JP2014524940A5 - - Google Patents
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- Publication number
- JP2014524940A5 JP2014524940A5 JP2014502874A JP2014502874A JP2014524940A5 JP 2014524940 A5 JP2014524940 A5 JP 2014524940A5 JP 2014502874 A JP2014502874 A JP 2014502874A JP 2014502874 A JP2014502874 A JP 2014502874A JP 2014524940 A5 JP2014524940 A5 JP 2014524940A5
- Authority
- JP
- Japan
- Prior art keywords
- prepreg
- type epoxy
- temperature
- epoxy resin
- curing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003822 epoxy resin Substances 0.000 claims description 41
- 229920000647 polyepoxide Polymers 0.000 claims description 41
- 229920001187 thermosetting polymer Polymers 0.000 claims description 17
- 229920005989 resin Polymers 0.000 claims description 16
- 239000011347 resin Substances 0.000 claims description 16
- 238000000034 method Methods 0.000 claims description 11
- PXKLMJQFEQBVLD-UHFFFAOYSA-N bisphenol F Chemical compound C1=CC(O)=CC=C1CC1=CC=C(O)C=C1 PXKLMJQFEQBVLD-UHFFFAOYSA-N 0.000 claims description 10
- 239000011342 resin composition Substances 0.000 claims description 9
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 claims description 8
- 239000003733 fiber-reinforced composite Substances 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 6
- CDAWCLOXVUBKRW-UHFFFAOYSA-N 2-aminophenol Chemical compound NC1=CC=CC=C1O CDAWCLOXVUBKRW-UHFFFAOYSA-N 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 229920003986 novolac Polymers 0.000 claims description 3
- VAUOPRZOGIRSMI-UHFFFAOYSA-N n-(oxiran-2-ylmethyl)aniline Chemical compound C1OC1CNC1=CC=CC=C1 VAUOPRZOGIRSMI-UHFFFAOYSA-N 0.000 claims description 2
- 238000001723 curing Methods 0.000 claims 10
- 239000010410 layer Substances 0.000 claims 8
- 238000000465 moulding Methods 0.000 claims 7
- 239000002245 particle Substances 0.000 claims 6
- 230000001186 cumulative effect Effects 0.000 claims 4
- 238000009826 distribution Methods 0.000 claims 3
- 239000011159 matrix material Substances 0.000 claims 3
- 239000012783 reinforcing fiber Substances 0.000 claims 3
- 238000000790 scattering method Methods 0.000 claims 3
- 238000010030 laminating Methods 0.000 claims 2
- 238000007872 degassing Methods 0.000 claims 1
- 239000000835 fiber Substances 0.000 claims 1
- 238000001879 gelation Methods 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 238000005470 impregnation Methods 0.000 claims 1
- 239000011229 interlayer Substances 0.000 claims 1
- 150000002924 oxiranes Chemical class 0.000 claims 1
- 229920005992 thermoplastic resin Polymers 0.000 claims 1
- LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 18
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- QTWJRLJHJPIABL-UHFFFAOYSA-N 2-methylphenol;3-methylphenol;4-methylphenol Chemical compound CC1=CC=C(O)C=C1.CC1=CC=CC(O)=C1.CC1=CC=CC=C1O QTWJRLJHJPIABL-UHFFFAOYSA-N 0.000 description 3
- 150000001412 amines Chemical class 0.000 description 3
- 229930003836 cresol Natural products 0.000 description 3
- 239000002243 precursor Substances 0.000 description 3
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N diphenyl Chemical compound C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 2
- IGALFTFNPPBUDN-UHFFFAOYSA-N phenyl-[2,3,4,5-tetrakis(oxiran-2-ylmethyl)phenyl]methanediamine Chemical compound C=1C(CC2OC2)=C(CC2OC2)C(CC2OC2)=C(CC2OC2)C=1C(N)(N)C1=CC=CC=C1 IGALFTFNPPBUDN-UHFFFAOYSA-N 0.000 description 2
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 2
- PUFWGUZSDHANBX-UHFFFAOYSA-N 1-phenyl-9h-fluorene Chemical compound C=12CC3=CC=CC=C3C2=CC=CC=1C1=CC=CC=C1 PUFWGUZSDHANBX-UHFFFAOYSA-N 0.000 description 1
- HECLRDQVFMWTQS-RGOKHQFPSA-N 1755-01-7 Chemical compound C1[C@H]2[C@@H]3CC=C[C@@H]3[C@@H]1C=C2 HECLRDQVFMWTQS-RGOKHQFPSA-N 0.000 description 1
- FLROJJGKUKLCAE-UHFFFAOYSA-N 3-amino-2-methylphenol Chemical compound CC1=C(N)C=CC=C1O FLROJJGKUKLCAE-UHFFFAOYSA-N 0.000 description 1
- VPWNQTHUCYMVMZ-UHFFFAOYSA-N 4,4'-sulfonyldiphenol Chemical compound C1=CC(O)=CC=C1S(=O)(=O)C1=CC=C(O)C=C1 VPWNQTHUCYMVMZ-UHFFFAOYSA-N 0.000 description 1
- CXXSQMDHHYTRKY-UHFFFAOYSA-N 4-amino-2,3,5-tris(oxiran-2-ylmethyl)phenol Chemical compound C1=C(O)C(CC2OC2)=C(CC2OC2)C(N)=C1CC1CO1 CXXSQMDHHYTRKY-UHFFFAOYSA-N 0.000 description 1
- 229920000049 Carbon (fiber) Polymers 0.000 description 1
- 235000010290 biphenyl Nutrition 0.000 description 1
- 239000004305 biphenyl Substances 0.000 description 1
- 239000004917 carbon fiber Substances 0.000 description 1
- 239000011203 carbon fibre reinforced carbon Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- GYZLOYUZLJXAJU-UHFFFAOYSA-N diglycidyl ether Chemical compound C1OC1COCC1CO1 GYZLOYUZLJXAJU-UHFFFAOYSA-N 0.000 description 1
- 150000002118 epoxides Chemical class 0.000 description 1
- 230000020169 heat generation Effects 0.000 description 1
- 125000001624 naphthyl group Chemical group 0.000 description 1
- AFEQENGXSMURHA-UHFFFAOYSA-N oxiran-2-ylmethanamine Chemical compound NCC1CO1 AFEQENGXSMURHA-UHFFFAOYSA-N 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161469529P | 2011-03-30 | 2011-03-30 | |
| US61/469,529 | 2011-03-30 | ||
| US201261586232P | 2012-01-13 | 2012-01-13 | |
| US61/586,232 | 2012-01-13 | ||
| PCT/US2012/031672 WO2012135754A1 (en) | 2011-03-30 | 2012-03-30 | Prepreg, fiber reinforced composite material, and manufacturing method for fiber reinforced composite material |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2014524940A JP2014524940A (ja) | 2014-09-25 |
| JP2014524940A5 true JP2014524940A5 (enExample) | 2015-04-09 |
| JP5971325B2 JP5971325B2 (ja) | 2016-08-17 |
Family
ID=46931959
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014502874A Active JP5971325B2 (ja) | 2011-03-30 | 2012-03-30 | プリプレグ、繊維強化複合材料、および繊維強化複合材料の製造方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US20140087178A1 (enExample) |
| EP (1) | EP2691199B1 (enExample) |
| JP (1) | JP5971325B2 (enExample) |
| KR (1) | KR101951058B1 (enExample) |
| CN (1) | CN103429371B (enExample) |
| BR (1) | BR112013024886A2 (enExample) |
| CA (1) | CA2830836A1 (enExample) |
| RU (1) | RU2013148117A (enExample) |
| WO (1) | WO2012135754A1 (enExample) |
Families Citing this family (47)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2888306B1 (en) * | 2012-11-15 | 2019-09-25 | Cytec Industries Inc. | Thermoset resin composite materials comprising inter-laminar toughening particles |
| US9205633B2 (en) * | 2013-03-15 | 2015-12-08 | Henkel IP & Holding GmbH | Prepreg curing process for preparing composites having superior surface finish and high fiber consolidation |
| CN105102513A (zh) * | 2013-03-29 | 2015-11-25 | 吉坤日矿日石能源株式会社 | 纤维强化复合材料的制造方法 |
| KR20180127543A (ko) * | 2013-12-06 | 2018-11-28 | 미쯔비시 케미컬 주식회사 | 섬유 강화 열가소성 플라스틱을 이용한 적층 기재와 이것을 이용한 성형품의 제조 방법 |
| JP6210007B2 (ja) * | 2014-03-26 | 2017-10-11 | 東レ株式会社 | プリプレグおよびその製造方法、ならびに炭素繊維強化複合材料 |
| CN106170525A (zh) * | 2014-04-14 | 2016-11-30 | 陶氏环球技术有限责任公司 | 用于预胶凝烘箱的环氧树脂组合物 |
| CA2957157A1 (en) * | 2014-09-19 | 2016-03-24 | Toray Industries, Inc. | Process for producing fiber-reinforced plastic |
| US10662302B2 (en) * | 2014-09-23 | 2020-05-26 | The Boeing Company | Polymer nanoparticles for improved distortion capability in composites |
| US9587076B2 (en) * | 2014-09-23 | 2017-03-07 | The Boeing Company | Polymer nanoparticles for controlling resin reaction rates |
| US10808123B2 (en) | 2014-09-23 | 2020-10-20 | The Boeing Company | Nanoparticles for improving the dimensional stability of resins |
| US10472472B2 (en) | 2014-09-23 | 2019-11-12 | The Boeing Company | Placement of modifier material in resin-rich pockets to mitigate microcracking in a composite structure |
| US10072126B2 (en) | 2014-09-23 | 2018-09-11 | The Boeing Company | Soluble nanoparticles for composite performance enhancement |
| ES2845687T3 (es) * | 2015-01-07 | 2021-07-27 | Toray Industries | Material preimpregnado |
| US10479029B2 (en) * | 2015-01-16 | 2019-11-19 | The Boeing Company | Composite forming apparatus |
| US10201959B2 (en) | 2015-01-30 | 2019-02-12 | The Boeing Company | Gradient curing of composite laminate parts |
| US20170021596A1 (en) * | 2015-05-05 | 2017-01-26 | Sunrez Corp. | Fiber Reinforced Core |
| CN104875790A (zh) * | 2015-05-26 | 2015-09-02 | 北京汽车股份有限公司 | 一种车顶盖及车顶盖的加工方法 |
| KR20180095502A (ko) * | 2015-12-16 | 2018-08-27 | 도레이 카부시키가이샤 | 프리프레그, 적층체, 섬유 강화 복합 재료, 및 섬유 강화 복합 재료의 제조 방법 |
| CN105415775A (zh) * | 2015-12-30 | 2016-03-23 | 联想(北京)有限公司 | 碳纤维板和电子设备 |
| CN105907062B (zh) * | 2016-05-10 | 2018-01-02 | 中南林业科技大学 | 高强低密度天然植物纤维增强聚己内酯复合材料及其制备方法 |
| US11090899B2 (en) * | 2016-05-26 | 2021-08-17 | Hanwha Azdel, Inc. | Prepregs, cores and composite articles including powder coated layers |
| US10472474B2 (en) | 2016-06-22 | 2019-11-12 | Hexcel Corporation | Semipreg with thermoplastic toughened novolac-based epoxy resin matrix |
| WO2018066600A1 (ja) * | 2016-10-04 | 2018-04-12 | 三菱ケミカル株式会社 | プリプレグ、プリプレグ積層体、および繊維強化複合材料 |
| CN110114393B (zh) * | 2016-10-26 | 2021-12-07 | 标准石墨烯有限公司 | 碳纤维预浸料或碳纤维增强塑料以及包含其的内部和外部材料 |
| US11001033B2 (en) | 2016-10-26 | 2021-05-11 | Toray Industries, Inc. | Prepreg laminate and fiber-reinforced composite material, and method of producing fiber-reinforced composite material |
| CN110461917B (zh) * | 2017-03-29 | 2022-04-12 | 东丽株式会社 | 预浸料坯以及纤维增强复合材料 |
| KR101951629B1 (ko) * | 2017-05-30 | 2019-02-25 | 주식회사 한국카본 | 내마모성이 우수한 얇은 폭 프리프레그, 이를 이용한 프리프레그 직물 및 이의 제조방법 |
| CN109134900B (zh) * | 2017-06-27 | 2022-06-07 | 深圳光启高等理工研究院 | 一种预浸料及其制备方法 |
| TR201722409A2 (tr) | 2017-12-28 | 2019-07-22 | Kordsa Teknik Tekstil As | Yüzey örtüsü ve yüzey fi̇lmi̇yle entegre prepreg tabakasi ve bunun üreti̇mi̇ i̇çi̇n i̇şlemler |
| US20210371612A1 (en) * | 2018-01-31 | 2021-12-02 | Toray Industries, Inc. | Prepreg sheets and prepreg stacks useful for preparing low void content fiber-reinforced composite materials |
| JP7209470B2 (ja) * | 2018-03-13 | 2023-01-20 | 帝人株式会社 | プリプレグ及び炭素繊維強化複合材料 |
| EP3778211A4 (en) * | 2018-03-30 | 2021-12-15 | Toray Industries, Inc. | MOLDED ARTICLE AND MOLDED ARTICLE MANUFACTURING PROCESS |
| US20210122892A1 (en) * | 2018-06-26 | 2021-04-29 | Toray Industries, Inc. | Prepreg and production method therefor, slit tape prepreg, carbon fiber-reinforced composite material |
| WO2020003662A1 (ja) * | 2018-06-26 | 2020-01-02 | 東レ株式会社 | プリプレグおよびその製造方法、スリットテーププリプレグ、炭素繊維強化複合材料 |
| WO2020040152A1 (ja) * | 2018-08-22 | 2020-02-27 | 東レ株式会社 | 離型シート付き多層構造プリプレグ、プリプレグロール、プリプレグテープおよび複合材料 |
| CN109263089B (zh) * | 2018-09-26 | 2021-01-01 | 牧世复合材料科技(苏州)有限公司 | 一种通过纤维增强树脂拉挤工艺制备夹芯型材的方法及所得型材 |
| JP2020101195A (ja) * | 2018-12-20 | 2020-07-02 | 本田技研工業株式会社 | 圧力容器及びその製造方法 |
| WO2020235488A1 (ja) * | 2019-05-23 | 2020-11-26 | 東レ株式会社 | 繊維強化樹脂基材の製造方法、繊維強化樹脂基材、およびその一体化成形品 |
| WO2021117461A1 (ja) * | 2019-12-11 | 2021-06-17 | 東レ株式会社 | プリプレグ、積層体および一体化成形品 |
| EP4074766A4 (en) | 2019-12-11 | 2023-12-27 | Toray Industries, Inc. | PREPREG, LAMINATE AND INTEGRATED MOLDING |
| RU2751337C1 (ru) * | 2020-11-27 | 2021-07-13 | Акционерное общество "Научно-исследовательский институт конструкционных материалов на основе графита "НИИграфит" | Антифрикционная композиция и способ её получения |
| CN113307643B (zh) * | 2021-06-02 | 2022-10-21 | 中国航空制造技术研究院 | 一种基于单向带SiCf/SiC复合材料制备方法 |
| JPWO2023008357A1 (enExample) * | 2021-07-27 | 2023-02-02 | ||
| CN113882090B (zh) * | 2021-11-02 | 2023-01-06 | 天津工业大学 | 基于单边缝合工艺的三维复合材料预制体制备方法及装置 |
| CN115256796B (zh) * | 2022-09-27 | 2022-12-09 | 四川纤谷塑业有限公司 | 一种玄武岩纤维复合材料的成型工艺 |
| CN115819973B (zh) * | 2022-11-04 | 2023-10-20 | 航天特种材料及工艺技术研究所 | 一种大尺寸连续气凝胶卷材快速复合制备方法 |
| WO2025116834A1 (en) * | 2023-12-01 | 2025-06-05 | Cukurova Universitesi Rektorlugu | High strength fiber used in air and space vehicles containing monofilament yarn interlayers for composite applications |
Family Cites Families (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4590122A (en) | 1980-12-18 | 1986-05-20 | Fiberite Corporation | High conductivity graphite material with electrically conductive filaments wrapped around warp and fill elements |
| CA2056034C (en) * | 1990-11-29 | 2001-04-17 | Toshihiro Hattori | Prepregs, process for producing the same and laminates produced with the same |
| JPH06240022A (ja) * | 1993-02-19 | 1994-08-30 | Dainippon Ink & Chem Inc | プリプレグ |
| JP3150901B2 (ja) * | 1996-03-22 | 2001-03-26 | 東邦レーヨン株式会社 | 木材強化用炭素繊維プリプレグおよび炭素繊維強化木材 |
| JPH10231372A (ja) | 1996-12-18 | 1998-09-02 | Toray Ind Inc | プリプレグおよびその製造方法 |
| US6139942A (en) * | 1997-02-06 | 2000-10-31 | Cytec Technology, Inc. | Resin composition, a fiber reinforced material having a partially impregnated resin and composites made therefrom |
| TW467940B (en) * | 1997-10-14 | 2001-12-11 | Toray Industries | Thermosetting resin composition for carbon-fiber reinforced composite material |
| ATE256550T1 (de) | 1998-05-20 | 2004-01-15 | Cytec Tech Corp | Herstellung von blasenfreien laminaten und deren anwendung |
| GB9907204D0 (en) * | 1999-03-30 | 1999-05-26 | Woolstencroft David H | A composite |
| JP4177041B2 (ja) | 2002-07-18 | 2008-11-05 | 三菱レイヨン株式会社 | 繊維強化複合材料の製造方法 |
| JP2004182923A (ja) * | 2002-12-05 | 2004-07-02 | Mitsubishi Rayon Co Ltd | プリプレグ及びそれを用いた繊維強化複合材料の製造方法 |
| ES2527168T3 (es) * | 2002-07-18 | 2015-01-21 | Mitsubishi Rayon Co., Ltd. | Preimpregnado y procedimientos para la producción de materiales compuestos reforzados con fibras |
| US7943078B2 (en) | 2004-02-17 | 2011-05-17 | Toray Industries, Inc. | RTM molding method and device |
| JP2009511297A (ja) * | 2005-10-11 | 2009-03-19 | シーアールシー フォー アドバンスト コンポジット ストラクチャーズ リミテッド | 乾燥強化繊維の結合方法 |
| JP4969363B2 (ja) * | 2006-08-07 | 2012-07-04 | 東レ株式会社 | プリプレグおよび炭素繊維強化複合材料 |
| GB0619401D0 (en) * | 2006-10-02 | 2006-11-08 | Hexcel Composites Ltd | Composite materials with improved performance |
| ES2365573T3 (es) * | 2007-04-17 | 2011-10-07 | Hexcel Corporation | Materiales compuestos preimpregnados con rendimiento mejorado. |
| JP5562832B2 (ja) * | 2007-04-17 | 2014-07-30 | ヘクセル コーポレイション | 熱可塑性粒子のブレンドを含む複合材料 |
| GB0717507D0 (en) | 2007-09-07 | 2007-10-17 | Cytec Tech Corp | Composite materials and their use |
| DK2168745T3 (da) * | 2008-09-30 | 2012-12-10 | Hexcel Composites Ltd | Semipreg-materiale med en egenskabsforstærkende overfladeharpiksfilm til forbedrede egenskaber |
| WO2010048122A1 (en) * | 2008-10-22 | 2010-04-29 | Cytec Technology Corp. | Improved processing of polymer matrix composites |
| WO2010099029A1 (en) | 2009-02-27 | 2010-09-02 | Cytec Technology Corp. | Epoxy compositions with improved mechanical performance |
-
2012
- 2012-03-30 CN CN201280011819.7A patent/CN103429371B/zh not_active Expired - Fee Related
- 2012-03-30 WO PCT/US2012/031672 patent/WO2012135754A1/en not_active Ceased
- 2012-03-30 CA CA 2830836 patent/CA2830836A1/en not_active Abandoned
- 2012-03-30 RU RU2013148117/05A patent/RU2013148117A/ru not_active Application Discontinuation
- 2012-03-30 JP JP2014502874A patent/JP5971325B2/ja active Active
- 2012-03-30 KR KR1020137026543A patent/KR101951058B1/ko not_active Expired - Fee Related
- 2012-03-30 BR BR112013024886A patent/BR112013024886A2/pt not_active IP Right Cessation
- 2012-03-30 US US14/009,045 patent/US20140087178A1/en not_active Abandoned
- 2012-03-30 EP EP12765220.4A patent/EP2691199B1/en active Active
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