JP2014518867A5 - - Google Patents
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- Publication number
- JP2014518867A5 JP2014518867A5 JP2014510714A JP2014510714A JP2014518867A5 JP 2014518867 A5 JP2014518867 A5 JP 2014518867A5 JP 2014510714 A JP2014510714 A JP 2014510714A JP 2014510714 A JP2014510714 A JP 2014510714A JP 2014518867 A5 JP2014518867 A5 JP 2014518867A5
- Authority
- JP
- Japan
- Prior art keywords
- isophorone
- distillation
- returning
- work
- manufacturing process
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- HJOVHMDZYOCNQW-UHFFFAOYSA-N Isophorone Chemical compound CC1=CC(=O)CC(C)(C)C1 HJOVHMDZYOCNQW-UHFFFAOYSA-N 0.000 claims 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 2
- 238000004821 distillation Methods 0.000 claims 1
- 238000001704 evaporation Methods 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 239000008213 purified water Substances 0.000 claims 1
- 238000010626 work up procedure Methods 0.000 claims 1
Claims (1)
- ５． 前記水性部分の蒸留による後処理の塔底部からの水をフラッシュ蒸発に供し、且つ、生じる精製水をイソホロンの製造工程に返送することを特徴とする、請求項１に記載のイソホロンの製造方法。
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102011075777A DE102011075777A1 (de) | 2011-05-13 | 2011-05-13 | Verfahren zur Herstellung von Isophoron in Gegenwart mindestens eines Entschäumers in der Abwasserkolonne im Aufarbeitungsteil |
| DE102011075777.5 | 2011-05-13 | ||
| PCT/EP2012/057562 WO2012156187A1 (de) | 2011-05-13 | 2012-04-25 | Verfahren zur herstellung von isophoron in gegenwart mindestens eines entschäumers in der abwasserkolonne im aufarbeitungsteil |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2014518867A JP2014518867A (ja) | 2014-08-07 |
| JP2014518867A5 true JP2014518867A5 (ja) | 2015-03-19 |
| JP6120830B2 JP6120830B2 (ja) | 2017-04-26 |
Family
ID=46025686
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014510714A Active JP6120830B2 (ja) | 2011-05-13 | 2012-04-25 | 後処理部における廃水塔内での少なくとも１つの脱泡剤の存在下でのイソホロンの製造方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US8884066B2 (ja) |
| EP (1) | EP2707352B1 (ja) |
| JP (1) | JP6120830B2 (ja) |
| CN (1) | CN102775287B (ja) |
| DE (1) | DE102011075777A1 (ja) |
| ES (1) | ES2557118T3 (ja) |
| WO (1) | WO2012156187A1 (ja) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102010062587A1 (de) | 2010-12-08 | 2012-06-14 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Isophoron |
| DE102011077705A1 (de) | 2011-06-17 | 2012-12-20 | Evonik Degussa Gmbh | Mikrobielles Verfahren zur Herstellung niedermolekularer, organischer Verbindungen umfassend die Produktabsorption durch Isophoron |
| DE102013215874A1 (de) * | 2013-08-12 | 2015-02-12 | Evonik Industries Ag | Hydrolyse der bei der Produktion von Isophoron anfallenden Rückstände zurRückgewinnung von Isophoron und Aceton |
| ES2644946T3 (es) * | 2015-10-19 | 2017-12-01 | Evonik Degussa Gmbh | Tratamiento del agua residual procedente de la preparación de isoforona con neutralización, filtración y procedimiento químico de oxidación realizado posteriormente y subsiguiente reducción |
| EP3178791A1 (de) | 2015-12-09 | 2017-06-14 | Evonik Degussa GmbH | Aufarbeitung des abwassers aus der isophoron produktion durch drucknassoxidation |
| EP3330247B1 (de) | 2016-12-02 | 2019-05-08 | Evonik Degussa GmbH | Katalytische oxidation von 3,5,5-trimethylcyclohexa-3-en-1-on (beta-isophoron) mit wasserstoffperoxid zu 2,6,6-trimethyl-2-cyclohexene-1,4-dion (keto-isophoron) |
| CN111377806B (zh) * | 2018-12-27 | 2022-07-12 | 万华化学集团股份有限公司 | 一种丙酮液相缩合法制异佛尔酮的后处理工艺 |
Family Cites Families (37)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2344226A (en) | 1941-05-31 | 1944-03-14 | Shell Dev | Production of isophorone |
| US2351352A (en) | 1941-07-29 | 1944-06-13 | Shell Dev | Separation of by-products from isophorone |
| US2399976A (en) | 1943-01-28 | 1946-05-07 | Shell Dev | Production of isophorone and related products |
| US2419051A (en) | 1944-12-05 | 1947-04-15 | Shell Dev | Hydrolysis of acetone autocondensation products |
| GB733650A (en) | 1951-09-08 | 1955-07-13 | Derives De L Acetylene S I D A | Isophorone and its homologues |
| DE1058047B (de) | 1953-12-24 | 1959-05-27 | Derives De L Acetylene Soc Ind | Verfahren zur Herstellung von Mesityloxyd oder seiner Homologen |
| DE1095818B (de) | 1958-09-15 | 1960-12-29 | Bergwerksgesellschaft Hibernia | Verfahren zur Herstellung von Isophoron |
| NL272258A (ja) | 1960-12-23 | |||
| DE1205525B (de) | 1960-12-23 | 1965-11-25 | Bergwerksgesellschaft Hibernia | Verfahren zur Aufarbeitung von Nebenprodukten der Isophoronherstellung |
| NL272976A (ja) | 1960-12-31 | |||
| GB1498017A (en) | 1974-05-15 | 1978-01-18 | Bp Chem Int Ltd | Isophorone production using a potassium hydroxide catalys |
| GB1528129A (en) * | 1975-10-20 | 1978-10-11 | Bp Chem Int Ltd | Process for the production of isophorone |
| US4165339A (en) | 1976-02-12 | 1979-08-21 | Union Carbide Corporation | Catalytic aldol condensations |
| US4086188A (en) | 1976-02-12 | 1978-04-25 | Union Carbide Corporation | Catalyst for aldol condensations |
| US4476324A (en) | 1982-06-02 | 1984-10-09 | Union Carbide Corporation | Catalyzed aldol condensations |
| US4970191A (en) | 1989-04-18 | 1990-11-13 | Aristech Chemical Corporation | Basic mixed oxide |
| US5352839A (en) | 1993-09-09 | 1994-10-04 | Aristech Chemical Corporation | Isophorone process |
| JPH08245485A (ja) | 1995-03-13 | 1996-09-24 | Daicel Chem Ind Ltd | イソホロンの製造方法 |
| JPH08245486A (ja) | 1995-03-16 | 1996-09-24 | Daicel Chem Ind Ltd | イソホロンの製造方法 |
| JPH0959204A (ja) | 1995-08-24 | 1997-03-04 | Mitsui Toatsu Chem Inc | アセトン脱水縮合物の製造方法 |
| JPH09151153A (ja) | 1995-11-30 | 1997-06-10 | Mitsui Toatsu Chem Inc | アセトン脱水縮合物の製造方法 |
| JPH09151152A (ja) | 1995-11-30 | 1997-06-10 | Mitsui Toatsu Chem Inc | アセトン脱水縮合物の製造方法 |
| JPH09157207A (ja) | 1995-12-14 | 1997-06-17 | Mitsui Toatsu Chem Inc | イソホロンの製造方法 |
| JPH09157208A (ja) | 1995-12-14 | 1997-06-17 | Mitsui Toatsu Chem Inc | イソホロンの製造方法 |
| JPH09169687A (ja) | 1995-12-21 | 1997-06-30 | Mitsui Toatsu Chem Inc | イソホロンの製造方法 |
| JPH09169688A (ja) | 1995-12-21 | 1997-06-30 | Mitsui Toatsu Chem Inc | イソホロンの製造方法 |
| FR2745566B1 (fr) | 1996-02-29 | 1998-04-24 | Atochem Elf Sa | Procede d'obtention d'isophorone |
| FR2780966B1 (fr) * | 1998-07-10 | 2000-09-08 | Rhodia Chimie Sa | Procede de recuperation de composes dans les produits lourds issus de leur fabrication |
| JP4281856B2 (ja) * | 1998-08-03 | 2009-06-17 | 旭化成ケミカルズ株式会社 | メチラールの製造方法 |
| DE10002793A1 (de) * | 2000-01-24 | 2001-07-26 | Basf Ag | Verwendung eines Extraktionsmittels bei der Herstellung von wasserfreier Ameisensäure |
| DE102007011483A1 (de) | 2007-03-07 | 2008-09-18 | Evonik Degussa Gmbh | Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin |
| DE102007052463A1 (de) | 2007-11-02 | 2009-05-07 | Evonik Degussa Gmbh | Fermentative Gewinnung von Aceton aus erneuerbaren Rohstoffen mittels neuen Stoffwechselweges |
| DE102009002583A1 (de) | 2009-04-23 | 2010-10-28 | Evonik Degussa Gmbh | Zellen und Verfahren zur Herstellung von Aceton |
| CN101633610B (zh) | 2009-08-13 | 2012-10-17 | 浙江大学 | 一种α-异佛尔酮的制备方法 |
| DE102010062594B4 (de) | 2010-12-08 | 2022-02-17 | Evonik Operations Gmbh | Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin |
| DE102010062587A1 (de) * | 2010-12-08 | 2012-06-14 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Isophoron |
| DE102010062603A1 (de) | 2010-12-08 | 2012-06-14 | Evonik Degussa Gmbh | Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin |
-
2011
- 2011-05-13 DE DE102011075777A patent/DE102011075777A1/de not_active Withdrawn
- 2011-05-27 CN CN201110140108.7A patent/CN102775287B/zh active Active
-
2012
- 2012-04-25 JP JP2014510714A patent/JP6120830B2/ja active Active
- 2012-04-25 US US14/116,233 patent/US8884066B2/en active Active
- 2012-04-25 EP EP12718179.0A patent/EP2707352B1/de active Active
- 2012-04-25 WO PCT/EP2012/057562 patent/WO2012156187A1/de active Application Filing
- 2012-04-25 ES ES12718179.0T patent/ES2557118T3/es active Active
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