JP2014503638A5 - - Google Patents
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- JP2014503638A5 JP2014503638A5 JP2013544520A JP2013544520A JP2014503638A5 JP 2014503638 A5 JP2014503638 A5 JP 2014503638A5 JP 2013544520 A JP2013544520 A JP 2013544520A JP 2013544520 A JP2013544520 A JP 2013544520A JP 2014503638 A5 JP2014503638 A5 JP 2014503638A5
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- oil
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- liquid hydrocarbon
- raw material
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- 239000003054 catalyst Substances 0.000 claims 15
- 239000002028 Biomass Substances 0.000 claims 14
- 235000019198 oils Nutrition 0.000 claims 12
- 239000004215 Carbon black (E152) Substances 0.000 claims 10
- 150000002430 hydrocarbons Chemical class 0.000 claims 10
- 239000007788 liquid Substances 0.000 claims 10
- 238000010335 hydrothermal treatment Methods 0.000 claims 9
- 239000002994 raw material Substances 0.000 claims 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 9
- 239000007789 gas Substances 0.000 claims 8
- 239000002245 particle Substances 0.000 claims 8
- MCMNRKCIXSYSNV-UHFFFAOYSA-N ZrO2 Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 4
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims 4
- 239000000203 mixture Substances 0.000 claims 4
- 239000007787 solid Substances 0.000 claims 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims 4
- 235000019737 Animal fat Nutrition 0.000 claims 3
- 235000019197 fats Nutrition 0.000 claims 3
- 229910052500 inorganic mineral Inorganic materials 0.000 claims 3
- 239000011707 mineral Substances 0.000 claims 3
- 238000000197 pyrolysis Methods 0.000 claims 3
- 235000014102 seafood Nutrition 0.000 claims 3
- 235000015112 vegetable and seed oil Nutrition 0.000 claims 3
- 235000019871 vegetable fat Nutrition 0.000 claims 3
- OFJATJUUUCAKMK-UHFFFAOYSA-N Cerium(IV) oxide Chemical compound [O-2]=[Ce+4]=[O-2] OFJATJUUUCAKMK-UHFFFAOYSA-N 0.000 claims 2
- NUJOXMJBOLGQSY-UHFFFAOYSA-N Manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 claims 2
- GNTDGMZSJNCJKK-UHFFFAOYSA-N Vanadium(V) oxide Chemical compound O=[V](=O)O[V](=O)=O GNTDGMZSJNCJKK-UHFFFAOYSA-N 0.000 claims 2
- 229910000420 cerium oxide Inorganic materials 0.000 claims 2
- PWZFXELTLAQOKC-UHFFFAOYSA-A dialuminum;hexamagnesium;carbonate;hexadecahydroxide;tetrahydrate Chemical compound O.O.O.O.[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Al+3].[Al+3].[O-]C([O-])=O PWZFXELTLAQOKC-UHFFFAOYSA-A 0.000 claims 2
- 229910052739 hydrogen Inorganic materials 0.000 claims 2
- 239000001257 hydrogen Substances 0.000 claims 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 2
- 229910001701 hydrotalcite Inorganic materials 0.000 claims 2
- 229960001545 hydrotalcite Drugs 0.000 claims 2
- 239000000395 magnesium oxide Substances 0.000 claims 2
- 229910000468 manganese oxide Inorganic materials 0.000 claims 2
- AMWRITDGCCNYAT-UHFFFAOYSA-L manganese(II,III) oxide Inorganic materials [Mn].O[Mn]=O.O[Mn]=O AMWRITDGCCNYAT-UHFFFAOYSA-L 0.000 claims 2
- 229910052751 metal Inorganic materials 0.000 claims 2
- 239000002184 metal Substances 0.000 claims 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N AI2O3 Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims 1
- 241000195493 Cryptophyta Species 0.000 claims 1
- 238000009835 boiling Methods 0.000 claims 1
- 230000003197 catalytic Effects 0.000 claims 1
- 229910052803 cobalt Inorganic materials 0.000 claims 1
- 229910052741 iridium Inorganic materials 0.000 claims 1
- 229910044991 metal oxide Inorganic materials 0.000 claims 1
- 150000004706 metal oxides Chemical class 0.000 claims 1
- 238000000034 method Methods 0.000 claims 1
- 229910052750 molybdenum Inorganic materials 0.000 claims 1
- 229910052759 nickel Inorganic materials 0.000 claims 1
- 229910052763 palladium Inorganic materials 0.000 claims 1
- 229910052697 platinum Inorganic materials 0.000 claims 1
- 229910052700 potassium Inorganic materials 0.000 claims 1
- 229910052703 rhodium Inorganic materials 0.000 claims 1
- 229910052707 ruthenium Inorganic materials 0.000 claims 1
- 239000000377 silicon dioxide Substances 0.000 claims 1
- 229910052721 tungsten Inorganic materials 0.000 claims 1
Claims (19)
- バイオマス原料を、多相生成物を生成するために有効な水熱処理条件下で触媒粒子および還元ガスの存在下で水と接触させる工程であって、前記触媒粒子が触媒担体上に配置された少なくとも1つの金属成分を含む工程と、
前記多相生成物を、少なくとも気相部分、液体炭化水素生成物、水性部分および固体部分を生成するために分離する工程と、
有効な水素処理の条件下で水素処理触媒の存在下で前記液体炭化水素生成物の少なくとも一部を水素処理する工程と
を含み、
前記液体炭化水素生成物の少なくとも一部が、水素処理の前に鉱物原料およびバイオ成分原料の少なくとも1つと組み合わされ、前記バイオ成分原料が、植物性の脂肪または油、動物性の脂肪または油、魚介類の脂肪または油、熱分解油および藻類の油の1つ以上を含む、
バイオマスの水熱処理方法。 - 前記有効な水熱処理条件が、約150℃〜約500℃の温度および約4.5barg(約450kPag)〜約300barg(約30MPag)の圧力を含む、請求項1に記載の方法。
- 前記有効な水熱処理条件が、少なくとも約2バール(200kPa)の還元ガスの分圧を含み、前記還元ガスが水素を含む、請求項1に記載の方法。
- 固体部分を生成するための前記多相生成物を分離する工程が、触媒部分およびバイオマスベースの固体部分を生成するために前記多相生成物を分離することを含む、請求項1に記載の方法。
- 前記バイオマス原料を、有効な水熱処理条件下で水と接触させる工程が、前記水の相変化をもたらさない、請求項1に記載の方法。
- 前記バイオマス原料および前記水が、バイオマスと水との混合物として反応器に導入される、請求項1に記載の方法。
- 前記水および前記バイオマスが、約3:1〜約5:1の水:バイオマスの重量比で存在する、請求項1に記載の方法。
- 前記触媒粒子の重量が、前記バイオマスの重量を基準として、約5重量%〜約20重量%である、請求項1に記載の方法。
- 前記液体炭化水素生成物を、その少なくとも90重量%が約193℃〜約360℃の沸点範囲を有する留分を生成するために分離する工程をさらに含む、請求項1に記載の方法。
- 前記触媒担体が、チタニア、ジルコニア、シリカ、バナジア、酸化マンガン、酸化セリウム、活性炭、酸化マグネシウム、ハイドロタルサイトまたはそれらの組み合わせを含む、請求項1に記載の方法。
- 前記触媒担体が、アルミナを実質的に含まない、請求項10に記載の方法。
- 前記少なくとも1つの金属成分が、Pt、Pd、Rh、Ru、Irまたはそれらの組み合わせを含む、請求項10に記載の方法。
- 前記触媒粒子が、チタニア、ジルコニア、バナジア、酸化マンガン、酸化セリウムまたはそれらの混合物を含む担体上にK、Co、Ni、MoおよびWの少なくとも1つを含む、請求項1に記載の方法。
- 前記バイオマス原料が、藻類ベースの原料を含む、請求項1に記載の方法。
- バイオマス原料を、多相生成物を生成するために有効な水熱処理条件下で触媒粒子の存在下で水と接触させる工程と、
液体炭化水素生成物を前記多相生成物から分離する工程と、
前記液体炭化水素生成物の少なくとも一部を、有効な水素処理条件下で水素処理触媒の存在下で水素処理する工程と
を含み、
前記液体炭化水素生成物の少なくとも一部が、水素処理の前に鉱物原料およびバイオ成分原料の少なくとも1つと組み合わされ、前記バイオ成分原料が、植物性の脂肪または油、動物性の脂肪または油、魚介類の脂肪または油、熱分解油および藻類の油の1つ以上を含む、
バイオマスの水熱処理方法。 - 前記水素処理条件が、約400psig(約2.8MPag)〜約1500psig(約10.3MPag)の全圧、約0.5時間−1〜約5.0時間−1のLHSV、および約500scf/bbl(約85Nm3/m3)〜約2000scf/bbl(約340Nm3/m3)の処理ガス速度を含む有効な接触脱ロウ条件を含む、請求項15に記載の方法。
- 前記有効な水素処理条件が、約315℃〜約425℃の温度、約300psig(約2.1MPag)〜約3000psig(約20.6MPag)の全圧、約0.2時間−1〜約10時間−1のLHSV、および約500scf/bbl(約85Nm3/m3)〜約10000scf/bbl(約1700Nm3/m3)の水素処理ガス速度を含む有効な水素化処理条件を含む、請求項15に記載の方法。
- バイオマス原料を、多相生成物を生成するために有効な水熱処理条件下で触媒粒子および還元ガスの存在下で水と接触させる工程であって、前記触媒粒子が活性炭または酸化金属を含む工程と、
前記多相生成物を、少なくとも気相部分、液体炭化水素生成物、水性部分および固体部分を生成するために分離する工程と、
有効な水素処理の条件下で水素処理触媒の存在下で前記液体炭化水素生成物の少なくとも一部を水素処理する工程と
を含み、
前記液体炭化水素生成物の少なくとも一部が、水素処理の前に鉱物原料およびバイオ成分原料の少なくとも1つと組み合わされ、前記バイオ成分原料が、植物性の脂肪または油、動物性の脂肪または油、魚介類の脂肪または油、熱分解油および藻類の油の1つ以上を含む、
バイオマスの水熱処理方法。 - 前記触媒粒子が、酸化マグネシウムまたはハイドロタルサイトを含む、請求項18に記載の方法。
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US42240010P | 2010-12-13 | 2010-12-13 | |
US61/422,400 | 2010-12-13 | ||
US13/285,519 US8487148B2 (en) | 2010-12-13 | 2011-10-31 | Hydrothermal treatment of biomass with heterogeneous catalyst |
US13/285,519 | 2011-10-31 | ||
PCT/US2011/062505 WO2012082367A1 (en) | 2010-12-13 | 2011-11-30 | Hydrothermal treatment of biomass with heterogeneous catalyst |
Publications (3)
Publication Number | Publication Date |
---|---|
JP2014503638A JP2014503638A (ja) | 2014-02-13 |
JP2014503638A5 true JP2014503638A5 (ja) | 2014-07-24 |
JP5666015B2 JP5666015B2 (ja) | 2015-02-04 |
Family
ID=45934648
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2013544520A Expired - Fee Related JP5666015B2 (ja) | 2010-12-13 | 2011-11-30 | 不均一触媒でのバイオマスの水熱処理 |
Country Status (6)
Country | Link |
---|---|
US (1) | US8487148B2 (ja) |
EP (1) | EP2652093A4 (ja) |
JP (1) | JP5666015B2 (ja) |
CN (1) | CN103261378B (ja) |
SG (1) | SG190821A1 (ja) |
WO (1) | WO2012082367A1 (ja) |
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US9102877B2 (en) | 2008-11-12 | 2015-08-11 | Sartec Corporation | Systems and methods for producing fuels from biomass |
US8471079B2 (en) * | 2008-12-16 | 2013-06-25 | Uop Llc | Production of fuel from co-processing multiple renewable feedstocks |
US8632675B2 (en) | 2008-12-24 | 2014-01-21 | Exxonmobil Research And Engineering Company | Co-processing of diesel biofeed and heavy oil |
FR2943071B1 (fr) * | 2009-03-10 | 2011-05-13 | Inst Francais Du Petrole | Procede d'hydrodesoxygenation de charges issues de sources renouvelables avec conversion limitee en decarboxylation mettant en oeuvre un catalyseur a base de nickel et de molybdene |
EP2406370A4 (en) | 2009-03-10 | 2013-08-14 | Srs Energy | FRACTIONATION OF ALGAE BIOMASS |
US8492600B2 (en) * | 2009-04-07 | 2013-07-23 | Gas Technology Institute | Hydropyrolysis of biomass for producing high quality fuels |
EP2449060A2 (en) | 2009-05-20 | 2012-05-09 | Yeda Research and Development Co. Ltd. | Catalytic gasification of organic matter in supercritical water |
CN101591573A (zh) | 2009-07-02 | 2009-12-02 | 复旦大学 | 一种将藻类水热液化制备液体燃料的方法 |
US8404908B2 (en) * | 2009-10-13 | 2013-03-26 | Uop Llc | Process for lignin conversion to chemicals or fuels with H2 generated from lignin depolymerization products |
EP2348091B1 (fr) * | 2010-01-12 | 2012-12-05 | IFP Energies nouvelles | Procédé d'hydroliquéfaction directe de biomasse comprenant deux etapes d'hydroconversion en lit bouillonnant |
CN101805629B (zh) * | 2010-03-22 | 2014-03-26 | 华东理工大学 | 生物质水热液化生产燃料油的方法 |
WO2011126382A1 (en) | 2010-04-07 | 2011-10-13 | Aquaflow Bionomic Corporation Limited | Hydrothermal transformation of microalgae through metal-base catalysis |
US20110287503A1 (en) | 2010-05-20 | 2011-11-24 | Uop Llc | Methods for producing hydrocarbon products from algal biomass |
US20120090223A1 (en) | 2010-10-13 | 2012-04-19 | Uop Llc | Methods for producing diesel range materials having improved cold flow properties |
-
2011
- 2011-10-31 US US13/285,519 patent/US8487148B2/en active Active
- 2011-11-30 SG SG2013037734A patent/SG190821A1/en unknown
- 2011-11-30 EP EP11848573.9A patent/EP2652093A4/en not_active Withdrawn
- 2011-11-30 JP JP2013544520A patent/JP5666015B2/ja not_active Expired - Fee Related
- 2011-11-30 CN CN201180059235.2A patent/CN103261378B/zh not_active Expired - Fee Related
- 2011-11-30 WO PCT/US2011/062505 patent/WO2012082367A1/en active Application Filing
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