JP2012031128A - 毛髪化粧料 - Google Patents
毛髪化粧料 Download PDFInfo
- Publication number
- JP2012031128A JP2012031128A JP2010174307A JP2010174307A JP2012031128A JP 2012031128 A JP2012031128 A JP 2012031128A JP 2010174307 A JP2010174307 A JP 2010174307A JP 2010174307 A JP2010174307 A JP 2010174307A JP 2012031128 A JP2012031128 A JP 2012031128A
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- JP
- Japan
- Prior art keywords
- acid
- mass
- hair
- salt
- carbon atoms
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 210000004209 hair Anatomy 0.000 title claims abstract description 102
- 239000002537 cosmetic Substances 0.000 title claims abstract description 24
- 150000003839 salts Chemical class 0.000 claims abstract description 42
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 26
- 239000000194 fatty acid Substances 0.000 claims abstract description 26
- 229930195729 fatty acid Natural products 0.000 claims abstract description 26
- 150000004665 fatty acids Chemical class 0.000 claims abstract description 20
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 125000003118 aryl group Chemical group 0.000 claims abstract description 7
- 125000001453 quaternary ammonium group Chemical group 0.000 claims abstract description 5
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims abstract description 5
- 150000003512 tertiary amines Chemical class 0.000 claims abstract description 5
- 125000004432 carbon atom Chemical group C* 0.000 claims description 42
- -1 halide ion Chemical class 0.000 claims description 41
- 125000000217 alkyl group Chemical group 0.000 claims description 32
- 239000000203 mixture Substances 0.000 claims description 25
- 239000004166 Lanolin Substances 0.000 claims description 10
- 125000003342 alkenyl group Chemical group 0.000 claims description 10
- 229940039717 lanolin Drugs 0.000 claims description 10
- 235000019388 lanolin Nutrition 0.000 claims description 10
- 239000003676 hair preparation Substances 0.000 claims description 9
- 125000002947 alkylene group Chemical group 0.000 claims description 8
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 6
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 6
- WSRCOZWDQPJAQT-UHFFFAOYSA-N 18-methylicosanoic acid Chemical compound CCC(C)CCCCCCCCCCCCCCCCC(O)=O WSRCOZWDQPJAQT-UHFFFAOYSA-N 0.000 claims description 5
- 150000008051 alkyl sulfates Chemical class 0.000 claims description 5
- XDOFQFKRPWOURC-UHFFFAOYSA-N 16-methylheptadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCCCC(O)=O XDOFQFKRPWOURC-UHFFFAOYSA-N 0.000 claims description 4
- PCGKIWPTIJPQHI-UHFFFAOYSA-N 16-methyloctadecanoic acid Chemical compound CCC(C)CCCCCCCCCCCCCCC(O)=O PCGKIWPTIJPQHI-UHFFFAOYSA-N 0.000 claims description 4
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 4
- CYRMSUTZVYGINF-UHFFFAOYSA-N trichlorofluoromethane Chemical compound FC(Cl)(Cl)Cl CYRMSUTZVYGINF-UHFFFAOYSA-N 0.000 claims description 4
- XBONULTVANIITL-UHFFFAOYSA-N 3-hexadecoxy-n,n-dimethylpropan-1-amine Chemical compound CCCCCCCCCCCCCCCCOCCCN(C)C XBONULTVANIITL-UHFFFAOYSA-N 0.000 claims description 3
- RLGQACBPNDBWTB-UHFFFAOYSA-N cetyltrimethylammonium ion Chemical compound CCCCCCCCCCCCCCCC[N+](C)(C)C RLGQACBPNDBWTB-UHFFFAOYSA-N 0.000 claims description 3
- BHQZSXXOSYWJSZ-UHFFFAOYSA-N n,n-dimethyl-3-octadecoxypropan-1-amine Chemical compound CCCCCCCCCCCCCCCCCCOCCCN(C)C BHQZSXXOSYWJSZ-UHFFFAOYSA-N 0.000 claims description 3
- KVBGVZZKJNLNJU-UHFFFAOYSA-N naphthalene-2-sulfonic acid Chemical compound C1=CC=CC2=CC(S(=O)(=O)O)=CC=C21 KVBGVZZKJNLNJU-UHFFFAOYSA-N 0.000 claims description 3
- FTNJQNQLEGKTGD-UHFFFAOYSA-N 1,3-benzodioxole Chemical compound C1=CC=C2OCOC2=C1 FTNJQNQLEGKTGD-UHFFFAOYSA-N 0.000 claims description 2
- ZONJATNKKGGVSU-UHFFFAOYSA-N 14-methylpentadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCC(O)=O ZONJATNKKGGVSU-UHFFFAOYSA-N 0.000 claims description 2
- VLJCQMPCVZKWIE-UHFFFAOYSA-N 17-methyl-nonadecanoic acid Chemical compound CCC(C)CCCCCCCCCCCCCCCC(O)=O VLJCQMPCVZKWIE-UHFFFAOYSA-N 0.000 claims description 2
- MYWSBJKVOUZCIA-UHFFFAOYSA-N 2-hydroxy-3,5-diiodobenzaldehyde Chemical compound OC1=C(I)C=C(I)C=C1C=O MYWSBJKVOUZCIA-UHFFFAOYSA-N 0.000 claims description 2
- YZKLUEWQADEGKP-UHFFFAOYSA-N 5-(2,4-dichlorophenyl)cyclohexane-1,3-dione Chemical compound ClC1=CC(Cl)=CC=C1C1CC(=O)CC(=O)C1 YZKLUEWQADEGKP-UHFFFAOYSA-N 0.000 claims description 2
- FXUKWLSZZHVEJD-UHFFFAOYSA-N C16:0-14-methyl Natural products CCC(C)CCCCCCCCCCCCC(O)=O FXUKWLSZZHVEJD-UHFFFAOYSA-N 0.000 claims description 2
- IIUXHTGBZYEGHI-UHFFFAOYSA-N iso-margaric acid Natural products CC(C)CCCCCCCCCCCCCC(O)=O IIUXHTGBZYEGHI-UHFFFAOYSA-N 0.000 claims description 2
- YETXGSGCWODRAA-UHFFFAOYSA-N 17-methyloctadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCCCCC(O)=O YETXGSGCWODRAA-UHFFFAOYSA-N 0.000 claims 2
- 125000000896 monocarboxylic acid group Chemical group 0.000 claims 1
- 230000001936 parietal effect Effects 0.000 abstract 1
- 230000001256 tonic effect Effects 0.000 abstract 1
- 229920001296 polysiloxane Polymers 0.000 description 20
- 210000003128 head Anatomy 0.000 description 16
- 230000000694 effects Effects 0.000 description 15
- 238000011156 evaluation Methods 0.000 description 14
- 239000002253 acid Substances 0.000 description 13
- 238000001035 drying Methods 0.000 description 13
- 239000000284 extract Substances 0.000 description 11
- 239000003921 oil Substances 0.000 description 10
- 235000019198 oils Nutrition 0.000 description 10
- 150000001875 compounds Chemical class 0.000 description 8
- 150000007524 organic acids Chemical class 0.000 description 8
- 238000000034 method Methods 0.000 description 7
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- KIWBPDUYBMNFTB-UHFFFAOYSA-N Ethyl hydrogen sulfate Chemical compound CCOS(O)(=O)=O KIWBPDUYBMNFTB-UHFFFAOYSA-N 0.000 description 6
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
- 150000001261 hydroxy acids Chemical class 0.000 description 6
- NBIIXXVUZAFLBC-UHFFFAOYSA-N phosphoric acid Substances OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 6
- 230000000630 rising effect Effects 0.000 description 6
- 229910052710 silicon Inorganic materials 0.000 description 6
- 239000010703 silicon Substances 0.000 description 6
- 229910000831 Steel Inorganic materials 0.000 description 5
- 230000002378 acidificating effect Effects 0.000 description 5
- 229940024606 amino acid Drugs 0.000 description 5
- 239000003093 cationic surfactant Substances 0.000 description 5
- 230000003699 hair surface Effects 0.000 description 5
- 150000007522 mineralic acids Chemical class 0.000 description 5
- 239000002245 particle Substances 0.000 description 5
- 239000010959 steel Substances 0.000 description 5
- GHOKWGTUZJEAQD-ZETCQYMHSA-N (D)-(+)-Pantothenic acid Chemical compound OCC(C)(C)[C@@H](O)C(=O)NCCC(O)=O GHOKWGTUZJEAQD-ZETCQYMHSA-N 0.000 description 4
- WGVGLSURTKMQQC-UHFFFAOYSA-N 3-aminopropyl-ethyl-dimethylazanium Chemical compound CC[N+](C)(C)CCCN WGVGLSURTKMQQC-UHFFFAOYSA-N 0.000 description 4
- ODHCTXKNWHHXJC-VKHMYHEASA-N 5-oxo-L-proline Chemical compound OC(=O)[C@@H]1CCC(=O)N1 ODHCTXKNWHHXJC-VKHMYHEASA-N 0.000 description 4
- RGHNJXZEOKUKBD-SQOUGZDYSA-N D-gluconic acid Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O RGHNJXZEOKUKBD-SQOUGZDYSA-N 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
- AEMRFAOFKBGASW-UHFFFAOYSA-N Glycolic acid Chemical compound OCC(O)=O AEMRFAOFKBGASW-UHFFFAOYSA-N 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 description 4
- ODHCTXKNWHHXJC-GSVOUGTGSA-N Pyroglutamic acid Natural products OC(=O)[C@H]1CCC(=O)N1 ODHCTXKNWHHXJC-GSVOUGTGSA-N 0.000 description 4
- ODHCTXKNWHHXJC-UHFFFAOYSA-N acide pyroglutamique Natural products OC(=O)C1CCC(=O)N1 ODHCTXKNWHHXJC-UHFFFAOYSA-N 0.000 description 4
- 150000007513 acids Chemical class 0.000 description 4
- 239000002390 adhesive tape Substances 0.000 description 4
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 4
- 150000001413 amino acids Chemical class 0.000 description 4
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 4
- 239000004359 castor oil Substances 0.000 description 4
- 235000019438 castor oil Nutrition 0.000 description 4
- 238000010586 diagram Methods 0.000 description 4
- 239000004205 dimethyl polysiloxane Substances 0.000 description 4
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 4
- 239000004744 fabric Substances 0.000 description 4
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 4
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 description 4
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 4
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 4
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 4
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 4
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 235000021355 Stearic acid Nutrition 0.000 description 3
- 125000005211 alkyl trimethyl ammonium group Chemical group 0.000 description 3
- 239000003945 anionic surfactant Substances 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- WOWHHFRSBJGXCM-UHFFFAOYSA-M cetyltrimethylammonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCC[N+](C)(C)C WOWHHFRSBJGXCM-UHFFFAOYSA-M 0.000 description 3
- 125000004122 cyclic group Chemical group 0.000 description 3
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical class OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 description 3
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N dodecahydrosqualene Natural products CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 3
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- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 3
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Abstract
【解決手段】(A)特定の第4級アンモニウム又はその塩、0.01〜20質量%、(B)特定のエーテル型第3級アミン又はその塩、0.01〜20質量%、(C)特定の分岐脂肪酸又はその塩、0.005〜6質量%、(D)芳香族スルホン酸塩、0.05〜10質量%、及び水を含有し、成分(C)と成分(D)の質量比(C)/(D)が、0.05〜1である毛髪化粧料。
【選択図】なし
Description
R1R2R3R4N+X− (1)
〔式(1)中、R1、R2、R3又はR4のうち少なくとも一つは、エーテル結合を有していてもよい炭素数16〜25、直鎖又は分岐鎖の、アルキル基又はアルケニル基を示し、残りのうち少なくとも二つ以上は、同一又は異なる、炭素数1〜6のアルキル基、又は−(AO)mHを示す(Aは同一又は異なる、炭素数2〜4のアルキレン基、mは1〜6の整数を示し、その配列は任意である)、X−はハロゲン化物イオン又は炭素数1〜2のアルキル硫酸イオンを示す。〕
(B)下記式(2)で表されるエーテル型第3級アミン又はその塩 0.01〜20質量%
R9−(O−R24)e−NR10R11 (2)
〔式(2)中、R9は炭素数6〜24、直鎖又は分岐鎖の、アルキル基又はアルケニル基を示し、R10及びR11は同一又は異なる、炭素数1〜6のアルキル基、又は−(AO)mHを示し(Aは同一又は異なる、炭素数2〜4のアルキレン基、mは1〜6の整数を示し、その配列は任意である)、R24はヒドロキシ基が置換していてもよい炭素数1〜3の直鎖アルキル基(eは1〜5の整数を示す)。〕
(C)下記式(3)で表される分岐脂肪酸又はその塩 0.005〜6質量%
CH3−CHR18−(CH2)nCOOH (3)
〔式(3)中、R18はメチル基又はエチル基を示し、nは14〜20の整数を示す。〕
(D)芳香族スルホン酸塩 0.05〜10質量%
及び水を含有し、
成分(C)と成分(D)の質量比(C)/(D)が、0.05〜1である毛髪化粧料
が提供される。
本発明の成分(A)のカチオン界面活性剤は、下記式(1)で表される。
〔式(1)中、R1、R2、R3又はR4のうち少なくとも一つは、エーテル結合を有していてもよい炭素数16〜25、直鎖又は分岐鎖の、アルキル基又はアルケニル基を示し、残りのうち少なくとも二つ以上は、同一又は異なる、炭素数1〜6のアルキル基、又は−(AO)mHを示す(Aは同一又は異なる、炭素数2〜4のアルキレン基、mは1〜6の整数を示し、その配列は任意である)、X−はハロゲン化物イオン又は炭素数1〜2のアルキル硫酸イオンを示す。〕
例えば下記一般式(4)で表される化合物が挙げられる。
R5−N+(CH3)3X− (4)
〔式中、R5は炭素数16〜22の直鎖又は分岐鎖のアルキル基を示し、X−はハロゲン(塩素又は臭素)化物イオン又は炭素数1〜2のアルキル硫酸イオンを示す。〕
例えば下記一般式(5)で表される化合物が挙げられる。
R6−O−R7−N+(CH3)3X− (5)
〔式中、R6は炭素数16〜22の直鎖又は分岐鎖のアルキル基を示し、R7はエチレン基又はプロピレン基を示し、X−はハロゲン(塩素又は臭素)化物イオン又は炭素数1〜2のアルキル硫酸イオンを示す。〕
例えば下記一般式で表される化合物が挙げられる。
R8 2−N+(CH3)2X− (6)
〔式中、R8は炭素数16〜22の直鎖又は分岐鎖のアルキル基を示し、X−は上記と同じである。〕
その中でも、使用時に良好な柔軟性及び滑り性、ならびに仕上がりの髪の自然な質感を付与する効果の観点から、(A−i)アルキルトリメチルアンモニウム(またはその塩)が好ましく、中でも、炭素数16〜22のアルキル基を有するトリメチルアンモニウム(またはその塩)が好ましく、特に炭素数16〜18のアルキル基を有するトリメチルアンモニウム(またはその塩)が好ましい、さらにセチルトリメチルアンモニウム塩が好ましい。
本発明の成分(B)は、下記式(2)で表される。
R9−(O−R24)e−NR10R11 (2)
〔式(2)中、R9は炭素数6〜24、直鎖又は分岐鎖の、アルキル基又はアルケニル基を示し、R10及びR11は同一又は異なる、炭素数1〜6のアルキル基、又は−(AO)mHを示し(Aは同一又は異なる、炭素数2〜4のアルキレン基、mは1〜6の整数を示し、その配列は任意である)、R24はヒドロキシ基が置換していてもよい炭素数1〜3の直鎖アルキル基(eは1〜5の整数を示す)。〕
例えば下記一般式(7)で表される化合物及びその塩が挙げられる。
例えば下記一般式(8)で表される化合物またはその塩が挙げられる。
本発明の成分(C)は、下記式(3)で表される。
CH3−CHR18−(CH2)nCOOH (3)
〔式(3)中、R18はメチル基又はエチル基を示し、nは14〜20の整数を示す。〕
本発明の成分(D)の、芳香族スルホン酸としては、芳香環を1つ含む2−ナフタレンスルホン酸、オキシベンゾンスルホン酸、サリチル酸又はグアイアズレンスルホン酸等が挙げられる。対イオンとしては、例えばナトリウム、カリウム等のアルカリ金属塩、カルシウム、マグネシウム等のアルカリ土類金属塩などが挙げられる。中でもスルホン酸塩が好ましく、特に2−ナフタレンスルホン酸ナトリウムが好ましい。
本発明の毛髪化粧料は塗布のしやすさ、滑らかな使用感、柔軟性のある感触の観点から脂肪族アルコールを併用することが望ましく、炭素数12〜22のアルキル、アルケニル基を有するものが好ましい。例えば、ベヘニルアルコール、ステアリルアルコール、セチルアルコール、ミリスチルアルコール、ラウリルアルコール、オレイルアルコール、イソステアリルアルコールなどが挙げられる。中でもステアリルアルコール、セチルアルコールが好ましい。これら脂肪族アルコールは単独で用いても、数種類組み合わせて用いてもよい。
(i)高重合ジメチルポリシロキサン
例えば、BY11−026、BY22−19〔東レ・ダウコーニング株式会社〕、FZ−3125〔日本ユニカー株式会社〕等が挙げられる。
上記以外に、ポリエーテル変性シリコーン、メチルフェニルポリシロキサン、脂肪酸変性シリコーン、アルコール変性シリコーン、アルコキシ変性シリコーン、エポキシ変性シリコーン、フッ素変性シリコーン、環状シリコーン、アルキル変性シリコーン等が挙げられる。
カプリン酸、ラウリン酸、ミリスチン酸、パルミチン酸、ステアリン酸、ベヘニン酸、オレイン酸、ヤシ油脂肪酸等の成分(C)以外の高級脂肪酸、流動パラフィン、流動イソパラフィン、ワセリン、スクワレン、スクワラン等の炭化水素油等が挙げられる。また、ツバキ油、マカデミアナッツ油、トウモロコシ油、オリーブ油、アボカド油、ヒマシ油、サフラワー油、ホホバ油、ヒマワリ油、ナタネ油、ゴマ油、大豆油、メドウフォーム油等の天然油;ミリスチン酸イソプロピル、パルミチン酸イソプロピル、ミルスチン酸ミリスチル、パルミチン酸オクチル、ステアリン酸ステアリル、ステアリン酸イソセチル、イソノナン酸イソノニル、イソノナン酸イソトリデシル、ステアリン酸硬化ヒマシ油、ヒドロキシステアリン酸硬化ヒマシ油、トリ2−エチルヘキサン酸グリセリル、テトラ2−エチルヘキサン酸ペンタエリスリトール、ジカプリン酸ネオペンチルグリコール、ジイソステアリン酸ジグリセリル、ジペンタエリスリトールとヒドロキシステアリン酸/ステアリン酸/ロジン酸等の混合脂肪酸とのエステル等のエステル油が挙げられる。
(i)アルキルアミドアミン(及びその塩)
例えば下記一般式(12)で表される化合物及びその塩が挙げられる。
コールドパーマ、ブリーチ等の美容処理を行った日本人女性の毛髪20g(約15−20cm)を束ね、シャンプーで洗浄した。この毛髪に毛髪化粧料2gを均一に塗布し、次いで30秒間流水ですすぎ流した後、タオルドライを行い、さらにドライヤー乾燥を行って毛髪の「洗髪後の滑らかさ」、「乾燥後毛髪全体のボリューム感」、「乾燥後の浮き毛・はね毛のなさ」、「乾燥後の指通り」、「乾燥後のまとまり」、を官能評価した。評価は、下記の評価基準に基づき、5人で4段階評価で行った。その評価の合計値を表1,2に示した。
「洗髪後の滑らかさ」
4:非常になめらか
3:ややなめらか
2:あまりなめらかでない
1:なめらかでない
4:非常に髪全体のボリューム感がある
3:やや髪全体にボリューム感がある
2:あまり髪全体にボリューム感がない
1:髪全体にボリューム感がない
4:まったく浮き毛・はね毛がみられない
3:ほとんど浮き毛・はね毛がみられない
2:浮き毛・はね毛がやや目立つ
1:浮き毛・はね毛が目立つ
4:非常に指通りがよい
3:やや指通りがよい
2:あまり指通りがよくない
1:指通りがよくない
4:非常によくまとまる
3:ややまとまる
2:あまりまとまらない
1:まとまらない
市販カーリングアイロン(巻き付け直径3cm)を用いて、官能評価後の毛髪束を130〜150℃の温度で5秒間巻き付ける操作を連続で2回繰り返した。ついたくせのつきやすさを、下記の評価基準に基づき、5人で4段階評価で行った。その評価の合計値を表1,2に示した。
「熱による癖づけの容易さ」
4:非常にくせがつきやすい
3:ややくせがつきやすい
2:くせがあまりつかない
1:くせがつかない
以下のようにして、毛髪の立ち上がり評価を行った。
<モデル毛束の作成>
(材料)
・サンプル毛髪:Europian Blond毛21本(長さ22〜23cm、平均径78.2μm(n=15;レーザー外径測定装置にて測定)DEMEO BROTHERS inc.より購入)
・シリコンマイクロチューブ:内径×外径(mm)0.4×0.5 長さ1.5cm×7本(品番1−8194−04 アズワン株式会社)
・鋼線(又はステンレス線):直径1.5mm長さ2.0cm×7本
・布粘着テープ:1cm×3cm(NICHIBAN No.102N)
・ビニールテープ:0.6cm×1.0cm(ヤマト株式会社NO200−19−5)
・ナイロンテグス:直径0.18mm 適量 (ハリスライカ本舗)
まず、1.5cmの長さに切断した直径0.5mm(内径0.4mm)のシリコンチューブに根元方向を揃えたサンプル毛髪3本を根元部分から通し端をシリコンチューブごとこま結びで止め、シリコンチューブ1を作成した。同様にして、シリコンチューブ1を7組作成し、そのうち1組のシリコンチューブ1についてビニールテープ2を巻き付けて太くし、芯部とした。次に、長さ2cm直径1.5mmの鋼線3(またはステンレス線)を用意し、残り6組のシリコンチューブ1を6本の鋼線3の間に配置し、芯部と残り1本の鋼線3を中心にして束ね、布粘着テープ4を用いて全体を巻き付けた。さらに、布粘着テープ4の上からテグス5を巻き締めてモデル毛束10を作成した。
図2〜4を用いて、立ち上がり量の測定方法について説明する。
毛髪化粧料をイオン交換水を用いて20倍希釈した水溶液をサンプル水溶液とした。
図2に示すようにして、固定具6を用いて、モデル毛束10を、サンプル毛髪が上向きになるように固定し、サンプル水溶液5mlをサンプル毛髪の毛束の屈曲部頂点付近に滴下し、その後イオン交換水5mlにて同様の滴下法で十分すすぎ、室温(25℃)、50(±10)RH%条件下10分間静置により十分自然乾燥させた。乾燥前後の毛束の屈曲部をデジカメにて撮影し、変化を記録した。
図3に示すように、すすぎ直後の毛束の屈曲部の高さの最大値を(h1)とし、図4に示すように、乾燥後の毛束の屈曲部の高さの最大値を高さ(h2)として、立ち上がり量(Δh=h2−h1)とした。
2 ビニールテープ
3 鋼線
4 布粘着テープ
5 テグス
6 固定具
10 モデル毛束
Claims (6)
- (A)下記式(1)で表される第4級アンモニウム又はその塩 0.01〜20質量%
R1R2R3R4N+X− (1)
〔式(1)中、R1、R2、R3又はR4のうち少なくとも一つは、エーテル結合を有していてもよい炭素数16〜25、直鎖又は分岐鎖の、アルキル基又はアルケニル基を示し、残りのうち少なくとも二つ以上は、同一又は異なる、炭素数1〜6のアルキル基、又は−(AO)mHを示す(Aは同一又は異なる、炭素数2〜4のアルキレン基、mは1〜6の整数を示し、その配列は任意である)、X−はハロゲン化物イオン又は炭素数1〜2のアルキル硫酸イオンを示す。〕
(B)下記式(2)で表されるエーテル型第3級アミン又はその塩 0.01〜20質量%
R9−(O−R24)e−NR10R11 (2)
〔式(2)中、R9は炭素数6〜24、直鎖又は分岐鎖の、アルキル基又はアルケニル基を示し、R10及びR11は同一又は異なる、炭素数1〜6のアルキル基、又は−(AO)mHを示し(Aは同一又は異なる、炭素数2〜4のアルキレン基、mは1〜6の整数を示し、その配列は任意である)、R24はヒドロキシ基が置換していてもよい炭素数1〜3の直鎖アルキル基(eは1〜5の整数を示す)。〕
(C)下記式(3)で表される分岐脂肪酸又はその塩 0.005〜6質量%
CH3−CHR18−(CH2)nCOOH (3)
〔式(3)中、R18はメチル基又はエチル基を示し、nは14〜20の整数を示す。〕
(D)芳香族スルホン酸塩 0.05〜10質量%
及び水を含有し、
成分(C)と成分(D)の質量比(C)/(D)が、0.05〜1である毛髪化粧料。 - 成分(A)が、セチルトリメチルアンモニウム又はその塩を少なくとも含む請求項1に記載の毛髪化粧料。
- 成分(B)が、N,N−ジメチル−3−ヘキサデシルオキシプロピルアミン、N,N−ジメチル−3−オクタデシルオキシプロピルアミン、又はこれらの塩から選ばれる1種または2種以上を含む請求項1または2に記載の毛髪化粧料。
- 成分(C)が、18−メチルエイコサン酸、14−メチルペンタデカン酸、14−メチルヘキサデカン酸、15−メチルヘキサデカン酸、15−メチルヘプタデカン酸、16−メチルヘプタデカン酸、16−メチルオクタデカン酸、17−メチルオクタデカン酸、17−メチルノナデカン酸、ラノリン脂肪酸から選ばれる1種または2種以上を含む請求項1または2記載の毛髪化粧料。
- 成分(D)が、2−ナフタレンスルホン酸又はその塩を少なくとも含む請求項1乃至4いずれか一項に記載の毛髪化粧料。
- 水で20質量倍に希釈した際のpH(25℃)が、1〜5である請求項1乃至5いずれか一項に記載の毛髪化粧料。
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JP2016216432A (ja) * | 2015-05-26 | 2016-12-22 | 花王株式会社 | 毛髪化粧料 |
JP2018070566A (ja) * | 2016-11-04 | 2018-05-10 | 花王株式会社 | メラニン分解促進剤 |
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TWI222872B (en) * | 1997-12-08 | 2004-11-01 | Kao Corp | Cuticle caring method, hair volume enhancing method and hair cosmetic composition |
FR2825269B1 (fr) | 2001-05-31 | 2003-08-08 | Oreal | Composition cosmetique comprenant des particules de carbonate de calcium et une association de tensioactifs |
ES2435741T3 (es) * | 2001-08-06 | 2013-12-23 | Kao Corporation | Composición acondicionadora |
JP3987314B2 (ja) * | 2001-09-14 | 2007-10-10 | 花王株式会社 | 毛髪化粧料 |
EP1443885B1 (en) | 2001-11-02 | 2015-01-21 | The Procter & Gamble Company | Composition containing a cationic polymer and water insoluble solid material |
FR2845279B1 (fr) | 2002-10-04 | 2006-06-16 | Oreal | Utilisation de latex cationiques non filmogenes pour l'augmentation de volume de la chevelure. |
CN101321512B (zh) * | 2005-12-01 | 2011-12-07 | 花王株式会社 | 水性毛发化妆品组合物 |
JP5094216B2 (ja) * | 2007-05-31 | 2012-12-12 | 花王株式会社 | 毛髪化粧料 |
JP4997079B2 (ja) * | 2007-11-27 | 2012-08-08 | 花王株式会社 | 毛髪化粧料 |
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2010
- 2010-08-03 JP JP2010174307A patent/JP5959796B2/ja active Active
-
2011
- 2011-07-29 CN CN2011800381760A patent/CN103052377A/zh active Pending
- 2011-07-29 US US13/814,185 patent/US20130139843A1/en not_active Abandoned
- 2011-07-29 BR BR112013002753A patent/BR112013002753A2/pt not_active Application Discontinuation
- 2011-07-29 WO PCT/JP2011/004320 patent/WO2012017634A1/ja active Application Filing
- 2011-07-29 EP EP11814271.0A patent/EP2601929A4/en not_active Withdrawn
- 2011-08-03 TW TW100127635A patent/TWI532505B/zh active
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JPH11228358A (ja) * | 1997-12-08 | 1999-08-24 | Kao Corp | 毛髪化粧料 |
JP2006045183A (ja) * | 2004-07-02 | 2006-02-16 | Kao Corp | 毛髪化粧料 |
JP2008297218A (ja) * | 2007-05-29 | 2008-12-11 | Kao Corp | 毛髪化粧料 |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2016216432A (ja) * | 2015-05-26 | 2016-12-22 | 花王株式会社 | 毛髪化粧料 |
JP2018070566A (ja) * | 2016-11-04 | 2018-05-10 | 花王株式会社 | メラニン分解促進剤 |
Also Published As
Publication number | Publication date |
---|---|
US20130139843A1 (en) | 2013-06-06 |
CN103052377A (zh) | 2013-04-17 |
EP2601929A4 (en) | 2015-08-05 |
TW201208709A (en) | 2012-03-01 |
BR112013002753A2 (pt) | 2016-08-30 |
WO2012017634A1 (ja) | 2012-02-09 |
JP5959796B2 (ja) | 2016-08-02 |
TWI532505B (zh) | 2016-05-11 |
EP2601929A1 (en) | 2013-06-12 |
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