JP2015518511A5 - - Google Patents
Download PDFInfo
- Publication number
- JP2015518511A5 JP2015518511A5 JP2015505968A JP2015505968A JP2015518511A5 JP 2015518511 A5 JP2015518511 A5 JP 2015518511A5 JP 2015505968 A JP2015505968 A JP 2015505968A JP 2015505968 A JP2015505968 A JP 2015505968A JP 2015518511 A5 JP2015518511 A5 JP 2015518511A5
- Authority
- JP
- Japan
- Prior art keywords
- reaction mixture
- oil
- mixture
- alcohol
- conversion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000011541 reaction mixture Substances 0.000 claims description 45
- 238000000034 method Methods 0.000 claims description 30
- 229910002651 NO3 Inorganic materials 0.000 claims description 28
- 238000006243 chemical reaction Methods 0.000 claims description 20
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims description 19
- 229910052799 carbon Inorganic materials 0.000 claims description 18
- 150000001875 compounds Chemical class 0.000 claims description 17
- 239000000203 mixture Substances 0.000 claims description 16
- -1 nitrate compound Chemical class 0.000 claims description 14
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 11
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 claims description 8
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 claims description 8
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 claims description 4
- AHRQMWOXLCFNAV-UHFFFAOYSA-O ethylammonium nitrate Chemical compound CC[NH3+].[O-][N+]([O-])=O AHRQMWOXLCFNAV-UHFFFAOYSA-O 0.000 claims description 4
- 150000002430 hydrocarbons Chemical group 0.000 claims description 4
- 235000010333 potassium nitrate Nutrition 0.000 claims description 4
- 239000004323 potassium nitrate Substances 0.000 claims description 4
- 235000010344 sodium nitrate Nutrition 0.000 claims description 4
- 239000004317 sodium nitrate Substances 0.000 claims description 4
- 229930195733 hydrocarbon Natural products 0.000 claims description 3
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 2
- 229910017604 nitric acid Inorganic materials 0.000 claims description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 22
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 18
- 239000003921 oil Substances 0.000 claims 12
- 238000001816 cooling Methods 0.000 claims 5
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 3
- 238000001914 filtration Methods 0.000 claims 3
- 238000010438 heat treatment Methods 0.000 claims 3
- DIVJHHZLRGLYFL-UHFFFAOYSA-N 3-[tris(2,4,5-trioxa-1-azabicyclo[1.1.1]pentan-3-yl)methyl]-2,4,5-trioxa-1-azabicyclo[1.1.1]pentane Chemical compound O1N2OC1(O2)C(C12ON(O1)O2)(C12ON(O1)O2)C12ON(O1)O2 DIVJHHZLRGLYFL-UHFFFAOYSA-N 0.000 claims 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims 2
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims 2
- DKGAVHZHDRPRBM-UHFFFAOYSA-N Tert-Butanol Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 claims 2
- 235000019441 ethanol Nutrition 0.000 claims 2
- 239000010705 motor oil Substances 0.000 claims 2
- 239000003208 petroleum Substances 0.000 claims 2
- 229910000029 sodium carbonate Inorganic materials 0.000 claims 2
- 235000017550 sodium carbonate Nutrition 0.000 claims 2
- 239000004215 Carbon black (E152) Substances 0.000 claims 1
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims 1
- 238000010521 absorption reaction Methods 0.000 claims 1
- 230000002378 acidificating effect Effects 0.000 claims 1
- 239000002585 base Substances 0.000 claims 1
- 230000003197 catalytic effect Effects 0.000 claims 1
- 239000010779 crude oil Substances 0.000 claims 1
- 238000004821 distillation Methods 0.000 claims 1
- 239000000446 fuel Substances 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 239000002245 particle Substances 0.000 claims 1
- 235000011118 potassium hydroxide Nutrition 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
- 235000011121 sodium hydroxide Nutrition 0.000 claims 1
- 238000005979 thermal decomposition reaction Methods 0.000 claims 1
- 239000010913 used oil Substances 0.000 claims 1
- 238000005292 vacuum distillation Methods 0.000 claims 1
- 230000003313 weakening effect Effects 0.000 claims 1
- 230000009257 reactivity Effects 0.000 description 2
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US13/445,738 US8492601B1 (en) | 2012-04-12 | 2012-04-12 | Methods for converting used oil into fuel |
| US13/445,738 | 2012-04-12 | ||
| PCT/US2013/036503 WO2013155498A1 (en) | 2012-04-12 | 2013-04-12 | Methods and systems for obtaining long chain carbons from petroleum based oil |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2017185540A Division JP6462083B2 (ja) | 2012-04-12 | 2017-09-27 | 石油系油から長鎖炭素を得るための方法及びシステム |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015518511A JP2015518511A (ja) | 2015-07-02 |
| JP2015518511A5 true JP2015518511A5 (enExample) | 2016-07-14 |
| JP6219369B2 JP6219369B2 (ja) | 2017-10-25 |
Family
ID=48792323
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015505703A Expired - Fee Related JP6170133B2 (ja) | 2012-04-12 | 2013-01-14 | 使用済み油を燃料へ変換する方法 |
| JP2015505968A Expired - Fee Related JP6219369B2 (ja) | 2012-04-12 | 2013-04-12 | 石油系油から長鎖炭素を得るための方法及びシステム |
| JP2017185540A Expired - Fee Related JP6462083B2 (ja) | 2012-04-12 | 2017-09-27 | 石油系油から長鎖炭素を得るための方法及びシステム |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015505703A Expired - Fee Related JP6170133B2 (ja) | 2012-04-12 | 2013-01-14 | 使用済み油を燃料へ変換する方法 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2017185540A Expired - Fee Related JP6462083B2 (ja) | 2012-04-12 | 2017-09-27 | 石油系油から長鎖炭素を得るための方法及びシステム |
Country Status (6)
| Country | Link |
|---|---|
| US (3) | US8492601B1 (enExample) |
| EP (2) | EP2836574A4 (enExample) |
| JP (3) | JP6170133B2 (enExample) |
| CA (2) | CA2869709A1 (enExample) |
| HK (1) | HK1207393A1 (enExample) |
| WO (2) | WO2013154627A1 (enExample) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8492601B1 (en) * | 2012-04-12 | 2013-07-23 | OTG Research, LLC | Methods for converting used oil into fuel |
| US8859833B2 (en) * | 2011-04-12 | 2014-10-14 | OTG Research, LLC | Methods and systems for obtaining long chain carbons from petroleum based oil |
| CN113234478B (zh) * | 2021-05-25 | 2022-10-11 | 山东交通学院 | 将废弃机油残留物沥青化的装置、方法及应用 |
Family Cites Families (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3124525A (en) * | 1964-03-10 | Ozone generator | ||
| US2474411A (en) * | 1948-03-17 | 1949-06-28 | Frederick C Bersworth | Method of reclaiming the hydrocarbon content of used hydrocarbon lubricants |
| US3607731A (en) * | 1969-04-09 | 1971-09-21 | Quvoe Chemical Ind Inc | Re-refined waste crankcase oils and method |
| US4260132A (en) * | 1979-08-06 | 1981-04-07 | Caterpillar Tractor Co. | Control valve with improved centering and detent mechanisms |
| EP0236021A3 (en) | 1986-02-24 | 1989-01-25 | ENSR Corporation (a Delaware Corporation) | Process for upgrading diesel oils |
| US4746420A (en) * | 1986-02-24 | 1988-05-24 | Rei Technologies, Inc. | Process for upgrading diesel oils |
| SU1442537A1 (ru) * | 1986-04-16 | 1988-12-07 | Институт химии им.В.И.Никитина | Способ регенерации отработанного моторного масла |
| US5141628A (en) * | 1987-08-19 | 1992-08-25 | Rwe-Entsorgung Aktiengesellschaft | Method of cleaning and regenerating used oils |
| AU5607594A (en) * | 1992-11-17 | 1994-06-08 | Green Oasis Environmental Inc. | A process for converting waste motor oil to diesel fuel |
| US5424467A (en) * | 1993-07-14 | 1995-06-13 | Idaho Research Foundation | Method for purifying alcohol esters |
| JP2000219886A (ja) * | 1999-02-01 | 2000-08-08 | Masatoshi Matsumura | 植物油（バージン油）又は植物性廃油のディーゼルエンジン用燃料化精製方法及び装置 |
| US6190541B1 (en) * | 1999-05-11 | 2001-02-20 | Exxon Research And Engineering Company | Process for treatment of petroleum acids (LAW824) |
| US20010020344A1 (en) | 1999-07-07 | 2001-09-13 | Thompson Claire L. | Emulsifier for an aqueous hydrocarbon fuel |
| CA2336513C (en) * | 2000-02-17 | 2010-08-24 | Tatsuo Tateno | Process for producing fatty acid esters and fuels comprising fatty acid ester |
| JP2003176492A (ja) * | 2001-12-12 | 2003-06-24 | Nisseki Technologies Co Ltd | 廃油再生処理剤及び廃油再生処理方法 |
| ES2201894B2 (es) * | 2002-01-18 | 2005-03-01 | Industrial Management, S.A | Procedimiento para producir combustibles biodiesel con propiedades mejoradas a baja temperatura. |
| JP2004124008A (ja) | 2002-10-07 | 2004-04-22 | Foundation For Advancement Of International Science | 植物油燃料の製造方法 |
| JP2006249419A (ja) * | 2005-02-10 | 2006-09-21 | Kokyo Sangyo Kk | 廃油の再生処理方法および再生処理剤 |
| WO2007062304A2 (en) | 2005-11-23 | 2007-05-31 | Novus International, Inc. | Biodiesel fuel compositions having increased oxidative stability |
| CA2631848C (en) * | 2005-12-12 | 2012-09-04 | Neste Oil Oyj | Process for producing a saturated hydrocarbon component |
| TW200831660A (en) | 2007-01-16 | 2008-08-01 | Yi-Hung Chen | Method of enhancing the oil conversion ratio |
| KR100778532B1 (ko) * | 2007-04-13 | 2007-11-28 | 최홍윤 | 폐유 처리방법 |
| WO2010006228A2 (en) * | 2008-07-11 | 2010-01-14 | Eudes De Crecy | A method of producing fatty acids for biofuel, biodiesel, and other valuable chemicals |
| US8859833B2 (en) * | 2011-04-12 | 2014-10-14 | OTG Research, LLC | Methods and systems for obtaining long chain carbons from petroleum based oil |
| US8492601B1 (en) * | 2012-04-12 | 2013-07-23 | OTG Research, LLC | Methods for converting used oil into fuel |
-
2012
- 2012-04-12 US US13/445,738 patent/US8492601B1/en not_active Expired - Fee Related
-
2013
- 2013-01-14 CA CA2869709A patent/CA2869709A1/en not_active Abandoned
- 2013-01-14 JP JP2015505703A patent/JP6170133B2/ja not_active Expired - Fee Related
- 2013-01-14 WO PCT/US2013/021467 patent/WO2013154627A1/en not_active Ceased
- 2013-01-14 EP EP13775645.8A patent/EP2836574A4/en not_active Withdrawn
- 2013-01-14 HK HK15107989.1A patent/HK1207393A1/xx unknown
- 2013-04-12 EP EP13775344.8A patent/EP2836573A4/en not_active Withdrawn
- 2013-04-12 WO PCT/US2013/036503 patent/WO2013155498A1/en not_active Ceased
- 2013-04-12 JP JP2015505968A patent/JP6219369B2/ja not_active Expired - Fee Related
- 2013-04-12 CA CA2869768A patent/CA2869768A1/en not_active Abandoned
- 2013-07-10 US US13/939,129 patent/US9006504B2/en not_active Expired - Fee Related
-
2015
- 2015-04-09 US US14/682,642 patent/US9499754B2/en not_active Expired - Fee Related
-
2017
- 2017-09-27 JP JP2017185540A patent/JP6462083B2/ja not_active Expired - Fee Related
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Panitchakarn et al. | Synthesis of high-purity Na-A and Na-X zeolite from coal fly ash | |
| Cho et al. | Transesterification of tributyrin with methanol over calcium oxide catalysts prepared from various precursors | |
| EA201600533A1 (ru) | Катализатор и способ ароматизации c-cгазов, легких углеводородных фракций и алифатических спиртов, а также их смесей | |
| US20120304530A1 (en) | Bio-Oil Upgrading Process | |
| CN102442679A (zh) | 一种菱沸石的合成方法 | |
| KR20120102381A (ko) | 열안정성이 향상된 액체연료 조성물 | |
| CN101270297A (zh) | 煤基合成气钴基费托合成液体燃料并附产芳烃的工艺 | |
| JP2015518511A5 (enExample) | ||
| Ding et al. | Effect of calcination temperature on the structure and catalytic performance of the cu-mcm-41 catalysts for the synthesis of dimethyl carbonate | |
| CN102557869B (zh) | 一种由生物质炭制备甲醇燃料的方法 | |
| KR20100052089A (ko) | 고산도 원유 중의 산성분 제거를 위한 촉매 및 그 제법 | |
| RU2010122282A (ru) | Катализатор и способ получения алифатических углеводородов из оксида углерода и водорода в его присутствии | |
| Lin et al. | Application of mesoporous catalysts over palm-oil biodiesel for adjusting fuel properties | |
| Tang et al. | Synthesis of no‐glycerol biodiesel through transesterification catalyzed by CaO from different precursors | |
| JP5755677B2 (ja) | Ｚｓｍ−５の製造方法 | |
| JP2015512996A5 (enExample) | ||
| CN101659878A (zh) | 改进型废轮胎油脱色、去味再生技术及其调配柴油的方法 | |
| CN103396827B (zh) | 煤液化油中碱性氮化合物的分离方法 | |
| JP2009515697A5 (enExample) | ||
| JP2017031042A (ja) | 活性炭の製造方法および活性炭 | |
| CN102824903A (zh) | 一种以白云石为原料制备的多孔固体碱催化剂及其应用 | |
| Kumagai et al. | Catalytic degradation of poly (ethylene terephthalate) for benzene-rich oil recovery using metal hydroxides | |
| CN102180445B (zh) | 一种高容量储氢材料硼氢化对/间苯二胺的制备方法 | |
| RU2520207C2 (ru) | Способ подготовки топливного газа | |
| Maloletnev et al. | Catalytic cracking of the semicoking tar of coal from the Shubarkol deposit |