JP2016505498A5 - - Google Patents
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- JP2016505498A5 JP2016505498A5 JP2015549410A JP2015549410A JP2016505498A5 JP 2016505498 A5 JP2016505498 A5 JP 2016505498A5 JP 2015549410 A JP2015549410 A JP 2015549410A JP 2015549410 A JP2015549410 A JP 2015549410A JP 2016505498 A5 JP2016505498 A5 JP 2016505498A5
- Authority
- JP
- Japan
- Prior art keywords
- molecular sieve
- peak
- degrees
- imax
- imin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000002808 molecular sieve Substances 0.000 claims description 47
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims description 47
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 22
- 238000000034 method Methods 0.000 claims description 13
- 239000013078 crystal Substances 0.000 claims description 11
- 229910052757 nitrogen Inorganic materials 0.000 claims description 11
- 239000002131 composite material Substances 0.000 claims description 8
- 238000002441 X-ray diffraction Methods 0.000 claims description 6
- 238000004375 physisorption Methods 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 2
- 238000002425 crystallisation Methods 0.000 claims 1
- 230000008025 crystallization Effects 0.000 claims 1
- 230000001747 exhibiting effect Effects 0.000 claims 1
- 238000001179 sorption measurement Methods 0.000 description 5
- 239000012084 conversion product Substances 0.000 description 2
- 150000002894 organic compounds Chemical class 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 229910052732 germanium Inorganic materials 0.000 description 1
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261740908P | 2012-12-21 | 2012-12-21 | |
| US61/740,908 | 2012-12-21 | ||
| EP13155722.5 | 2013-02-19 | ||
| EP13155722 | 2013-02-19 | ||
| PCT/US2013/071456 WO2014099262A1 (en) | 2012-12-21 | 2013-11-22 | Small crystal zsm-5, its synthesis and use |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2016505498A JP2016505498A (ja) | 2016-02-25 |
| JP2016505498A5 true JP2016505498A5 (OSRAM) | 2017-01-12 |
| JP6238377B2 JP6238377B2 (ja) | 2017-11-29 |
Family
ID=47739133
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015549410A Active JP6238377B2 (ja) | 2012-12-21 | 2013-11-22 | 小さな結晶ｚｓｍ−５、その合成および使用 |
Country Status (10)
| Country | Link |
|---|---|
| US (2) | US10081552B2 (OSRAM) |
| EP (3) | EP3056470B1 (OSRAM) |
| JP (1) | JP6238377B2 (OSRAM) |
| KR (1) | KR102166191B1 (OSRAM) |
| CN (2) | CN104870367B (OSRAM) |
| CA (1) | CA2895232C (OSRAM) |
| RU (1) | RU2640759C2 (OSRAM) |
| SG (2) | SG11201503973UA (OSRAM) |
| WO (1) | WO2014099262A1 (OSRAM) |
| ZA (1) | ZA201503617B (OSRAM) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SG11201503973UA (en) * | 2012-12-21 | 2015-06-29 | Exxonmobil Chem Patents Inc | Small crystal zsm-5, its synthesis and use |
| US10053403B2 (en) | 2015-02-04 | 2018-08-21 | Exxonmobil Chemical Patents Inc. | Catalyst compositions and their use in transalkylation of heavy aromatics to xylenes |
| US10118165B2 (en) | 2015-02-04 | 2018-11-06 | Exxonmobil Chemical Patents Inc. | Catalyst compositions and use in heavy aromatics conversion processes |
| WO2016129659A1 (ja) * | 2015-02-13 | 2016-08-18 | 東ソー株式会社 | ペンタシル型ゼオライト及びその製造方法 |
| US9851313B2 (en) * | 2015-03-03 | 2017-12-26 | Panalytical B.V. | Quantitative X-ray analysis—ratio correction |
| CA3015142C (en) | 2016-02-19 | 2022-02-15 | Exxonmobil Research And Engineering Company | Small crystal, high surface area emm-30 zeolites, their synthesis and use |
| US10273161B2 (en) | 2017-01-11 | 2019-04-30 | Chevron U.S.A. Inc. | Synthesis of MFI framework type molecular sieves |
| CN113454027B (zh) * | 2019-02-27 | 2023-06-27 | 雪佛龙美国公司 | 分子筛ssz-115、其合成和用途 |
| EP4017940A1 (en) | 2019-08-20 | 2022-06-29 | ExxonMobil Research and Engineering Company | Metal-organic framework catalysts and their use in catalytic cracking |
| US10737946B1 (en) * | 2019-08-29 | 2020-08-11 | Chevron U.S.A. Inc. | Synthesis of aluminum-containing molecular sieves of SEW framework type |
| JP2022163831A (ja) * | 2021-04-15 | 2022-10-27 | 東ソー株式会社 | Ｍｆｉ型ゼオライト |
| EP4406646B1 (en) | 2023-01-27 | 2025-10-01 | Hindustan Petroleum Corporation Limited | Nano size crystal zsm-5 and its preparation and applications thereof |
| WO2025058925A1 (en) | 2023-09-12 | 2025-03-20 | ExxonMobil Technology and Engineering Company | Zeolitic materials in polyolefin decomposition via pyrolysis |
Family Cites Families (26)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3702886A (en) | 1969-10-10 | 1972-11-14 | Mobil Oil Corp | Crystalline zeolite zsm-5 and method of preparing the same |
| US3941871A (en) | 1973-11-02 | 1976-03-02 | Mobil Oil Corporation | Crystalline silicates and method of preparing the same |
| JPS59184723A (ja) | 1983-04-06 | 1984-10-20 | Res Assoc Petroleum Alternat Dev<Rapad> | 結晶性メタロシリケ−トの製造法 |
| US5240892A (en) | 1987-09-02 | 1993-08-31 | Mobil Oil Corporation | Small crystal ZSM-5, as a catalyst |
| EP0514715B1 (en) * | 1991-05-17 | 1997-12-29 | Asahi Kasei Kogyo Kabushiki Kaisha | Method for producing a particulate zeolite |
| GB9122498D0 (en) * | 1991-10-23 | 1991-12-04 | Exxon Chemical Patents Inc | Process for preparing uniform mfitype zeolite crystals |
| ZA933879B (en) * | 1992-06-05 | 1993-12-27 | Exxon Chemical Patents Inc | ZSM-5-zeolite |
| ES2172667T3 (es) * | 1995-06-06 | 2002-10-01 | Exxonmobil Oil Corp | Cristal de grandes dimensiones zsm-5, sintesis y utilizacion del mismo. |
| DE19951781A1 (de) | 1999-10-27 | 2001-05-03 | Sued Chemie Ag | Verfahren zur Herstellung von synthetischen Zeolithen mit MFI-Struktur |
| WO2001049607A1 (en) | 2000-01-05 | 2001-07-12 | Exxon Chemical Patents Inc. | Porous inorganic macrostructure materials and process for their preparation |
| CN1100005C (zh) * | 2000-06-28 | 2003-01-29 | 中国科学院山西煤炭化学研究所 | 导向剂法快速合成zsm－5分子筛的方法 |
| EP1587756A4 (en) | 2002-12-30 | 2011-07-06 | Sk Energy Co Ltd | PROCESS FOR THE PREPARATION OF ZSM-5 BY VARIABLE TEMPERATURE WITHOUT ORGANIC STENCIL MATERIAL |
| CN1281494C (zh) * | 2004-06-29 | 2006-10-25 | 中国石油化工股份有限公司 | 一种小晶粒zsm－5沸石的制备方法 |
| ITMI20042136A1 (it) * | 2004-11-08 | 2005-02-08 | Sasol Italy S P A | Procedimento perfezionato per la preparazione di zeoliti zsm-5 |
| RU2313486C1 (ru) | 2006-04-12 | 2007-12-27 | Общество с ограниченной ответственностью "Томскнефтехим" (ООО "Томскнефтехим") | Синтетический цеолит и способ его получения |
| RU2312063C1 (ru) | 2006-04-12 | 2007-12-10 | Общество с ограниченной ответственностью "Томскнефтехим" (ООО "Томскнефтехим") | Синтетический пористый кристаллический материал и способ его получения |
| RU2313488C1 (ru) | 2006-04-24 | 2007-12-27 | Общество с ограниченной ответственностью "Томскнефтехим" (ООО "Томскнефтехим") | Синтетический цеолит и способ его получения |
| CN100455511C (zh) * | 2006-11-10 | 2009-01-28 | 南京工业大学 | 一种合成小晶粒zsm-5沸石分子筛的方法 |
| CN101733143B (zh) * | 2008-11-21 | 2012-08-01 | 中国石油化工股份有限公司 | 小晶粒zsm-5分子筛及其用途 |
| KR101147007B1 (ko) * | 2009-02-02 | 2012-05-22 | 한국과학기술원 | 싸이클릭다이암모늄을 이용한 메조기공 및 마크로기공을 추가적으로 포함하는 ｂｅａ, ｍｔｗ, ｍｆｉ 구조의 제올라이트의 제조과정 |
| US8951498B2 (en) * | 2010-07-30 | 2015-02-10 | University Of Iowa Research Foundation | Synthesis of hierarchical nanocrystalline zeolites with controlled particle size and mesoporosity |
| CN102372284B (zh) * | 2010-08-23 | 2013-01-09 | 中国石油化工股份有限公司 | 小晶粒zsm-5沸石的制备方法 |
| KR101923248B1 (ko) | 2011-08-04 | 2018-11-28 | 엑손모빌 케미칼 패턴츠 인코포레이티드 | Emm-23 분자체 물질, 그의 합성 및 용도 |
| CN102502696B (zh) | 2011-11-16 | 2014-04-23 | 大连理工大学 | 一种zsm-5沸石的合成方法 |
| SG11201503973UA (en) * | 2012-12-21 | 2015-06-29 | Exxonmobil Chem Patents Inc | Small crystal zsm-5, its synthesis and use |
| WO2014099261A1 (en) * | 2012-12-21 | 2014-06-26 | Exxonbobil Chemical Patents Inc. | Synthesis of zsm-5 |
-
2013
- 2013-11-22 SG SG11201503973UA patent/SG11201503973UA/en unknown
- 2013-11-22 WO PCT/US2013/071456 patent/WO2014099262A1/en not_active Ceased
- 2013-11-22 CN CN201380066799.8A patent/CN104870367B/zh active Active
- 2013-11-22 JP JP2015549410A patent/JP6238377B2/ja active Active
- 2013-11-22 EP EP16163846.5A patent/EP3056470B1/en active Active
- 2013-11-22 EP EP17186970.4A patent/EP3266747A1/en not_active Withdrawn
- 2013-11-22 KR KR1020157016273A patent/KR102166191B1/ko active Active
- 2013-11-22 EP EP13808320.9A patent/EP2935102B1/en active Active
- 2013-11-22 RU RU2015129627A patent/RU2640759C2/ru active
- 2013-11-22 CA CA2895232A patent/CA2895232C/en active Active
- 2013-11-22 US US14/648,800 patent/US10081552B2/en active Active
- 2013-11-22 CN CN201710862536.8A patent/CN107697928B/zh active Active
- 2013-11-22 SG SG10201705927UA patent/SG10201705927UA/en unknown
-
2015
- 2015-05-21 ZA ZA2015/03617A patent/ZA201503617B/en unknown
-
2018
- 2018-08-22 US US16/108,216 patent/US10662068B2/en active Active
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