JP2016128163A - 一定濃度の蒸発のための方法およびその方法を使用する装置 - Google Patents
一定濃度の蒸発のための方法およびその方法を使用する装置 Download PDFInfo
- Publication number
- JP2016128163A JP2016128163A JP2016000294A JP2016000294A JP2016128163A JP 2016128163 A JP2016128163 A JP 2016128163A JP 2016000294 A JP2016000294 A JP 2016000294A JP 2016000294 A JP2016000294 A JP 2016000294A JP 2016128163 A JP2016128163 A JP 2016128163A
- Authority
- JP
- Japan
- Prior art keywords
- evaporator
- precursor
- conduit
- heat exchanger
- inner casing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims abstract description 16
- 230000008020 evaporation Effects 0.000 title description 2
- 238000001704 evaporation Methods 0.000 title description 2
- 239000002243 precursor Substances 0.000 claims abstract description 144
- 239000012530 fluid Substances 0.000 claims abstract description 103
- 238000004891 communication Methods 0.000 claims abstract description 21
- 238000010438 heat treatment Methods 0.000 claims description 17
- 238000001816 cooling Methods 0.000 claims description 9
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 230000036760 body temperature Effects 0.000 claims 1
- 230000008569 process Effects 0.000 abstract description 5
- 239000007788 liquid Substances 0.000 description 13
- 229910052751 metal Inorganic materials 0.000 description 11
- 239000002184 metal Substances 0.000 description 11
- 239000000126 substance Substances 0.000 description 10
- -1 diisopropyl tellurium Chemical compound 0.000 description 8
- 239000000758 substrate Substances 0.000 description 8
- XCZXGTMEAKBVPV-UHFFFAOYSA-N trimethylgallium Chemical compound C[Ga](C)C XCZXGTMEAKBVPV-UHFFFAOYSA-N 0.000 description 7
- 239000000463 material Substances 0.000 description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- 239000000919 ceramic Substances 0.000 description 4
- 229920000642 polymer Polymers 0.000 description 4
- 239000004065 semiconductor Substances 0.000 description 4
- 238000003860 storage Methods 0.000 description 4
- RGGPNXQUMRMPRA-UHFFFAOYSA-N triethylgallium Chemical compound CC[Ga](CC)CC RGGPNXQUMRMPRA-UHFFFAOYSA-N 0.000 description 4
- 239000011701 zinc Substances 0.000 description 4
- 239000012159 carrier gas Substances 0.000 description 3
- 238000000151 deposition Methods 0.000 description 3
- 230000008021 deposition Effects 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 2
- 229910021627 Tin(IV) chloride Inorganic materials 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- ILAHWRKJUDSMFH-UHFFFAOYSA-N boron tribromide Chemical compound BrB(Br)Br ILAHWRKJUDSMFH-UHFFFAOYSA-N 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000005229 chemical vapour deposition Methods 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 239000002826 coolant Substances 0.000 description 2
- 239000012809 cooling fluid Substances 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- HQWPLXHWEZZGKY-UHFFFAOYSA-N diethylzinc Chemical compound CC[Zn]CC HQWPLXHWEZZGKY-UHFFFAOYSA-N 0.000 description 2
- AXAZMDOAUQTMOW-UHFFFAOYSA-N dimethylzinc Chemical compound C[Zn]C AXAZMDOAUQTMOW-UHFFFAOYSA-N 0.000 description 2
- ILXWFJOFKUNZJA-UHFFFAOYSA-N ethyltellanylethane Chemical compound CC[Te]CC ILXWFJOFKUNZJA-UHFFFAOYSA-N 0.000 description 2
- 239000006260 foam Substances 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- XCLKKWIIZMHQIV-UHFFFAOYSA-N isobutylgermane Chemical compound CC(C)C[Ge] XCLKKWIIZMHQIV-UHFFFAOYSA-N 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 238000012544 monitoring process Methods 0.000 description 2
- XHXFXVLFKHQFAL-UHFFFAOYSA-N phosphoryl trichloride Chemical compound ClP(Cl)(Cl)=O XHXFXVLFKHQFAL-UHFFFAOYSA-N 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 239000010453 quartz Substances 0.000 description 2
- 229920006395 saturated elastomer Polymers 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- 229910052714 tellurium Inorganic materials 0.000 description 2
- IEXRMSFAVATTJX-UHFFFAOYSA-N tetrachlorogermane Chemical compound Cl[Ge](Cl)(Cl)Cl IEXRMSFAVATTJX-UHFFFAOYSA-N 0.000 description 2
- HPGGPRDJHPYFRM-UHFFFAOYSA-J tin(iv) chloride Chemical compound Cl[Sn](Cl)(Cl)Cl HPGGPRDJHPYFRM-UHFFFAOYSA-J 0.000 description 2
- KKOFCVMVBJXDFP-UHFFFAOYSA-N triethylstibane Chemical compound CC[Sb](CC)CC KKOFCVMVBJXDFP-UHFFFAOYSA-N 0.000 description 2
- JLTRXTDYQLMHGR-UHFFFAOYSA-N trimethylaluminium Chemical compound C[Al](C)C JLTRXTDYQLMHGR-UHFFFAOYSA-N 0.000 description 2
- HTDIUWINAKAPER-UHFFFAOYSA-N trimethylarsine Chemical compound C[As](C)C HTDIUWINAKAPER-UHFFFAOYSA-N 0.000 description 2
- PORFVJURJXKREL-UHFFFAOYSA-N trimethylstibine Chemical compound C[Sb](C)C PORFVJURJXKREL-UHFFFAOYSA-N 0.000 description 2
- VXEGSRKPIUDPQT-UHFFFAOYSA-N 4-[4-(4-methoxyphenyl)piperazin-1-yl]aniline Chemical compound C1=CC(OC)=CC=C1N1CCN(C=2C=CC(N)=CC=2)CC1 VXEGSRKPIUDPQT-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 1
- 229910001218 Gallium arsenide Inorganic materials 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- PHSPJQZRQAJPPF-UHFFFAOYSA-N N-alpha-Methylhistamine Chemical compound CNCCC1=CN=CN1 PHSPJQZRQAJPPF-UHFFFAOYSA-N 0.000 description 1
- 239000004696 Poly ether ether ketone Substances 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- 229910001069 Ti alloy Inorganic materials 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 230000001154 acute effect Effects 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- VMPVEPPRYRXYNP-UHFFFAOYSA-I antimony(5+);pentachloride Chemical compound Cl[Sb](Cl)(Cl)(Cl)Cl VMPVEPPRYRXYNP-UHFFFAOYSA-I 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- JMBNQWNFNACVCB-UHFFFAOYSA-N arsenic tribromide Chemical compound Br[As](Br)Br JMBNQWNFNACVCB-UHFFFAOYSA-N 0.000 description 1
- 229940077468 arsenic tribromide Drugs 0.000 description 1
- OEYOHULQRFXULB-UHFFFAOYSA-N arsenic trichloride Chemical compound Cl[As](Cl)Cl OEYOHULQRFXULB-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- SLLGVCUQYRMELA-UHFFFAOYSA-N chlorosilicon Chemical compound Cl[Si] SLLGVCUQYRMELA-UHFFFAOYSA-N 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000002542 deteriorative effect Effects 0.000 description 1
- MROCJMGDEKINLD-UHFFFAOYSA-N dichlorosilane Chemical compound Cl[SiH2]Cl MROCJMGDEKINLD-UHFFFAOYSA-N 0.000 description 1
- BUMGIEFFCMBQDG-UHFFFAOYSA-N dichlorosilicon Chemical compound Cl[Si]Cl BUMGIEFFCMBQDG-UHFFFAOYSA-N 0.000 description 1
- 239000004205 dimethyl polysiloxane Substances 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000002019 doping agent Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- JMMJWXHSCXIWRF-UHFFFAOYSA-N ethyl(dimethyl)indigane Chemical compound CC[In](C)C JMMJWXHSCXIWRF-UHFFFAOYSA-N 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 description 1
- 230000009477 glass transition Effects 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 230000013632 homeostatic process Effects 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 229910052741 iridium Inorganic materials 0.000 description 1
- GKOZUEZYRPOHIO-UHFFFAOYSA-N iridium atom Chemical compound [Ir] GKOZUEZYRPOHIO-UHFFFAOYSA-N 0.000 description 1
- 230000007257 malfunction Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229910000510 noble metal Inorganic materials 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000013307 optical fiber Substances 0.000 description 1
- 230000005693 optoelectronics Effects 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 229910052763 palladium Inorganic materials 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 1
- 229920000058 polyacrylate Polymers 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 229920002530 polyetherether ketone Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920000098 polyolefin Polymers 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 1
- 239000004810 polytetrafluoroethylene Substances 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 229910052703 rhodium Inorganic materials 0.000 description 1
- 239000010948 rhodium Substances 0.000 description 1
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 229910052594 sapphire Inorganic materials 0.000 description 1
- 239000010980 sapphire Substances 0.000 description 1
- 229910000077 silane Inorganic materials 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- AIFMYMZGQVTROK-UHFFFAOYSA-N silicon tetrabromide Chemical compound Br[Si](Br)(Br)Br AIFMYMZGQVTROK-UHFFFAOYSA-N 0.000 description 1
- 239000005049 silicon tetrachloride Substances 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 230000028016 temperature homeostasis Effects 0.000 description 1
- QTQRGDBFHFYIBH-UHFFFAOYSA-N tert-butylarsenic Chemical compound CC(C)(C)[As] QTQRGDBFHFYIBH-UHFFFAOYSA-N 0.000 description 1
- ZGNPLWZYVAFUNZ-UHFFFAOYSA-N tert-butylphosphane Chemical compound CC(C)(C)P ZGNPLWZYVAFUNZ-UHFFFAOYSA-N 0.000 description 1
- 229920001169 thermoplastic Polymers 0.000 description 1
- 229920001187 thermosetting polymer Polymers 0.000 description 1
- 239000004416 thermosoftening plastic Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- FAQYAMRNWDIXMY-UHFFFAOYSA-N trichloroborane Chemical compound ClB(Cl)Cl FAQYAMRNWDIXMY-UHFFFAOYSA-N 0.000 description 1
- ZDHXKXAHOVTTAH-UHFFFAOYSA-N trichlorosilane Chemical compound Cl[SiH](Cl)Cl ZDHXKXAHOVTTAH-UHFFFAOYSA-N 0.000 description 1
- 239000005052 trichlorosilane Substances 0.000 description 1
- JOHWNGGYGAVMGU-UHFFFAOYSA-N trifluorochlorine Chemical compound FCl(F)F JOHWNGGYGAVMGU-UHFFFAOYSA-N 0.000 description 1
- VEDJZFSRVVQBIL-UHFFFAOYSA-N trisilane Chemical compound [SiH3][SiH2][SiH3] VEDJZFSRVVQBIL-UHFFFAOYSA-N 0.000 description 1
- 238000007740 vapor deposition Methods 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01B—BOILING; BOILING APPARATUS ; EVAPORATION; EVAPORATION APPARATUS
- B01B1/00—Boiling; Boiling apparatus for physical or chemical purposes ; Evaporation in general
- B01B1/005—Evaporation for physical or chemical purposes; Evaporation apparatus therefor, e.g. evaporation of liquids for gas phase reactions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01B—BOILING; BOILING APPARATUS ; EVAPORATION; EVAPORATION APPARATUS
- B01B1/00—Boiling; Boiling apparatus for physical or chemical purposes ; Evaporation in general
- B01B1/06—Preventing bumping
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/22—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the deposition of inorganic material, other than metallic material
- C23C16/30—Deposition of compounds, mixtures or solid solutions, e.g. borides, carbides, nitrides
- C23C16/34—Nitrides
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/4411—Cooling of the reaction chamber walls
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/4412—Details relating to the exhausts, e.g. pumps, filters, scrubbers, particle traps
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/448—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for generating reactive gas streams, e.g. by evaporation or sublimation of precursor materials
- C23C16/4481—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for generating reactive gas streams, e.g. by evaporation or sublimation of precursor materials by evaporation using carrier gas in contact with the source material
- C23C16/4482—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for generating reactive gas streams, e.g. by evaporation or sublimation of precursor materials by evaporation using carrier gas in contact with the source material by bubbling of carrier gas through liquid source material
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/448—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for generating reactive gas streams, e.g. by evaporation or sublimation of precursor materials
- C23C16/4486—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for generating reactive gas streams, e.g. by evaporation or sublimation of precursor materials by producing an aerosol and subsequent evaporation of the droplets or particles
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/455—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
- C23C16/45523—Pulsed gas flow or change of composition over time
- C23C16/45525—Atomic layer deposition [ALD]
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/50—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating using electric discharges
- C23C16/511—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating using electric discharges using microwave discharges
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/02104—Forming layers
- H01L21/02365—Forming inorganic semiconducting materials on a substrate
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T29/00—Metal working
- Y10T29/49—Method of mechanical manufacture
- Y10T29/49396—Condenser, evaporator or vaporizer making
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- General Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Computer Hardware Design (AREA)
- Inorganic Chemistry (AREA)
- Plasma & Fusion (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Manufacturing & Machinery (AREA)
- Dispersion Chemistry (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Power Engineering (AREA)
- Chemical Vapour Deposition (AREA)
- Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
【解決手段】熱交換器300は蒸発器100と流体連絡して、蒸発器は外部ケーシング102及び内部ケーシング110を含み、内部ケーシングはプレート200と接触し、内部ケーシングは第1の導管210及び第2の導管214を取り囲み、第1の導管は蒸発器にキャリア流体を導入し、第2の導管は前駆体を同伴したキャリア流体を取り出し、外部ケーシングは取り外し可能にプレートに取り付けられ、プレートは第1の前駆体導管306と接触し、第1の前駆体導管は熱交換器から蒸発器へ前駆体を導入し、熱交換器は、熱交換器と蒸発器の周りの周囲温度が約±35℃以内(境界値を含む)の量で変動する時、蒸発器内の前駆体を実質的に一定の温度に維持する距離で蒸発器の近傍に配置されている装置。
【選択図】図2
Description
本明細書において、熱交換器において前駆体を加熱または冷却する工程;前駆体を熱交換器から蒸発器に送り出す工程;キャリア流体を第1の導管を介して蒸発器に導入する工程;キャリア流体で前駆体をスパージする工程;並びに、前駆体を同伴したキャリア流体を第2の導管を介して蒸発器から取り出す工程;を含む方法であって、蒸発器は外部ケーシングおよび内部ケーシングを含み;内部ケーシングは外部ケーシング内に配置されており;内部ケーシングはプレートと接触しており;内部ケーシングは第1の導管および第2の導管を取り囲んでおり;熱交換器と蒸発器との近さは、熱交換器および蒸発器の周りの周囲温度が約±35℃以内(境界値を含む)の量で変動する場合に、蒸発器内の前駆体を実質的に一定の温度に維持するのに有効である;方法も開示される。
本明細書において、逆U字型導管をプレートの第1の穴の中に、逆J字型導管をプレートの第2の穴の中に、および第1の前駆体導管をプレートの第3の穴の中に配置する工程、ここで前記プレートは熱交換器に固定されている;並びに、熱交換器がプレートに接触している面と反対側のプレートの面上に内部ケーシングおよび外部ケーシングを配置する工程、ここで内部ケーシングは外部ケーシング内に収容されており、内部ケーシングは逆U字型導管、逆J字型導管および第1の前駆体導管を取り囲んでいる;を含む装置を製造する方法も開示される。
ある要素が別の要素「上」にあると称される場合には、その要素は当該別の要素上に直接存在しうるか、またはそれらの間に介在要素が存在しうると理解されるであろう。これに対して、ある要素が別の要素の「直接上」にあると称される場合には、介在要素は存在しない。本発明において使用される場合、用語「および/または」は関連して列挙された項目の1以上のいずれかおよび全ての組み合わせを包含する。本明細書において使用される場合、「基体」とは、蒸着によってその上に金属含有膜が堆積されるあらゆる表面をいう。
ある実施形態においては、熱交換器および蒸発器の周りの周囲温度が約±15℃以内(境界値を含む)の温度で、特に約±25℃以内(境界値を含む)の温度で、さらに特に約±35℃以内(境界値を含む)の温度で変動する場合に、第1の熱交換器の中央から蒸発器(またはバブラー)まで伸びる流体径路における前駆体の温度の変動はない。
102 外部ケーシング
104 第1の端部
106 第2の端部
108 第1のフランジ
110 内部ケーシング
112 第1の穴
114 第2の穴
116 第3の穴
118 空間
120 低レベルマーク
122 高レベルマーク
124 充填開始マーク
126 充填停止マーク
130、132 ポート
200 プレート
202 第2のフランジ
204 第1のポート
206 第2のポート
208 シールまたはガスケット
210 第1の導管
212 スパージャー
214 第2の導管
216 スプラッシュシールド
220 入口ポート
222 出口ポート
230 加熱または冷却ジャケット
300 熱交換器
302 第2の前駆体導管
304 外部ジャケット
306 第1の前駆体導管
308 レベル検出装置
312 熱電対または感温抵抗器
Claims (10)
- 蒸発器および熱交換器を含む装置であって、
熱交換器は蒸発器と流体連絡しており;
蒸発器は外部ケーシングおよび内部ケーシングを含み;内部ケーシングは外部ケーシング内に配置されており;内部ケーシングはプレートと接触しており;内部ケーシングは第1の導管および第2の導管を取り囲んでおり;
第1の導管は蒸発器にキャリア流体を導入するように機能し;
第2の導管は前駆体を同伴したキャリア流体を取り出すように機能し;
外部ケーシングは取り外し可能にプレートに取り付けられており;プレートは第1の前駆体導管と接触しており;第1の前駆体導管は熱交換器から蒸発器へ前駆体を導入するように機能し;熱交換器は、熱交換器および蒸発器の周りの周囲温度が±35℃以内の量で変動する場合に、熱交換器の中央から蒸発器まで伸びる流体経路における前駆体の温度の変動を±0.5℃以内に維持する距離で蒸発器の近傍に配置されている;
蒸発器および熱交換器を含む装置。 - 第1の導管が逆U字型導管であり、逆U字型導管が、キャリア流体を蒸発器に導入するための第1のポートと流体連絡している一方の端、およびスパージャーと流体連絡している反対側の端を有する、請求項1に記載の装置。
- 第2の導管が逆J字型導管であり、逆J字型導管が、前駆体を同伴したキャリア流体を蒸発器から取り出すための第2のポートと流体連絡している一方の端、およびスプラッシュシールドと流体連絡している反対側の端を有する、請求項1に記載の装置。
- 熱交換器と蒸発器との近さが、熱交換器および蒸発器の周りの周囲温度が±35℃以内の量で変動する場合に、キャリア流体の前駆体に対する重量比が0.5%以上の量で変化しないように維持する、請求項1に記載の装置。
- 熱交換器と蒸発器との近さが、熱交換器から蒸発器への流体経路における前駆体の温度の変動を±0.1℃以内に維持する、請求項1に記載の装置。
- 逆U字型導管がプレートの穴を通って蒸発器内に配置される、請求項2に記載の装置。
- 逆J字型導管がプレートの穴を通って蒸発器内に配置される、請求項3に記載の装置。
- 熱交換器において前駆体を加熱または冷却する工程;
前駆体を熱交換器から蒸発器に送り出す工程;
キャリア流体を第1の導管を介して蒸発器に導入する工程;
キャリア流体で前駆体をスパージする工程;並びに、
前駆体を同伴したキャリア流体を第2の導管を介して蒸発器から取り出す工程;を含み、
蒸発器は外部ケーシングおよび内部ケーシングを含み;内部ケーシングは外部ケーシング内に配置されており;内部ケーシングはプレートと接触しており;内部ケーシングは第1の導管および第2の導管を取り囲んでおり;
熱交換器と蒸発器との近さが、熱交換器および蒸発器の周りの周囲温度が±35℃以内の量で変動する場合に、熱交換器の中央から蒸発器まで伸びる流体経路における前駆体の温度の変動を±0.5℃以内に維持する;
方法。 - 外部ケーシングと内部ケーシングとの間の空間において流体を循環させることをさらに含む、請求項8に記載の方法。
- 第1の導管として逆U字型導管をプレートの第1の穴の中に、第2の導管として逆J字型導管をプレートの第2の穴の中に、および第1の前駆体導管をプレートの第3の穴の中に配置する工程、ここで、前記プレートは熱交換器に固定されている;並びに、
熱交換器がプレートに接触している面と反対側のプレートの面上に内部ケーシングおよび外部ケーシングを配置して蒸発器を形成する工程、ここで、内部ケーシングは外部ケーシング内に収容されており、内部ケーシングは逆U字型導管および逆J字型導管を取り囲んでおり、第1の前駆体導管は、内部ケーシングの内側が第1の前駆体導管と流体連絡するようにプレートに接続しており、熱交換器は、熱交換器および蒸発器の周りの周囲温度が±35℃以内の量で変動する場合に、熱交換器の中央から蒸発器まで伸びる流体経路中の前駆体の温度の変動を±0.5℃以内に維持する配管を介して熱交換器が蒸発器に接続することにより、蒸発器の近傍に配置されている;
を含む、請求項1に記載の装置を製造する方法。
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US12/687,288 US8555809B2 (en) | 2010-01-14 | 2010-01-14 | Method for constant concentration evaporation and a device using the same |
US12/687288 | 2010-01-14 |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2011002670A Division JP2011167680A (ja) | 2010-01-14 | 2011-01-11 | 一定濃度の蒸発のための方法およびその方法を使用する装置 |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2016128163A true JP2016128163A (ja) | 2016-07-14 |
JP6317375B2 JP6317375B2 (ja) | 2018-04-25 |
Family
ID=43608149
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2011002670A Withdrawn JP2011167680A (ja) | 2010-01-14 | 2011-01-11 | 一定濃度の蒸発のための方法およびその方法を使用する装置 |
JP2016000294A Active JP6317375B2 (ja) | 2010-01-14 | 2016-01-04 | 一定濃度の蒸発のための方法およびその方法を使用する装置 |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2011002670A Withdrawn JP2011167680A (ja) | 2010-01-14 | 2011-01-11 | 一定濃度の蒸発のための方法およびその方法を使用する装置 |
Country Status (6)
Country | Link |
---|---|
US (1) | US8555809B2 (ja) |
EP (1) | EP2345473B1 (ja) |
JP (2) | JP2011167680A (ja) |
KR (1) | KR101778622B1 (ja) |
CN (1) | CN102162092B (ja) |
TW (1) | TWI482875B (ja) |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7883745B2 (en) * | 2007-07-30 | 2011-02-08 | Micron Technology, Inc. | Chemical vaporizer for material deposition systems and associated methods |
US8555809B2 (en) * | 2010-01-14 | 2013-10-15 | Rohm And Haas Electronic Materials, Llc | Method for constant concentration evaporation and a device using the same |
WO2013126323A1 (en) * | 2012-02-23 | 2013-08-29 | Applied Materials, Inc. | Method and apparatus for precursor delivery |
KR101389011B1 (ko) * | 2012-03-28 | 2014-04-24 | 주식회사 유니텍스 | 소스 컨테이너 및 기상 증착용 반응로 |
US9957612B2 (en) | 2014-01-17 | 2018-05-01 | Ceres Technologies, Inc. | Delivery device, methods of manufacture thereof and articles comprising the same |
JP6094513B2 (ja) * | 2014-02-28 | 2017-03-15 | 東京エレクトロン株式会社 | 処理ガス発生装置、処理ガス発生方法、基板処理方法及び記憶媒体 |
DE102014106129A1 (de) * | 2014-04-30 | 2015-11-05 | Thyssenkrupp Ag | Verfahren und Vorrichtung zur kontinuierlichen Präkursorzuführung |
US9924837B1 (en) * | 2017-02-09 | 2018-03-27 | R. Joseph Trojan | Vacuum blender |
JP6965569B2 (ja) * | 2017-05-17 | 2021-11-10 | 住友電気工業株式会社 | ガラス原料容器 |
KR102344996B1 (ko) | 2017-08-18 | 2021-12-30 | 삼성전자주식회사 | 전구체 공급 유닛, 기판 처리 장치 및 그를 이용한 반도체 소자의 제조방법 |
KR102474052B1 (ko) * | 2018-01-15 | 2022-12-02 | 어플라이드 머티어리얼스, 인코포레이티드 | 반도체 제조 생산성을 위한 진보된 온도 모니터링 시스템 및 방법들 |
WO2020122884A1 (en) * | 2018-12-11 | 2020-06-18 | Applied Materials, Inc. | Ampoule splash mitigation |
CN113684471B (zh) * | 2021-08-02 | 2023-04-11 | 江苏鎏溪光学科技有限公司 | 一种化学气相沉积过程中反应气氛的监控系统及方法 |
Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5659134U (ja) * | 1979-10-09 | 1981-05-21 | ||
US4545801A (en) * | 1984-02-07 | 1985-10-08 | Sumitomo Electric Industries, Ltd. | Raw material supply device |
JPS61502888A (ja) * | 1984-08-02 | 1986-12-11 | エイ・ティ・アンド・ティ・コーポレーション | オプティカル・プリフォ−ム製造における蒸気吐出制御方法及びその装置 |
JPH01122835U (ja) * | 1988-02-03 | 1989-08-21 | ||
US4861524A (en) * | 1987-03-19 | 1989-08-29 | Merck Patent Gesellschaft Mit Beschrankter Haftung | Apparatus for producing a gas mixture by the saturation method |
JPH02145768A (ja) * | 1988-11-28 | 1990-06-05 | Koujiyundo Kagaku Kenkyusho:Kk | 液体原料気化装置 |
JPH05138008A (ja) * | 1990-10-22 | 1993-06-01 | Watkins Johnson Co | 液体源バブラー |
JPH06196419A (ja) * | 1992-12-24 | 1994-07-15 | Canon Inc | 化学気相堆積装置及びそれによる半導体装置の製造方法 |
JPH1085581A (ja) * | 1996-05-24 | 1998-04-07 | Ebara Corp | 気化器 |
JP2004027365A (ja) * | 2002-06-25 | 2004-01-29 | Samsung Electronics Co Ltd | 化学気相蒸着工程の原料物質供給装置 |
Family Cites Families (58)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1344423A (en) * | 1917-08-16 | 1920-06-22 | Morley Manker Company | Vaporizer for heavy oils |
US1770384A (en) * | 1927-04-05 | 1930-07-15 | Irving E Aske | Electric heater and vaporizer |
US2020038A (en) * | 1932-01-05 | 1935-11-05 | Brown Co | Multiple effect evaporator |
US1960098A (en) * | 1932-05-17 | 1934-05-22 | Breitenbach August | Humidifier or vaporizer |
DE687810C (de) * | 1936-06-24 | 1940-02-06 | Industriegasverwertung Ag F | igter Gase mit tiefliegendem Siedepunkt in Druckgas |
US2264926A (en) * | 1939-05-09 | 1941-12-02 | Raymond D York | Crucible furnace |
US2755293A (en) * | 1951-12-04 | 1956-07-17 | Barber Greene Co | Method of treating materials |
US2750758A (en) * | 1954-07-12 | 1956-06-19 | Mohawk Cabinet Company Inc | Automatic defrosting refrigerator cabinet |
US2896658A (en) * | 1954-12-13 | 1959-07-28 | Sam P Jones | Regulator-vaporizer for a liquefied gas carburetion system |
US2836412A (en) * | 1955-08-22 | 1958-05-27 | Titanium Metals Corp | Arc melting crucible |
US3000364A (en) * | 1957-01-30 | 1961-09-19 | Babcock & Wilcox Co | Reactor with superheater coil encircling heat carrier lift pipe |
US3078529A (en) * | 1959-04-24 | 1963-02-26 | Titanium Metals Corp | Melting crucible and cooling means therefor |
US3153439A (en) * | 1962-06-04 | 1964-10-20 | Carl E Golden | Liquid petroleum gas vaporizer |
US3398720A (en) * | 1966-09-26 | 1968-08-27 | Combustion Eng | Once-through steam generator having a central manifold and tube bundles of spiral tube construction |
US3407787A (en) * | 1967-01-03 | 1968-10-29 | Ransome Torck & Burner Co | Lpg vaporizer |
DE1619695A1 (de) * | 1967-02-21 | 1971-07-01 | Bayer Ag | Verfahren und Vorrichtung zum thermischen Behandeln von Fluessigkeiten |
US3728100A (en) * | 1969-09-03 | 1973-04-17 | Consarc Corp | Electric furnace,particularly of the type using a dry crucible to melt highly reactive metals,and method |
US3724530A (en) * | 1970-10-12 | 1973-04-03 | V Baglai | Apparatus for electroslag remelting of metals |
DE2243714C3 (de) * | 1972-09-06 | 1975-07-24 | Otto Junker Gmbh, 5107 Simmerath | Vakuuminduktionsofen fur die Beheizung und Behandlung metallischer Schmelzen |
GB1449724A (en) * | 1973-03-06 | 1976-09-15 | Philips Nv | Apparatus for evaporating liquids |
US3965871A (en) * | 1974-03-22 | 1976-06-29 | Morton Clyde M | Converter vaporizer |
CH619150A5 (ja) * | 1976-01-30 | 1980-09-15 | Vaclav Feres | |
JPS5364670A (en) * | 1976-11-20 | 1978-06-09 | Mitsui Eng & Shipbuild Co Ltd | Vaporizer for low temperature liquified gas |
CH662638A5 (de) * | 1982-11-24 | 1987-10-15 | Sulzer Ag | Waermeuebertragersystem, vorzugsweise fuer ein prozessgas. |
FR2540739A1 (fr) * | 1983-02-11 | 1984-08-17 | Elf France | Dispositif et installations pour la distillation par evaporation en couches minces, en particulier pour hydrocarbures, et procede de mise en oeuvre de ce dispositif |
US5356487A (en) * | 1983-07-25 | 1994-10-18 | Quantum Group, Inc. | Thermally amplified and stimulated emission radiator fiber matrix burner |
DE3332679C2 (de) * | 1983-09-10 | 1994-08-11 | Feres Vaclav | Dünnschichtverdampfer |
JP2502653B2 (ja) * | 1988-02-17 | 1996-05-29 | 松下電器産業株式会社 | 金属薄膜の製造装置 |
DE4107844A1 (de) * | 1991-03-12 | 1992-09-17 | Feres Vaclav | Duennschichtverdampfer |
DE4124018C1 (ja) * | 1991-07-19 | 1992-11-19 | Leybold Ag, 6450 Hanau, De | |
US5363694A (en) * | 1993-11-17 | 1994-11-15 | United Technologies Corporation | Ampoule rupture detection system |
DE19524261B4 (de) * | 1995-07-04 | 2006-08-17 | J. Eberspächer GmbH & Co. KG | Verfahren zum Starten eines Verdampfungsbrenners |
EP0814177A3 (en) * | 1996-05-23 | 2000-08-30 | Ebara Corporation | Vaporizer apparatus and film deposition apparatus therewith |
US5862605A (en) * | 1996-05-24 | 1999-01-26 | Ebara Corporation | Vaporizer apparatus |
DE69720631T2 (de) * | 1996-10-04 | 2003-10-16 | Shinko Electric Co Ltd | Verfahren zum Feilen von Metall auf einen hohen Reinheitsgrad |
TW565626B (en) * | 1996-11-20 | 2003-12-11 | Ebara Corp | Liquid feed vaporization system and gas injection device |
JPH10147870A (ja) * | 1996-11-20 | 1998-06-02 | Ebara Corp | 液体原料の気化装置 |
ITTO970080A1 (it) * | 1997-02-04 | 1998-08-04 | Marco Vincenzo Ginatta | Procedimento per la produzione elettrolitica di metalli |
US6637475B2 (en) * | 1997-07-11 | 2003-10-28 | Advanced Technology Materials, Inc. | Bulk chemical delivery system |
CN1242248A (zh) | 1998-02-27 | 2000-01-26 | 液体空气乔治洛德方法利用和研究有限公司 | 连续的气体饱和系统及方法 |
US6135433A (en) * | 1998-02-27 | 2000-10-24 | Air Liquide America Corporation | Continuous gas saturation system and method |
EP0962260B1 (en) * | 1998-05-28 | 2005-01-05 | Ulvac, Inc. | Material evaporation system |
US6202591B1 (en) * | 1998-11-12 | 2001-03-20 | Flex Products, Inc. | Linear aperture deposition apparatus and coating process |
JP3909792B2 (ja) * | 1999-08-20 | 2007-04-25 | パイオニア株式会社 | 化学気相成長法における原料供給装置及び原料供給方法 |
DE19963322B4 (de) * | 1999-12-21 | 2005-09-29 | Bernd Füsting | Sorptionswärmespeicher hoher Energiedichte |
US6505469B1 (en) * | 2001-10-15 | 2003-01-14 | Chart Inc. | Gas dispensing system for cryogenic liquid vessels |
US6799440B2 (en) * | 2002-02-22 | 2004-10-05 | General Electric Company | Optical fiber deposition tube fused in deuterium atmosphere for attenuation improvement |
US7601225B2 (en) * | 2002-06-17 | 2009-10-13 | Asm International N.V. | System for controlling the sublimation of reactants |
US6921062B2 (en) * | 2002-07-23 | 2005-07-26 | Advanced Technology Materials, Inc. | Vaporizer delivery ampoule |
US7011299B2 (en) * | 2002-09-16 | 2006-03-14 | Matheson Tri-Gas, Inc. | Liquid vapor delivery system and method of maintaining a constant level of fluid therein |
EP2369035B9 (en) * | 2003-08-04 | 2014-05-21 | LG Display Co., Ltd. | Evaporation source |
US7965441B2 (en) * | 2004-09-30 | 2011-06-21 | Industrial Technology Research Institute | Optical film with super low retardation and polarizing plate containing the same |
KR100697691B1 (ko) * | 2005-07-27 | 2007-03-20 | 삼성전자주식회사 | 소스 가스 공급 유닛 및 이를 갖는 화학 기상 증착 장치 |
US7464917B2 (en) * | 2005-10-07 | 2008-12-16 | Appiled Materials, Inc. | Ampoule splash guard apparatus |
US7775508B2 (en) * | 2006-10-31 | 2010-08-17 | Applied Materials, Inc. | Ampoule for liquid draw and vapor draw with a continuous level sensor |
US7736399B2 (en) * | 2006-11-07 | 2010-06-15 | Delphi Technologies, Inc. | Electrically-heated metal vaporizer for fuel/air preparation in a hydrocarbon reformer assembly |
WO2009134041A2 (en) * | 2008-04-29 | 2009-11-05 | Sunic System. Ltd. | Evaporator and vacuum deposition apparatus having the same |
US8555809B2 (en) * | 2010-01-14 | 2013-10-15 | Rohm And Haas Electronic Materials, Llc | Method for constant concentration evaporation and a device using the same |
-
2010
- 2010-01-14 US US12/687,288 patent/US8555809B2/en active Active
-
2011
- 2011-01-11 EP EP11150646.5A patent/EP2345473B1/en active Active
- 2011-01-11 JP JP2011002670A patent/JP2011167680A/ja not_active Withdrawn
- 2011-01-11 TW TW100100904A patent/TWI482875B/zh active
- 2011-01-13 KR KR1020110003494A patent/KR101778622B1/ko active IP Right Grant
- 2011-01-14 CN CN2011100249449A patent/CN102162092B/zh active Active
-
2016
- 2016-01-04 JP JP2016000294A patent/JP6317375B2/ja active Active
Patent Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5659134U (ja) * | 1979-10-09 | 1981-05-21 | ||
US4545801A (en) * | 1984-02-07 | 1985-10-08 | Sumitomo Electric Industries, Ltd. | Raw material supply device |
JPS61502888A (ja) * | 1984-08-02 | 1986-12-11 | エイ・ティ・アンド・ティ・コーポレーション | オプティカル・プリフォ−ム製造における蒸気吐出制御方法及びその装置 |
US4861524A (en) * | 1987-03-19 | 1989-08-29 | Merck Patent Gesellschaft Mit Beschrankter Haftung | Apparatus for producing a gas mixture by the saturation method |
JPH01122835U (ja) * | 1988-02-03 | 1989-08-21 | ||
JPH02145768A (ja) * | 1988-11-28 | 1990-06-05 | Koujiyundo Kagaku Kenkyusho:Kk | 液体原料気化装置 |
JPH05138008A (ja) * | 1990-10-22 | 1993-06-01 | Watkins Johnson Co | 液体源バブラー |
JPH06196419A (ja) * | 1992-12-24 | 1994-07-15 | Canon Inc | 化学気相堆積装置及びそれによる半導体装置の製造方法 |
JPH1085581A (ja) * | 1996-05-24 | 1998-04-07 | Ebara Corp | 気化器 |
JP2004027365A (ja) * | 2002-06-25 | 2004-01-29 | Samsung Electronics Co Ltd | 化学気相蒸着工程の原料物質供給装置 |
Also Published As
Publication number | Publication date |
---|---|
US8555809B2 (en) | 2013-10-15 |
EP2345473B1 (en) | 2016-10-12 |
CN102162092A (zh) | 2011-08-24 |
TWI482875B (zh) | 2015-05-01 |
EP2345473A3 (en) | 2012-02-29 |
JP2011167680A (ja) | 2011-09-01 |
KR20110083552A (ko) | 2011-07-20 |
EP2345473A2 (en) | 2011-07-20 |
JP6317375B2 (ja) | 2018-04-25 |
CN102162092B (zh) | 2013-12-18 |
KR101778622B1 (ko) | 2017-09-26 |
US20110171383A1 (en) | 2011-07-14 |
TW201137161A (en) | 2011-11-01 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
JP6317375B2 (ja) | 一定濃度の蒸発のための方法およびその方法を使用する装置 | |
JP6788067B2 (ja) | 蒸気送達装置、その製造方法およびその使用方法 | |
US20180334744A1 (en) | Evaporation vessel apparatus and method | |
US4979643A (en) | Chemical refill system | |
US9914997B2 (en) | Method for supplying a process with an enriched carrier gas | |
EP0229050B1 (en) | Chemical refill system |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20170302 |
|
A711 | Notification of change in applicant |
Free format text: JAPANESE INTERMEDIATE CODE: A711 Effective date: 20170309 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20170601 |
|
A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20170703 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20171002 |
|
TRDD | Decision of grant or rejection written | ||
A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20180305 |
|
A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20180329 |
|
R150 | Certificate of patent or registration of utility model |
Ref document number: 6317375 Country of ref document: JP Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |