHW-UHFFFAOYSA-N 2-methylbutan-2-ol Chemical compound CCC(C)(C)O MSXVEPNJUHWQHW-UHFFFAOYSA-N 0.000 description 5
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 5
- 230000032683 aging Effects 0.000 description 5
- 150000001323 aldoses Chemical class 0.000 description 5
- 229910052783 alkali metal Inorganic materials 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 5
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 4
- 229920002245 Dextrose equivalent Polymers 0.000 description 4
- 150000001340 alkali metals Chemical class 0.000 description 4
- 239000004202 carbamide Substances 0.000 description 4
- 230000006835 compression Effects 0.000 description 4
- 238000007906 compression Methods 0.000 description 4
- 238000005984 hydrogenation reaction Methods 0.000 description 4
- 239000002557 mineral fiber Substances 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 3
- 229930006000 Sucrose Natural products 0.000 description 3
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 3
- 229920001577 copolymer Polymers 0.000 description 3
- 238000004132 cross linking Methods 0.000 description 3
- 239000000839 emulsion Substances 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 239000011491 glass wool Substances 0.000 description 3
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 3
- 239000000845 maltitol Substances 0.000 description 3
- 235000010449 maltitol Nutrition 0.000 description 3
- 239000011435 rock Substances 0.000 description 3
- 239000005720 sucrose Substances 0.000 description 3
- HDTRYLNUVZCQOY-UHFFFAOYSA-N α-D-glucopyranosyl-α-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(O)C(O)C(CO)O1 HDTRYLNUVZCQOY-UHFFFAOYSA-N 0.000 description 2
- BBMCTIGTTCKYKF-UHFFFAOYSA-N 1-heptanol Chemical compound CCCCCCCO BBMCTIGTTCKYKF-UHFFFAOYSA-N 0.000 description 2
- KJCVRFUGPWSIIH-UHFFFAOYSA-N 1-naphthol Chemical compound C1=CC=C2C(O)=CC=CC2=C1 KJCVRFUGPWSIIH-UHFFFAOYSA-N 0.000 description 2
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 description 2
- QQOMQLYQAXGHSU-UHFFFAOYSA-N 2,3,6-Trimethylphenol Chemical compound CC1=CC=C(C)C(O)=C1C QQOMQLYQAXGHSU-UHFFFAOYSA-N 0.000 description 2
- NKTOLZVEWDHZMU-UHFFFAOYSA-N 2,5-xylenol Chemical compound CC1=CC=C(C)C(O)=C1 NKTOLZVEWDHZMU-UHFFFAOYSA-N 0.000 description 2
- NXXYKOUNUYWIHA-UHFFFAOYSA-N 2,6-Dimethylphenol Chemical compound CC1=CC=CC(C)=C1O NXXYKOUNUYWIHA-UHFFFAOYSA-N 0.000 description 2
- JAHNSTQSQJOJLO-UHFFFAOYSA-N 2-(3-fluorophenyl)-1h-imidazole Chemical compound FC1=CC=CC(C=2NC=CN=2)=C1 JAHNSTQSQJOJLO-UHFFFAOYSA-N 0.000 description 2
- IXQGCWUGDFDQMF-UHFFFAOYSA-N 2-Ethylphenol Chemical compound CCC1=CC=CC=C1O IXQGCWUGDFDQMF-UHFFFAOYSA-N 0.000 description 2
- CETWDUZRCINIHU-UHFFFAOYSA-N 2-heptanol Chemical compound CCCCCC(C)O CETWDUZRCINIHU-UHFFFAOYSA-N 0.000 description 2
- CRBJBYGJVIBWIY-UHFFFAOYSA-N 2-isopropylphenol Chemical compound CC(C)C1=CC=CC=C1O CRBJBYGJVIBWIY-UHFFFAOYSA-N 0.000 description 2
- JWAZRIHNYRIHIV-UHFFFAOYSA-N 2-naphthol Chemical compound C1=CC=CC2=CC(O)=CC=C21 JWAZRIHNYRIHIV-UHFFFAOYSA-N 0.000 description 2
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 description 2
- YCOXTKKNXUZSKD-UHFFFAOYSA-N 3,4-xylenol Chemical compound CC1=CC=C(O)C=C1C YCOXTKKNXUZSKD-UHFFFAOYSA-N 0.000 description 2
- TUAMRELNJMMDMT-UHFFFAOYSA-N 3,5-xylenol Chemical compound CC1=CC(C)=CC(O)=C1 TUAMRELNJMMDMT-UHFFFAOYSA-N 0.000 description 2
- HMNKTRSOROOSPP-UHFFFAOYSA-N 3-Ethylphenol Chemical compound CCC1=CC=CC(O)=C1 HMNKTRSOROOSPP-UHFFFAOYSA-N 0.000 description 2
- MXLMTQWGSQIYOW-UHFFFAOYSA-N 3-methyl-2-butanol Chemical compound CC(C)C(C)O MXLMTQWGSQIYOW-UHFFFAOYSA-N 0.000 description 2
- HXDOZKJGKXYMEW-UHFFFAOYSA-N 4-ethylphenol Chemical compound CCC1=CC=C(O)C=C1 HXDOZKJGKXYMEW-UHFFFAOYSA-N 0.000 description 2
- MQWCXKGKQLNYQG-UHFFFAOYSA-N 4-methylcyclohexan-1-ol Chemical compound CC1CCC(O)CC1 MQWCXKGKQLNYQG-UHFFFAOYSA-N 0.000 description 2
- KWSLGOVYXMQPPX-UHFFFAOYSA-N 5-[3-(trifluoromethyl)phenyl]-2h-tetrazole Chemical group FC(F)(F)C1=CC=CC(C2=NNN=N2)=C1 KWSLGOVYXMQPPX-UHFFFAOYSA-N 0.000 description 2
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical group [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 2
- 229920001353 Dextrin Polymers 0.000 description 2
- 239000004375 Dextrin Substances 0.000 description 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 description 2
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 description 2
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 2
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 2
- HDTRYLNUVZCQOY-WSWWMNSNSA-N Trehalose Natural products O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-WSWWMNSNSA-N 0.000 description 2
- MUPFEKGTMRGPLJ-UHFFFAOYSA-N UNPD196149 Natural products OC1C(O)C(CO)OC1(CO)OC1C(O)C(O)C(O)C(COC2C(C(O)C(O)C(CO)O2)O)O1 MUPFEKGTMRGPLJ-UHFFFAOYSA-N 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 2
- 150000001299 aldehydes Chemical class 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- HDTRYLNUVZCQOY-LIZSDCNHSA-N alpha,alpha-trehalose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-LIZSDCNHSA-N 0.000 description 2
- 150000001412 amines Chemical class 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- UJMDYLWCYJJYMO-UHFFFAOYSA-N benzene-1,2,3-tricarboxylic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1C(O)=O UJMDYLWCYJJYMO-UHFFFAOYSA-N 0.000 description 2
- QMKYBPDZANOJGF-UHFFFAOYSA-N benzene-1,3,5-tricarboxylic acid Chemical compound OC(=O)C1=CC(C(O)=O)=CC(C(O)=O)=C1 QMKYBPDZANOJGF-UHFFFAOYSA-N 0.000 description 2
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 2
- GUBGYTABKSRVRQ-QUYVBRFLSA-N beta-maltose Chemical compound OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O GUBGYTABKSRVRQ-QUYVBRFLSA-N 0.000 description 2
- 229910052796 boron Inorganic materials 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 125000001309 chloro group Chemical group Cl* 0.000 description 2
- HNEGQIOMVPPMNR-IHWYPQMZSA-N citraconic acid Chemical compound OC(=O)C(/C)=C\C(O)=O HNEGQIOMVPPMNR-IHWYPQMZSA-N 0.000 description 2
- 235000019425 dextrin Nutrition 0.000 description 2
- 238000006047 enzymatic hydrolysis reaction Methods 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 239000001530 fumaric acid Substances 0.000 description 2
- 239000003365 glass fiber Substances 0.000 description 2
- 239000008103 glucose Substances 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 description 2
- QNVRIHYSUZMSGM-UHFFFAOYSA-N hexan-2-ol Chemical compound CCCCC(C)O QNVRIHYSUZMSGM-UHFFFAOYSA-N 0.000 description 2
- ZOCHHNOQQHDWHG-UHFFFAOYSA-N hexan-3-ol Chemical compound CCCC(O)CC ZOCHHNOQQHDWHG-UHFFFAOYSA-N 0.000 description 2
- 229920001519 homopolymer Polymers 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- ROBFUDYVXSDBQM-UHFFFAOYSA-N hydroxymalonic acid Chemical compound OC(=O)C(O)C(O)=O ROBFUDYVXSDBQM-UHFFFAOYSA-N 0.000 description 2
- PHTQWCKDNZKARW-UHFFFAOYSA-N isoamylol Chemical compound CC(C)CCO PHTQWCKDNZKARW-UHFFFAOYSA-N 0.000 description 2
- QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 description 2
- 125000000468 ketone group Chemical group 0.000 description 2
- RLSSMJSEOOYNOY-UHFFFAOYSA-N m-cresol Chemical compound CC1=CC=CC(O)=C1 RLSSMJSEOOYNOY-UHFFFAOYSA-N 0.000 description 2
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 2
- 239000011976 maleic acid Substances 0.000 description 2
- VQHSOMBJVWLPSR-WUJBLJFYSA-N maltitol Chemical compound OC[C@H](O)[C@@H](O)[C@@H]([C@H](O)CO)O[C@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O VQHSOMBJVWLPSR-WUJBLJFYSA-N 0.000 description 2
- 229940035436 maltitol Drugs 0.000 description 2
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 description 2
- LVHBHZANLOWSRM-UHFFFAOYSA-N methylenebutanedioic acid Natural products OC(=O)CC(=C)C(O)=O LVHBHZANLOWSRM-UHFFFAOYSA-N 0.000 description 2
- HNEGQIOMVPPMNR-UHFFFAOYSA-N methylfumaric acid Natural products OC(=O)C(C)=CC(O)=O HNEGQIOMVPPMNR-UHFFFAOYSA-N 0.000 description 2
- BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 description 2
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- SJWFXCIHNDVPSH-UHFFFAOYSA-N octan-2-ol Chemical compound CCCCCCC(C)O SJWFXCIHNDVPSH-UHFFFAOYSA-N 0.000 description 2
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- WLJVNTCWHIRURA-UHFFFAOYSA-N pimelic acid Chemical compound OC(=O)CCCCCC(O)=O WLJVNTCWHIRURA-UHFFFAOYSA-N 0.000 description 2
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- 239000011591 potassium Substances 0.000 description 2
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- CYIDZMCFTVVTJO-UHFFFAOYSA-N pyromellitic acid Chemical compound OC(=O)C1=CC(C(O)=O)=C(C(O)=O)C=C1C(O)=O CYIDZMCFTVVTJO-UHFFFAOYSA-N 0.000 description 2
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- CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 description 2
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- 239000011734 sodium Substances 0.000 description 2
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- 229910001379 sodium hypophosphite Inorganic materials 0.000 description 2
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- 150000000000 tetracarboxylic acids Chemical class 0.000 description 2
- LDHQCZJRKDOVOX-UHFFFAOYSA-N trans-crotonic acid Natural products CC=CC(O)=O LDHQCZJRKDOVOX-UHFFFAOYSA-N 0.000 description 2
- KQTIIICEAUMSDG-UHFFFAOYSA-N tricarballylic acid Chemical compound OC(=O)CC(C(O)=O)CC(O)=O KQTIIICEAUMSDG-UHFFFAOYSA-N 0.000 description 2
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- ARCGXLSVLAOJQL-UHFFFAOYSA-N trimellitic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C(C(O)=O)=C1 ARCGXLSVLAOJQL-UHFFFAOYSA-N 0.000 description 2
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 2
- NDVWOBYBJYUSMF-RNFRBKRXSA-N (1r,2r)-2-methylcyclohexan-1-ol Chemical compound C[C@@H]1CCCC[C@H]1O NDVWOBYBJYUSMF-RNFRBKRXSA-N 0.000 description 1
- NDVWOBYBJYUSMF-NKWVEPMBSA-N (1r,2s)-2-methylcyclohexan-1-ol Chemical compound C[C@H]1CCCC[C@H]1O NDVWOBYBJYUSMF-NKWVEPMBSA-N 0.000 description 1
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- 229910052751 metal Inorganic materials 0.000 description 1
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- 229910052698 phosphorus Inorganic materials 0.000 description 1
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- 239000001205 polyphosphate Substances 0.000 description 1
- 235000011176 polyphosphates Nutrition 0.000 description 1
- 125000006239 protecting group Chemical group 0.000 description 1
- 125000001453 quaternary ammonium group Chemical group 0.000 description 1
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- 239000001488 sodium phosphate Substances 0.000 description 1
- 229910000162 sodium phosphate Inorganic materials 0.000 description 1
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- 235000010356 sorbitol Nutrition 0.000 description 1
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- 238000005507 spraying Methods 0.000 description 1
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- 238000003756 stirring Methods 0.000 description 1
- 125000000472 sulfonyl group Chemical group *S(*)(=O)=O 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- UFDHBDMSHIXOKF-UHFFFAOYSA-N tetrahydrophthalic acid Chemical group OC(=O)C1=C(C(O)=O)CCCC1 UFDHBDMSHIXOKF-UHFFFAOYSA-N 0.000 description 1
- MAZWDMBCPDUFDJ-UHFFFAOYSA-N trans-Traumatinsaeure Natural products OC(=O)CCCCCCCCC=CC(O)=O MAZWDMBCPDUFDJ-UHFFFAOYSA-N 0.000 description 1
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- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
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- D04H1/4209—Inorganic fibres
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- C03C25/00—Surface treatment of fibres or filaments made from glass, minerals or slags
- C03C25/10—Coating
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- C03C25/00—Surface treatment of fibres or filaments made from glass, minerals or slags
- C03C25/10—Coating
- C03C25/24—Coatings containing organic materials
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- C08K5/00—Use of organic ingredients
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- C08K5/09—Carboxylic acids; Metal salts thereof; Anhydrides thereof
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- C09D103/00—Coating compositions based on starch, amylose or amylopectin or on their derivatives or degradation products
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- C09J103/00—Adhesives based on starch, amylose or amylopectin or on their derivatives or degradation products
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- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
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- C09J133/04—Homopolymers or copolymers of esters
- C09J133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
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Abstract
Description
(a)水素化糖、還元糖、非還元糖及びそれらの混合物から選ばれる少なくとも1種の炭水化物、
(b)少なくとも1種のポリカルボン酸又はそのような酸の塩若しくは酸無水物、
(c)成分(a)及び(b)の総計に対して1〜25重量%の、酸又は塩基(ブロンステッド)官能基を含まずかつオクタノール/水分配係数(Log Kow)が1〜3である、少なくとも1種の脂肪族、脂環式又は芳香族モノアルコール、
を含む、水性組成物である。
成分(a)/成分(b)の重量比は好ましくは70/30〜30/70であり、特に60/40〜40/60である。
P = [X]octanol/[X]aqueous
(式中、
[X]octanol は水で飽和されたオクタノール中のXの濃度であり、そして
[X]aqueous はオクタノールで飽和された水中のXの濃度であり、
2つの相は室温であり、そして互いに接触している)。
0〜2部のシラン、特にアミノシラン、
0〜40部、好ましくは4〜25部のオイル又はオイルエマルジョン、
0〜5部のシリコーン、
0〜20部の、水素化糖以外のポリオール、
0〜30部、好ましくは0〜20部の尿素、
0〜30部の、リグニンスルホン酸アンモニウム(ALS)又はリグニンスルホン酸ナトリウムなどのリグニン誘導体、及び、動物性又は植物性タンパク質から選ばれる増量充填材(エクステンダー)。
−上記のとおりの水性サイジング組成物を、ミネラルウール繊維に適用すること、及び、
−水性サイジング組成物の溶媒相を蒸発させ、そして該組成物の非揮発性残留物を熱硬化させることを含む。
重量部で表現された表1に示す成分を含むサイジング組成物を調製する。
容器中に、強く撹拌しながら、水(最終組成物の約80%)、水素化糖(マルチトールシロップ)、クエン酸、次亜リン酸ナトリウム(触媒)、防塵性オイルエマルジョン、シリコーンエマルジョン、そして、1−フェノキシ−2−エタノールを導入することによりサイジング組成物を調製する。
本発明により調製したサンプル2の厚さ回復率は、参照サンプルの90日後の厚さ回復率よりも優れた厚さ回復率を示し、一方、比較サンプル1の厚さ回復率は参照サンプルの厚さ回復率よりも約2%〜3%低いことが判る。
Claims (15)
- 以下を含む、ミネラルウール系絶縁製品用の水性サイジング組成物:
(a)水素化糖、還元糖、非還元糖及びそれらの混合物から選ばれる少なくとも1種の炭水化物、
(b)少なくとも1種のポリカルボン酸又はそのような酸の塩若しくは酸無水物、
(c)成分(a)及び(b)の総計に対して1〜25重量%の、酸又は塩基官能基を含まずかつオクタノール/水分配係数(Log Kow)が1〜3である、少なくとも1種の脂肪族、脂環式又は芳香族モノアルコール。 - 前記モノアルコール(c)の濃度は、成分(a)及び(b)の総計に対して、1.5重量%〜10重量%、好ましくは2重量%〜8重量%であることを特徴とする、請求項1に記載の組成物。
- 前記オクタノール/水分配係数は、1.05〜2.0、好ましくは1.1〜1.5であることを特徴とする、請求項1又は2に記載の組成物。
- 前記モノアルコールは、脂肪族モノアルコール及び脂環式モノアルコールから選ばれることを特徴とする、請求項1〜3のいずれか一項に記載の組成物。
- 前記モノアルコールは、少なくとも1つの芳香環を含むことを特徴とする、請求項1〜4のいずれか一項に記載の組成物。
- 前記モノアルコールは、2−フェノキシエタノールであることを特徴とする、請求項1〜5のいずれか一項に記載の組成物。
- 前記ポリカルボン酸は、ポリカルボン酸モノマーであることを特徴とする、請求項1〜6のいずれか一項に記載の組成物。
- 前記ポリカルボン酸は、クエン酸であることを特徴とする、請求項1〜7のいずれか一項に記載の組成物。
- 前記炭水化物中の水素化糖の割合は、25重量%〜100重量%であることを特徴とする、請求項1に記載の組成物。
- 前記炭水化物は、少なくとも30重量%、好ましくは少なくとも50重量%、特に少なくとも70重量%の水素化糖を含むことを特徴とする、請求項8に記載の組成物。
- 前記水素化糖は、単糖類、二糖類、オリゴ糖及び多糖類の水素化生成物並びにそれらの混合物から選ばれることを特徴とする、請求項1〜10のいずれか一項に記載の組成物。
- 前記水素化糖は、デンプン加水分解物の水素化した生成物であることを特徴とする、請求項1〜11のいずれか一項に記載の組成物。
- 前記成分(a)及び(b)は、各々独立して、サイジング組成物の固形分の30〜70重量%であることを特徴とする、請求項1〜12のいずれか一項に記載の組成物。
- 以下を含む、ミネラルウール系の絶縁製品の製造方法:
−請求項1〜13のいずれか一項に記載の水性サイジング組成物をミネラルウール繊維に適用すること、
−前記水性サイジング組成物の溶媒相を蒸発させ、そして前記組成物の非揮発性残留物を熱硬化させること。 - 請求項14に記載の方法によって得られた、防音性及び/又は断熱性製品。
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FR1454885A FR3021651A1 (fr) | 2014-05-28 | 2014-05-28 | Composition de liant pour laine minerale |
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PCT/FR2015/051135 WO2015181458A1 (fr) | 2014-05-28 | 2015-04-27 | Composition de liant pour laine minerale |
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JP2017514029A (ja) * | 2014-04-15 | 2017-06-01 | サン−ゴバン イゾベール | 非還元糖と水素添加糖とに基づくサイジング組成物、及び得られる絶縁製品 |
JP2020529524A (ja) * | 2017-07-31 | 2020-10-08 | サン−ゴバン イゾベール | ミネラルウールの製造方法 |
JP2020537055A (ja) * | 2017-10-09 | 2020-12-17 | オウェンス コーニング インテレクチュアル キャピタル リミテッド ライアビリティ カンパニー | 水性バインダー組成物 |
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FR3055622B1 (fr) | 2016-09-02 | 2022-04-01 | Saint Gobain Isover | Procede de fabrication de laine minerale |
FR3069464B1 (fr) | 2017-07-31 | 2019-08-09 | Saint-Gobain Isover | Installation de fabrication de laine minerale et dispositif de projection d’une composition d’encollage equipant une telle installation |
FI3794172T3 (fi) | 2018-05-18 | 2023-06-16 | Owens Corning Intellectual Capital Llc | Kuitu kaksiosaisella sidosainejärjestelmällä |
FR3091702B1 (fr) | 2019-01-11 | 2021-01-01 | Saint Gobain Isover | Procédé de fabrication d’un produit d’isolation à base de laine minérale |
FR3104152B1 (fr) | 2019-12-04 | 2021-12-10 | Saint Gobain Isover | Procédé pour améliorer les performances acoustiques d’un produit isolant á base de fibres minérales et produit |
US11813833B2 (en) | 2019-12-09 | 2023-11-14 | Owens Corning Intellectual Capital, Llc | Fiberglass insulation product |
EP3896045A1 (en) | 2020-04-16 | 2021-10-20 | URSA Insulation, S.A. | Binders and curable resins for mineral wool |
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SI3148951T1 (sl) | 2019-12-31 |
CA2947385A1 (fr) | 2015-12-03 |
JP6530427B2 (ja) | 2019-06-12 |
CN106459700B (zh) | 2019-09-27 |
KR20170012249A (ko) | 2017-02-02 |
AU2015265804A1 (en) | 2016-12-15 |
RU2016149892A3 (ja) | 2018-11-07 |
PL3148951T3 (pl) | 2020-01-31 |
AU2015265804B2 (en) | 2019-01-31 |
FR3021651A1 (fr) | 2015-12-04 |
CL2016003033A1 (es) | 2017-05-12 |
MX2016014966A (es) | 2017-04-11 |
WO2015181458A1 (fr) | 2015-12-03 |
EP3148951B1 (fr) | 2019-08-14 |
AR102114A1 (es) | 2017-02-08 |
SG11201609918QA (en) | 2016-12-29 |
RU2677510C2 (ru) | 2019-01-17 |
US10119211B2 (en) | 2018-11-06 |
CN106459700A (zh) | 2017-02-22 |
US20170198425A1 (en) | 2017-07-13 |
UA120055C2 (uk) | 2019-09-25 |
EP3148951A1 (fr) | 2017-04-05 |
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