JP2016124780A - 結合表面を横切る構造的および物理的特性を保持しつつセラミック発泡体を接合するための方法および処方 - Google Patents
結合表面を横切る構造的および物理的特性を保持しつつセラミック発泡体を接合するための方法および処方 Download PDFInfo
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- JP2016124780A JP2016124780A JP2015199216A JP2015199216A JP2016124780A JP 2016124780 A JP2016124780 A JP 2016124780A JP 2015199216 A JP2015199216 A JP 2015199216A JP 2015199216 A JP2015199216 A JP 2015199216A JP 2016124780 A JP2016124780 A JP 2016124780A
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Images
Classifications
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- C04B37/00—Joining burned ceramic articles with other burned ceramic articles or other articles by heating
- C04B37/001—Joining burned ceramic articles with other burned ceramic articles or other articles by heating directly with other burned ceramic articles
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- B32B5/22—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed
- B32B5/32—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed at least two layers being foamed and next to each other
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
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Abstract
【解決手段】少なくとも1つの繊維材料、フラックス剤、および増粘剤を含む、セラミック結合材料18であり、セラミック結合材料18は、2つの隣接する基材の面を結合するために、設定温度で焼成される。
【選択図】図1A
Description
グリーン結合材料が、以下の原料を混合することによって調製された。
NextelTM 312(アルミナ−ボリア−シリカ)チョップド繊維 12wt%
メタホウ酸リチウム粉末 0.1wt%
メチルセルロース 88wt%
必要に応じて、水
12、16 結合表面
18 結合材料層
19 アセンブリ
20 別個の基材
24 結合材料層
25 複雑なアセンブリ
Claims (15)
- 繊維材料と、
フラックス剤と、
増粘剤と、を含み、
繊維材料が、結合材料によって結合された少なくとも1つの基材構成要素のCTEと実質的に類似するCTEを有する、
結合材料。 - 繊維材料が、平均長さが約1/16インチから約1/2インチである、チョップド繊維である、請求項1に記載の結合材料。
- 繊維材料が、シリカ(SiO2)の繊維、アルミナ(Al2O3)の繊維、酸化ジルコニウム(ZrO2)の繊維、酸化チタン(TiO2)の繊維、アルミニウムシリケート(Al−Si−オキシド)の繊維、ホウケイ酸アルミニウム(アルカリ金属を有するまたは有さない)の繊維、炭素の繊維、ホウケイ酸の繊維、窒化ケイ素(SiN)の繊維、または炭化ケイ素(SiC)の繊維、およびこれらの繊維の組み合わせから選択される、請求項1または2に記載の結合材料。
- 繊維材料が、硬化される前に、約50wt%から約90wt%の範囲の量で、結合材料中に存在する、請求項1から3の何れか1項に記載の結合材料。
- フラックス剤が、炭酸ナトリウム、炭化ホウ素、メタホウ酸リチウム、ホウ酸カドミウム、ホウ酸リチウム、ホウ化ケイ素、ホウケイ酸カドミウム、酸化ビスマス、ホウケイ酸鉛、テトラホウ酸リチウム、ホウ酸カドミウム、ホウケイ酸カドミウム、またはホウケイ酸鉛、およびそれらの組み合わせである、請求項1から4の何れか1項に記載の結合材料。
- フラックス剤が、硬化される前に、約0.01wt%未満から約5wt%の範囲の量で、結合材料中に存在する、請求項1から5の何れか1項に記載の結合材料。
- 増粘剤が、澱粉、植物ガム、糖、タンパク質、ペクチン、セルロース系材料、ゼラチン、合成増粘剤、およびこれらの組み合わせであり、増粘剤が、硬化される前に、約0wt%を超えて約10wt%までの範囲の量で、結合材料中に存在する、請求項1から6の何れか1項に記載の結合材料。
- (a)第1の基材断片の第1の結合表面および第2の基材断片の第2の結合表面から選択された少なくとも1つの結合表面に結合材料を付ける段階であって、結合材料が繊維材料、フラックス剤、および増粘剤をさらに含み、繊維材料が第1および第2の基材の少なくとも1つのCTEと実質的に類似するCTEを有する、段階と、
(b)結合材料が第1の結合表面と第2の結合表面との間に配置され未硬化の結合材料を含むセラミック構造体を形成するように、第1の結合表面と第2の結合表面とを接合する段階と、
(c)約1,000℃から約1,600℃の温度で、硬化された結合材料を含むセラミック構造体が形成されるのに十分な時間、セラミック構造体を加熱する段階と、を含む、硬化されたセラミック構造体を形成する方法。 - 繊維材料が、平均長さが約1/16インチから約1/2インチである、チョップド繊維である、請求項8に記載の方法。
- 繊維材料が、シリカ(SiO2)の繊維、アルミナ(Al2O3)の繊維、酸化ジルコニウム(ZrO2)の繊維、酸化チタン(TiO2)の繊維、アルミニウムシリケート(Al−Si−オキシド)の繊維、ホウケイ酸アルミニウム(アルカリ金属を有するまたは有さない)の繊維、炭素の繊維、ホウケイ酸の繊維、窒化ケイ素(SiN)の繊維、または炭化ケイ素(SiC)の繊維、およびこれらの繊維の組み合わせから選択される、請求項8または9に記載の方法。
- 繊維材料が、硬化される前に、約50wt%から約90wt%の範囲の量で、結合材料中に存在する、請求項8から10の何れか1項に記載の方法。
- フラックス剤が、炭酸ナトリウム、炭化ホウ素、メタホウ酸リチウム、ホウ酸カドミウム、ホウ酸リチウム、ホウ化ケイ素、ホウケイ酸カドミウム、酸化ビスマス、ホウケイ酸鉛、テトラホウ酸リチウム、ホウ酸カドミウム、ホウケイ酸カドミウム、またはホウケイ酸鉛、およびそれらの組み合わせであり、フラックス剤が、硬化される前に、約0.01wt%未満から約5wt%の範囲の量で、結合材料中に存在する、請求項8から11の何れか1項に記載の方法。
- 増粘剤が、澱粉、植物ガム、糖、タンパク質、ペクチン、セルロース系材料、ゼラチン、合成増粘剤、およびこれらの組み合わせであり、増粘剤が、硬化される前に、約0wt%を超えて約10wt%までの範囲の量で、結合材料中に存在する、請求項8から12の何れか1項に記載の方法。
- 結合材料が、
約1/16インチから約1/2インチの平均長さを有するチョップドホウケイ酸アルミニウム繊維を約50wt%から約90wt%、
約0.01wt%未満から約5wt%のメタホウ酸リチウム、および
約0wt%を超えて約10wt%までのメチルセルロース、を含む水性混合物であり、
ホウケイ酸アルミニウムは、結合材料によって結合される少なくとも1つの基材のCTEと実質的に類似するCTEを有する、請求項8〜13の何れか1項に記載の方法。 - 結合表面を有する第1のセラミック発泡体基材、結合表面を有する第2のセラミック発泡体基材を含み、第1および第2の基材は、請求項26〜32の何れか1項に記載の方法により接合され、実質的に同じCTEを有する複合材料構造体。
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US9463880B2 (en) | 2013-02-07 | 2016-10-11 | The Boeing Company | Method and system of making composite structures having gap fillers with chopped fiber material |
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JP2020050583A (ja) * | 2018-09-26 | 2020-04-02 | ザ・ボーイング・カンパニーThe Boeing Company | セラミック組成物およびセラミック組成物を製造する方法 |
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AU2015243021A1 (en) | 2016-07-14 |
US20200224003A1 (en) | 2020-07-16 |
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JP6664181B2 (ja) | 2020-03-13 |
EP3040322B1 (en) | 2022-02-23 |
RU2698658C9 (ru) | 2019-11-28 |
CN105732069B (zh) | 2021-03-16 |
US20160185935A1 (en) | 2016-06-30 |
US11718731B2 (en) | 2023-08-08 |
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RU2015141771A (ru) | 2017-04-06 |
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