JP2010513027A - 分散系を製造するための装置および分散系を製造する方法 - Google Patents
分散系を製造するための装置および分散系を製造する方法 Download PDFInfo
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- JP2010513027A JP2010513027A JP2009543193A JP2009543193A JP2010513027A JP 2010513027 A JP2010513027 A JP 2010513027A JP 2009543193 A JP2009543193 A JP 2009543193A JP 2009543193 A JP2009543193 A JP 2009543193A JP 2010513027 A JP2010513027 A JP 2010513027A
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- stator
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- ROORDVPLFPIABK-UHFFFAOYSA-N diphenyl carbonate Chemical compound C=1C=CC=CC=1OC(=O)OC1=CC=CC=C1 ROORDVPLFPIABK-UHFFFAOYSA-N 0.000 description 1
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- RXOHFPCZGPKIRD-UHFFFAOYSA-N naphthalene-2,6-dicarboxylic acid Chemical compound C1=C(C(O)=O)C=CC2=CC(C(=O)O)=CC=C21 RXOHFPCZGPKIRD-UHFFFAOYSA-N 0.000 description 1
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- 150000007524 organic acids Chemical class 0.000 description 1
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- 125000005702 oxyalkylene group Chemical group 0.000 description 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 1
- 229940044654 phenolsulfonic acid Drugs 0.000 description 1
- 125000000951 phenoxy group Chemical group [H]C1=C([H])C([H])=C(O*)C([H])=C1[H] 0.000 description 1
- 235000021317 phosphate Nutrition 0.000 description 1
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- 229920006324 polyoxymethylene Polymers 0.000 description 1
- 229920001451 polypropylene glycol Polymers 0.000 description 1
- 229920000909 polytetrahydrofuran Polymers 0.000 description 1
- 229920006295 polythiol Polymers 0.000 description 1
- 229920000166 polytrimethylene carbonate Polymers 0.000 description 1
- UWHMFGKZAYHMDJ-UHFFFAOYSA-N propane-1,2,3-trithiol Chemical compound SCC(S)CS UWHMFGKZAYHMDJ-UHFFFAOYSA-N 0.000 description 1
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- 238000010526 radical polymerization reaction Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
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- 229920006395 saturated elastomer Polymers 0.000 description 1
- 125000000467 secondary amino group Chemical group [H]N([*:1])[*:2] 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- FZHAPNGMFPVSLP-UHFFFAOYSA-N silanamine Chemical class [SiH3]N FZHAPNGMFPVSLP-UHFFFAOYSA-N 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 229950000244 sulfanilic acid Drugs 0.000 description 1
- 125000001273 sulfonato group Chemical class [O-]S(*)(=O)=O 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 150000003512 tertiary amines Chemical class 0.000 description 1
- FAGUFWYHJQFNRV-UHFFFAOYSA-N tetraethylenepentamine Chemical compound NCCNCCNCCNCCN FAGUFWYHJQFNRV-UHFFFAOYSA-N 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 description 1
- RUELTTOHQODFPA-UHFFFAOYSA-N toluene 2,6-diisocyanate Chemical compound CC1=C(N=C=O)C=CC=C1N=C=O RUELTTOHQODFPA-UHFFFAOYSA-N 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- 239000002888 zwitterionic surfactant Substances 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/50—Mixing liquids with solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
- B01F23/41—Emulsifying
- B01F23/4105—Methods of emulsifying
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/27—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices
- B01F27/271—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator
- B01F27/2711—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator provided with intermeshing elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
- B01F2101/2805—Mixing plastics, polymer material ingredients, monomers or oligomers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2215/00—Auxiliary or complementary information in relation with mixing
- B01F2215/04—Technical information in relation with mixing
- B01F2215/0413—Numerical information
- B01F2215/0436—Operational information
- B01F2215/0472—Numerical temperature values
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2215/00—Auxiliary or complementary information in relation with mixing
- B01F2215/04—Technical information in relation with mixing
- B01F2215/0413—Numerical information
- B01F2215/0436—Operational information
- B01F2215/0481—Numerical speed values
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dispersion Chemistry (AREA)
- Polyurethanes Or Polyureas (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Colloid Chemistry (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
- Graft Or Block Polymers (AREA)
Abstract
Description
本願は、2006年12月19日出願の米国特許仮出願第60/875,657号、標題「A device for producing dispersions and method of producing dispersions」(分散系を製造するための装置および分散系を製造する方法)の優先権を主張する非仮出願であり、その教示は本明細書の下文において完全に再現されるかのように本明細書に組み込まれる。
(1)スルホン酸基含有化合物、例えば2−オキシエタンスルホン酸、フェノールスルホン酸、スルホ安息香酸、スルホコハク酸、5−スルホイソフタル酸、スルファニル酸、1,3−フェニレンジアミン−4,6−ジスルホン酸、および2,4−ジアミノトルエン−5−スルホン酸、ならびにそれらの誘導体、またはそれらを共重合することにより得られるポリエステルポリオール;
(2)カルボン酸含有化合物、例えば2,2−ジメチロールプロピオン酸、2,2−ジメチロール酪酸、2,2−ジメチロール吉草酸、ジオキシマレイン酸、2,6−ジオキシ安息香酸、および3,4−ジアミノ安息香酸、ならびにそれらの誘導体、またはそれらを共重合することにより得られるポリエステルポリオール;第三級アミノ基含有化合物、例えばメチルジエタノールアミン、ブチルジエタノールアミン、およびアルキルジイソプロパノールアミン、ならびにそれらの誘導体、またはそれらを共重合することにより得られるポリエステルポリオールもしくはポリエーテルポリオール;
(3)上記第三級アミノ基含有化合物の反応生成物、またはそれらの誘導体、または四級化剤、例えばメチルクロライド、メチルブロミド、ジメチル硫酸、ジエチル硫酸、ベンジルクロライド、ベンジルブロミド、エチレンクロロヒドリン、エチレンブロモヒドリン、エピクロロヒドリン、およびブロモブタンなどを用いてそれらを共重合することにより得られるポリエステルポリオールもしくはポリエーテルポリオール;
(4)非イオン基含有化合物、例えばポリオキシエチレングリコールまたはポリオキシエチレン−ポリオキシプロピレン共重合体グリコール(少なくとも30重量%のエチレンオキシド反復単位と少なくとも1つの活性水素をポリマー中に有し、また、300〜20,000の分子量を有する)、ポリオキシエチレン−ポリオキシブチレン共重合体グリコール、ポリオキシエチレン−ポリオキシアルキレン共重合体グリコール、およびそれらのモノアルキルエーテル、あるいはそれらを共重合することにより得られるポリエステル−ポリエーテルポリオール;ならびに
(5)それらの組合せ
が挙げられる。
Claims (13)
- 第1の固定子と;
第2の固定子と;
前記第1の固定子および前記第2の固定子を包み込んでいる(encasing)シェルと;
回転子(rotor)と、ここで、前記回転体(rotator)は前記第1の固定子と前記第2の固定子との間に配置され、それにより第1のチャンバおよび第2のチャンバを形成し;
前記第1のチャンバの中に入る少なくとも1つの第1の入口と;
前記第2のチャンバから外に出る少なくとも1つの出口と
を備える、分散系を製造するための装置。 - 前記装置が、前記第2のチャンバの中に入る少なくとも1つの第2の入口をさらに含む、請求項1に記載の装置。
- 前記第1のチャンバが高剪断チャンバであり、かつ前記第2のチャンバが低剪断チャンバである、請求項1に記載の装置。
- 前記第2の固定子が、前記第1の固定子よりも少ない数の環状の(ring-shaped)固定子歯を有する、請求項1に記載の装置。
- 前記回転子が第1の表面および第2の表面を有し、かつ、前記第2の表面が前記第1の表面よりも少ない数の環状の回転子歯を有する、請求項4に記載の装置。
- ポリウレタン分散系を製造する方法であって、
第1の固定子と;
第2の固定子と;
前記第1の固定子および前記第2の固定子を包み込んでいるシェルと;
回転子と、ここで、前記回転体は前記第1の固定子と前記第2の固定子との間に配置され、それにより第1のチャンバおよび第2のチャンバを形成し;
前記第1のチャンバの中に入る少なくとも1つの第1の入口と;
前記第2のチャンバから外に出る少なくとも1つの出口と;
前記第2のチャンバの中に入る少なくとも1つの第2の入口と
を備える、分散系を製造するための装置を準備する工程と;
プレポリマー相および水相を、前記第1の入口を経由して前記第1のチャンバの中に導入する工程と;
前記プレポリマー相を前記水相中で乳化する工程と;
それによりプレポリマー乳濁液を製造する工程と;
鎖延長剤を、前記第2の入口を経由して前記第2のチャンバ中の前記乳濁液の中に導入する工程と;
前記プレポリマーを鎖延長する工程と;
それによりポリウレタン分散系を製造する工程と
を含む、方法。 - 前記第1のチャンバが高剪断チャンバであり、かつ前記第2のチャンバが低剪断チャンバである、請求項6に記載のポリウレタン分散系を製造する方法。
- 前記第2の固定子が、前記第1の固定子よりも少ない数の環状の固定子歯を有する、請求項6に記載のポリウレタン分散系を製造する方法。
- 前記回転子が第1の表面および第2の表面を有し、かつ、前記第2の表面が前記第1の表面よりも少ない数の環状の回転子歯を有する、請求項6に記載のポリウレタン分散系を製造する方法。
- 高分子分散系、乳濁液またはラテックスを製造する方法であって、
第1の固定子と;
第2の固定子と;
前記第1の固定子および前記第2の固定子を包み込んでいるシェルと;
回転子と、ここで、前記回転体は前記第1の固定子と前記第2の固定子との間に配置され、それにより第1のチャンバおよび第2のチャンバを形成し;
前記第1のチャンバの中に入る少なくとも1つの第1の入口と;
前記第2のチャンバから外に出る少なくとも1つの出口と;
所望により、前記第2のチャンバの中に入る少なくとも1つの第2の入口と
を備える、分散系を製造するための装置を準備する工程と;
ポリマー相および水相を、前記第1の入口を経由して前記第1のチャンバの中に導入する工程と;
前記ポリマー相を前記水相中で乳化する工程と;
それによりポリマー乳濁液を製造する工程と;
所望により、希釈剤相を、前記随意の前記第2の入口を経由して前記第2のチャンバの中に導入する工程と;
それにより前記高分子分散系、乳濁液またはラテックスを製造する工程と
を含む、方法。 - 前記第1のチャンバが高剪断チャンバであり、かつ前記第2のチャンバが低剪断チャンバである、請求項10に記載の高分子分散系を製造する方法。
- 前記第2の固定子が、前記第1の固定子よりも少ない数の環状の固定子歯を有する、請求項10に記載の高分子分散系を製造する方法。
- 前記回転子が第1の表面および第2の表面を有し、かつ、前記第2の表面が前記第1の表面よりも少ない数の環状の回転子歯を有する、請求項10に記載の高分子分散系を製造する方法。
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JP2016166199A (ja) * | 2009-11-02 | 2016-09-15 | マンカインド コーポレ−ション | 析出プロセスにおいて医薬粒子を生成するための反応器 |
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EP2121171B1 (en) | 2011-01-26 |
WO2008077116B1 (en) | 2008-10-23 |
BRPI0719471A2 (pt) | 2014-02-11 |
CN101610832B (zh) | 2015-01-21 |
WO2008077116A3 (en) | 2008-08-28 |
KR20090094459A (ko) | 2009-09-07 |
ATE496686T1 (de) | 2011-02-15 |
EP2121171A2 (en) | 2009-11-25 |
KR101454045B1 (ko) | 2014-10-27 |
US8506889B2 (en) | 2013-08-13 |
BRPI0719471B1 (pt) | 2018-07-03 |
MX2009006625A (es) | 2009-08-26 |
CA2673168A1 (en) | 2008-06-26 |
TWI428172B (zh) | 2014-03-01 |
JP4949482B2 (ja) | 2012-06-06 |
US20120327739A1 (en) | 2012-12-27 |
WO2008077116A2 (en) | 2008-06-26 |
US8283393B2 (en) | 2012-10-09 |
RU2009127796A (ru) | 2011-01-27 |
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US20090312489A1 (en) | 2009-12-17 |
DE602007012310D1 (de) | 2011-03-10 |
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