JP2013058674A5

JP2013058674A5 -

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Publication number: JP2013058674A5
Authority: JP; Japan
Prior art keywords: compound; nmr; toluene; iodoazulene; pph
Prior art date: 2011-09-09
Legal status : Granted

Application number

JP2011197043A

Other languages

English (en)

Japanese (ja)

Other versions

JP2013058674A (ja

JP5995230B2 (ja

Filing date

2011-09-09

Publication date

2014-10-16

2011-09-09 Application filed filed Critical

2011-09-09 Priority to JP2011197043A priority Critical patent/JP5995230B2/ja

2011-09-09 Priority claimed from JP2011197043A external-priority patent/JP5995230B2/ja

2013-03-28 Publication of JP2013058674A publication Critical patent/JP2013058674A/ja

2014-10-16 Publication of JP2013058674A5 publication Critical patent/JP2013058674A5/ja

2016-09-21 Application granted granted Critical

2016-09-21 Publication of JP5995230B2 publication Critical patent/JP5995230B2/ja

Status Active legal-status Critical Current

2031-09-09 Anticipated expiration legal-status Critical

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YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
QFLWZFQWSBQYPS-AWRAUJHKSA-N (3S)-3-[[(2S)-2-[[(2S)-2-[5-[(3aS,6aR)-2-oxo-1,3,3a,4,6,6a-hexahydrothieno[3,4-d]imidazol-4-yl]pentanoylamino]-3-methylbutanoyl]amino]-3-(4-hydroxyphenyl)propanoyl]amino]-4-[1-bis(4-chlorophenoxy)phosphorylbutylamino]-4-oxobutanoic acid Chemical compound CCCC(NC(=O)[C@H](CC(O)=O)NC(=O)[C@H](Cc1ccc(O)cc1)NC(=O)[C@@H](NC(=O)CCCCC1SC[C@@H]2NC(=O)N[C@H]12)C(C)C)P(=O)(Oc1ccc(Cl)cc1)Oc1ccc(Cl)cc1 QFLWZFQWSBQYPS-AWRAUJHKSA-N 0.000 description 2
238000005160 1H NMR spectroscopy Methods 0.000 description 2
GQHQNTFHIMYMRF-UHFFFAOYSA-N 6-iodoazulene Chemical compound C1=CC(I)=CC=C2C=CC=C21 GQHQNTFHIMYMRF-UHFFFAOYSA-N 0.000 description 2
HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
229940125773 compound 10 Drugs 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
239000013078 crystal Substances 0.000 description 1
238000000605 extraction Methods 0.000 description 1
ZLVXBBHTMQJRSX-VMGNSXQWSA-N jdtic Chemical compound C1([C@]2(C)CCN(C[C@@H]2C)C[C@H](C(C)C)NC(=O)[C@@H]2NCC3=CC(O)=CC=C3C2)=CC=CC(O)=C1 ZLVXBBHTMQJRSX-VMGNSXQWSA-N 0.000 description 1
238000005259 measurement Methods 0.000 description 1
239000000203 mixture Substances 0.000 description 1
239000012299 nitrogen atmosphere Substances 0.000 description 1
239000012044 organic layer Substances 0.000 description 1
238000001953 recrystallisation Methods 0.000 description 1
238000010992 reflux Methods 0.000 description 1
229910000029 sodium carbonate Inorganic materials 0.000 description 1
229910052938 sodium sulfate Inorganic materials 0.000 description 1
235000011152 sodium sulphate Nutrition 0.000 description 1
239000002904 solvent Substances 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1

JP2011197043A 2011-09-09 2011-09-09 有機半導体材料及びそれを用いた有機半導体デバイス Active JP5995230B2 (ja)