JP2013545470A - 穀類タンパク質の液化方法 - Google Patents
穀類タンパク質の液化方法 Download PDFInfo
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- JP2013545470A JP2013545470A JP2013541254A JP2013541254A JP2013545470A JP 2013545470 A JP2013545470 A JP 2013545470A JP 2013541254 A JP2013541254 A JP 2013541254A JP 2013541254 A JP2013541254 A JP 2013541254A JP 2013545470 A JP2013545470 A JP 2013545470A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
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- A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
- A23J1/12—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from cereals, wheat, bran, or molasses
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
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- A—HUMAN NECESSITIES
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- A—HUMAN NECESSITIES
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
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- A—HUMAN NECESSITIES
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- A—HUMAN NECESSITIES
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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Abstract
Description
a)1種以上の穀類タンパク質を含む組成物を提供する工程であって、この組成物が、組成物の5〜40重量%(%w/w)の乾燥物質を含む工程、次に、
b)1種以上の加水分解酵素及び/又は加工助剤を組成物に加える工程、次に、
c)所望により組成物を事前調整する工程、次に、
d)組成物を懸濁する工程、を含む。
i)前出の液化工程に従って、1種以上の穀類タンパク質を含む組成物を液化させる工程、次に、
ii)所望により組成物を前処理する工程、次に、
iii)50〜85℃の温度にて、少なくとも5分にわたって組成物をインキュベートする工程、を含む。
a)1種以上の穀類タンパク質を含む組成物を提供する工程であって、前記組成物が、組成物の5〜40重量%の乾燥物質を含む工程、次に、
b)1種以上の加水分解酵素及び/又は加工助剤を組成物に加える工程、次に、
c)所望により組成物を事前調整する工程、次に、
d)組成物を懸濁する工程、を含む。
−組成部を加熱する処理、
−組成物を混合する処理、
−組成物のpHを調整する処理、
−加工助剤を組成物に加える処理、のうちいずれか1つを含み、又は2つ以上を組み合わせて含む。
a)小麦バイタルグルテンを含む組成物を提供する工程であって、前記組成物が、組成物の5〜40重量%の乾燥物質を含む工程、次に、
b)1種以上の加水分解酵素を加える工程、次に
c)組成物を前処理する工程、次に
d)組成物を懸濁する工程、を含む、方法。
i)上記に開示された液化工程に従って、1種以上の穀類タンパク質を含む組成物を液化する工程、次に
ii)所望により組成物を前処理する工程、次に、
iii)50〜85℃の温度にて、少なくとも5分にわたって組成物をインキュベートする工程、を含む。
2.1種以上の加水分解酵素及び/又は加工助剤を組成物に加える工程、次に、
3.組成物を前処理する工程、次に、
4.組成物を懸濁する工程、次に、
5.工程4で得た組成物を前処理する工程、次に、
6.50〜85℃の温度にて、少なくとも5分にわたって組成物をインキュベートする工程、を含む。
小麦バイタルグルテンを次の通りに液化した。一般的な小麦植物から生成した小麦バイタルグルテン(VWG)を用意した(乾燥物質30%、37℃及びpH5.8)。次の酵素をインラインで添加した。
2.Ban(登録商標)480LS(Novozymes):0.06重量%(酵素重量/VWG乾燥重量)
3.Rohalase(登録商標)Sep(AB enzymes):0.03重量%(酵素重量/VWG乾燥重量)
小麦バイタルグルテン及び酵素組成物を、4段階式モノポンプにより流速400l/hでユニットに供給し、ユニット中で、組成物を最初に50℃に加熱した。加熱溶媒には温度60℃の水を使用した。加熱は、静的加熱ミキサー(SMR DN 150 plus、製品番号CT−1810)により実施した。次に、組成物を、静的ミキサー(混合要素を3つ備えるSMX DN 50、混合要素を7つ備えるSMX DN 65、混合要素を10備えるSMX plus DN 80を取り付けた、Sulzer SMX TM plus DN 80型)により混合した。次いで、組成物はインライン式高せん断ミキサー(2 DT混合ブレードと、11kワットのモーターを装備させた、Typhoon HSI20)を用い、チップ速度11m/sで、1500rpmで懸濁した。
タンパク質の消化性:99.2%
沈殿:170/200(pH6.2)
加水分解タンパク質の解析方法
加水分解度:OPA法(Shmidt,D.G.,Tobben,A.J.P.M.,VMT.19,13〜15,1993)
タンパク質消化性:Dierick及びHendrickx(1990)に記載の通りのin vitro消化性試験に従った。
一般的な小麦植物から生成した小麦バイタルグルテン(VWG)を用意した(乾燥物質30%、38℃及びpH5.7)。実施例1に記載のものと同様の酵素及び酵素投与量で添加した。実施例1に記載のものと同様の液化条件を適用し、グルテン及び酵素組成物を液化した。
一般的な小麦植物から生成した小麦バイタルグルテンを用意した(乾燥物質30%、37℃及びpH5.5)。亜硫酸水素ナトリウム(Sigma−Aldrich,カタログ番号24,397−3)を、インラインで0.06重量%(亜硫酸水素ナトリウム/VWG乾燥重量)で添加した。取り扱い易さのため、亜硫酸水素ナトリウムを希釈して10%水溶液とした。
2.Ban(登録商標)480LS(Novozymes):0.07重量
%(酵素重量/VWG乾燥重量)
3.Rohalase(登録商標)Sep(AB enzymes):0.035重量%(酵素重量/VWG乾燥重量)
撹拌開始から10分後、研究室スケールでインキュベーションを実施するために、70℃にて、撹拌容器にタンクから2Lの試料を移し入れた。
インキュベーション開始から3時間後の加水分解度:6.6%
Claims (13)
- 1種以上の穀類タンパク質を液化する方法であって、
a)1種以上の穀類タンパク質を含む組成物を提供する工程であって、前記組成物が、前記組成物の5〜40重量%の乾燥物質を含む工程、次に、
b)1種以上の加水分解酵素及び/又は加工助剤を前記組成物に加える工程、次に、
c)所望により前記組成物を事前調整する工程、次に、
d)前記組成物を懸濁する工程、を含む、方法。 - 前記懸濁化が、1m/s〜100m/s、好ましくは5m/s〜20m/sのチップ速度で稼働する少なくとも1つのローターを備えた装置による動的混合を含むことを特徴とする、請求項1に記載の方法。
- 前記穀類タンパク質が小麦バイタルグルテンであることを特徴とする、請求項1又は2に記載の方法。
- 前記事前調整が、混合、加熱、加工助剤の添加、pH調製、及びこれらの組み合わせを含むことを特徴とする、請求項1〜3のいずれか一項に記載の方法。
- 前記組成物を40〜55℃に加熱することを特徴とする、請求項4に記載の方法。
- 前記加工助剤が、システイン、グルタチオン、亜硫酸水素、亜硫酸、アスコルビン酸、これらの塩、並びにこれらの組み合わせからなる群から選択されることを特徴とする、請求項4又は5に記載の方法。
- 連続するプラグ流による方法であることを特徴とする、請求項1〜6のいずれか一項に記載の方法。
- 加水分解穀類タンパク質の製造方法であって、
i)請求項1〜7のいずれか一項に記載の方法、
ii)工程i)で得られた前記組成物を所望により前処理する工程、
iii)50〜85℃の温度にて、少なくとも5分にわたって前記組成物をインキュベートする工程、を含む、方法。 - 前記工程ii)の前処理が、15分以内で温度を50〜85℃に加熱することを含むことを特徴とする、請求項8に記載の方法。
- 直接蒸気を導入することで、前記工程ii)の前処理の前記加熱を実施することを特徴とする、請求項9に記載の方法。
- セミバッチ法、複数反応器による連続法又は連続するプラグ流による方法であることを特徴とする、請求項8〜10のいずれか一項に記載の方法。
- 請求項8〜11のいずれか一項に記載の方法により得ることのできる加水分解穀類タンパク質。
- 請求項12に記載の加水分解穀類タンパク質の食品及び飼料用途での使用。
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