JP2011502924A5 - - Google Patents
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- Publication number
- JP2011502924A5 JP2011502924A5 JP2010532074A JP2010532074A JP2011502924A5 JP 2011502924 A5 JP2011502924 A5 JP 2011502924A5 JP 2010532074 A JP2010532074 A JP 2010532074A JP 2010532074 A JP2010532074 A JP 2010532074A JP 2011502924 A5 JP2011502924 A5 JP 2011502924A5
- Authority
- JP
- Japan
- Prior art keywords
- solvent
- filtration
- mixture
- reaction
- concentrating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002904 solvent Substances 0.000 claims 8
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims 6
- 238000001914 filtration Methods 0.000 claims 6
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims 6
- 239000006227 byproduct Substances 0.000 claims 5
- 238000000034 method Methods 0.000 claims 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 5
- CBWJKNQKWLEEPG-UHFFFAOYSA-N dihydridoborate(1-) Chemical compound [BH2-] CBWJKNQKWLEEPG-UHFFFAOYSA-N 0.000 claims 4
- 230000002194 synthesizing effect Effects 0.000 claims 4
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims 3
- 239000000203 mixture Substances 0.000 claims 3
- 239000011541 reaction mixture Substances 0.000 claims 3
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims 2
- 239000002253 acid Substances 0.000 claims 2
- 230000002378 acidificating effect Effects 0.000 claims 2
- 125000001931 aliphatic group Chemical group 0.000 claims 2
- 239000007810 chemical reaction solvent Substances 0.000 claims 2
- 238000004090 dissolution Methods 0.000 claims 2
- 239000003456 ion exchange resin Substances 0.000 claims 2
- 229920003303 ion-exchange polymer Polymers 0.000 claims 2
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 claims 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims 1
- 239000004327 boric acid Substances 0.000 claims 1
- 229920001429 chelating resin Polymers 0.000 claims 1
- 239000012046 mixed solvent Substances 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US163307P | 2007-11-02 | 2007-11-02 | |
| US61/001,633 | 2007-11-02 | ||
| PCT/US2008/012473 WO2009058408A1 (en) | 2007-11-02 | 2008-11-03 | Methods of preparing clusterboron |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2011502924A JP2011502924A (ja) | 2011-01-27 |
| JP2011502924A5 true JP2011502924A5 (enExample) | 2011-12-08 |
| JP5710976B2 JP5710976B2 (ja) | 2015-04-30 |
Family
ID=40591393
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010532074A Expired - Fee Related JP5710976B2 (ja) | 2007-11-02 | 2008-11-03 | クラスターボロンの調製方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US8753600B2 (enExample) |
| EP (1) | EP2205524B1 (enExample) |
| JP (1) | JP5710976B2 (enExample) |
| KR (2) | KR101586868B1 (enExample) |
| CN (1) | CN101848855B (enExample) |
| WO (1) | WO2009058408A1 (enExample) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2789207C (en) * | 2010-02-10 | 2015-09-01 | M-I Drilling Fluids Uk Limited | Method and system for decontaminating sand |
| WO2013115889A2 (en) | 2011-11-18 | 2013-08-08 | The Curators Of The University Of Missouri | Process and device for the production of polyhedral boranes |
| CN120965735A (zh) * | 2021-08-26 | 2025-11-18 | 吉林奥来德光电材料股份有限公司 | 硼化合物、发光材料和有机电致发光器件 |
| KR102859382B1 (ko) * | 2023-03-21 | 2025-09-12 | 파미셀 주식회사 | 대용량 고순도의 dNTP 제조 방법 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3577679B2 (ja) * | 1995-03-24 | 2004-10-13 | 日本化学工業株式会社 | メソポーラスアルミノシリケートの製造方法 |
| KR100788474B1 (ko) * | 2002-06-26 | 2007-12-24 | 세미이큅, 인코포레이티드 | 자기 요크 어셈블리 |
| WO2005060602A2 (en) * | 2003-12-12 | 2005-07-07 | Semequip, Inc. | Controlling the flow of vapors sublimated from solids |
| TWI375660B (en) * | 2004-01-22 | 2012-11-01 | Semequip Inc | Isotopically-enriched boranes and methods of preparing them |
| JP5025633B2 (ja) * | 2004-02-02 | 2012-09-12 | エスイーエム・エクイップ インコーポレイテッド | Ｂ１０ｈ１０２−アンモニウム塩の製造方法及びｂ１８ｈ２２の製造方法 |
| US8623309B2 (en) * | 2007-11-02 | 2014-01-07 | Semequip, Inc. | Methods of preparing clusterboron |
| JP5710975B2 (ja) * | 2007-11-02 | 2015-04-30 | セメクイップ， インコーポレイテッド | クラスターボロンの調製方法 |
-
2008
- 2008-11-03 JP JP2010532074A patent/JP5710976B2/ja not_active Expired - Fee Related
- 2008-11-03 WO PCT/US2008/012473 patent/WO2009058408A1/en not_active Ceased
- 2008-11-03 KR KR1020107010911A patent/KR101586868B1/ko not_active Expired - Fee Related
- 2008-11-03 KR KR1020157025455A patent/KR20150108947A/ko not_active Ceased
- 2008-11-03 CN CN200880114573.XA patent/CN101848855B/zh not_active Expired - Fee Related
- 2008-11-03 EP EP08844999.6A patent/EP2205524B1/en not_active Not-in-force
-
2011
- 2011-01-18 US US13/008,724 patent/US8753600B2/en not_active Expired - Fee Related
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