JP2009122662A - 偏光板、光学フィルムおよび画像表示装置 - Google Patents
偏光板、光学フィルムおよび画像表示装置 Download PDFInfo
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- JP2009122662A JP2009122662A JP2008270799A JP2008270799A JP2009122662A JP 2009122662 A JP2009122662 A JP 2009122662A JP 2008270799 A JP2008270799 A JP 2008270799A JP 2008270799 A JP2008270799 A JP 2008270799A JP 2009122662 A JP2009122662 A JP 2009122662A
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- Prior art keywords
- liquid crystal
- polarizing plate
- film
- transparent protective
- protective film
- Prior art date
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Landscapes
- Polarising Elements (AREA)
- Liquid Crystal (AREA)
Abstract
【解決手段】偏光子の片面に、接着剤層、透明保護フィルムAおよび液晶光学補償層をこの順で有し、他の片面に接着剤層、透明保護フィルムBをこの順で有する偏光板であって、前記液晶光学補償層は、液晶の光軸を傾斜配向させて得られる液晶光学補償層であり、かつ、前記透明保護フィルムAおよび透明保護フィルムBのいずれか少なくとも一方は、ラクトン環構造を有する(メタ)アクリル系樹脂を含有することを特徴とする偏光板。
【選択図】図1
Description
前記液晶光学補償層は、液晶の光軸を傾斜配向させて得られる液晶光学補償層であり、かつ、
前記透明保護フィルムAおよび透明保護フィルムBのいずれか少なくとも一方は、ラクトン環構造を有する(メタ)アクリル系樹脂を含有することを特徴とする偏光板、に関する。
ロイル基、メタクリロイル基、アジド基、エポキシ基などがあげられる。
透明保護フィルムの波長590nmにおける屈折率nx、ny、nzを、平行ニコル回転法を原理とする自動複屈折測定装置(王子計測機器株式会社製,自動複屈折計KOBRA21ADH)により計測し、面内位相差Re、厚み方向位相差Rthを算出した。
JIS Z0208の透湿度試験(カップ法)に準じて、温度40℃、湿度92%RHの雰囲気中、面積1m2の試料を24時間に通過する水蒸気のg数を測定した値である。
調製した接着剤水溶液(常温:23℃)を、レオメーター(RSI‐HS,HAAKE社製)により測定した。
アルミナコロイド水溶液を粒度分布計(日機装社製,ナノトラックUPA150)により、動的光散乱法(光相関法)で測定した。
平均重合度2400、ケン化度99.9モル%、厚さ75μmのポリビニルアルコールフィルムを、30℃の温水中に60秒間浸漬して膨潤させた。次いで、0.3重量%(重量比:ヨウ素/ヨウ化カリウム=0.5/8)の30℃のヨウ素溶液中で1分間染色しながら、3.5倍まで延伸した。次いで、65℃の3重量%のホウ酸エステル水溶液中に10秒間浸漬しながら総合延伸倍率が6倍まで延伸した。その後、40℃のオーブンで3分間乾燥を行い、厚さ30μmの偏光子を得た。
以下に示すものを用いた。
透明保護フィルム1:前記一般式(1)中、R1は水素原子、R2およびR3はメチル基であるラクトン環構造を有する(メタ)アクリル系樹脂[共重合モノマーの重量比:メタクリル酸メチル/2−(ヒドロキシメチル)アクリル酸メチル=8/2;ラクトン環化率約100%]90重量部とアクリロニトリル−スチレン(AS)樹脂{トーヨーAS AS20,東洋スチレン(株)製}10重量部の混合物を押出成形し、縦2.0倍、横2.4倍に延伸した透明保護フィルム(厚さ40μm,Re=0nm,Rth=0nm)を用いた。
透明保護フィルム2:厚さ40μmのトリアセチルセルロースフィルム(富士フィルム(株)製,Re=1nm,Rth=50nm)を用いた。
透明保護フィルム3:厚さ50μmのポリエチレンテレフタレートフィルム(東洋紡績(株)製,商品名:コスモシャインA4100(片面易接着処理層付),Re=100nm)を用いた。
富士フイルム社製のワイドビュー(WV)フィルムを用いた。WVフィルムは、透明基材フィルムであるセルロース系高分子フィルム(透明保護フィルム2)上に、ディスコティック液晶分子が傾斜配向しているディスコティック液晶層(DIS:表1中で略)を有していた。
アセトアセチル基を含有するポリビニルアルコール系樹脂(平均重合度:1200,ケン化度:98.5モル%,アセトアセチル化度:5モル%)100部に対し、メチロールメラミン50部を、30℃の温度条件下に、純水に溶解し、固形分濃度3.7%に調整した水溶液を調製した。前記水溶液100部に対し、アルミナコロイド水溶液(平均粒子径15nm,固形分濃度10%,正電荷)18部を加えて接着剤水溶液を調製した。接着剤水溶液の粘度は9.6mPa・sであった。接着剤水溶液のpHは、4−4.5の範囲であった。これを接着剤1とする。また、前記接着剤1において、アルミナコロイド水溶液を加えなかった接着剤水溶液を調製した。接着剤水溶液の粘度は7.0mPa・sであった。接着剤水溶液のpHは、4−4.5の範囲であった。これを接着剤2とする。
<偏光板の作成>
前記WVフィルムの透明基材フィルム(本発明の透明保護フィルム2に相当)側を、ケン化処理した後、そのケン化処理面に、上記接着剤2を乾燥後の接着剤層の厚みが80nmとなるように塗布したものを用意した。また、上記透明保護フィルム1の片面に、上記接着剤2を乾燥後の接着剤層の厚みが80nmとなるように塗布したもの用意した。接着剤の塗布は、その調製から30分間後に23℃の温度条件下で行なった。次いで、23℃の温度条件下で偏光子の両面に、前記接着剤付きの透明保護フィルム(WVフィルムおよび透明保護フィルム1)をロール機で貼り合せた後、55℃で6分間乾燥して偏光板を作成した。
実施例1において、偏光板の作成にあたり、透明保護フィルムの種類、接着剤の種類を表1に示すように変えたこと以外は実施例1と同様にして作成した。
得られた偏光板について下記評価を行った。結果を表1に示す。
偏光板を、偏光子の吸収軸が長辺に対して45°となり、17インチモニターに合致するように切り出した。当該偏光板の積層フィルム面(液晶光学補償層側)にアクリル系粘着剤層を貼り付けた。この粘着剤層付きの偏光板を、TN型液晶セルの両面に、偏光板(偏光子)の吸収軸が直交するように貼り付けたものをサンプル(液晶パネル)とした。サンプルについて、加熱試験(80℃,24時間)、加湿試験(60℃,90%RH,24時間)を行った。試験後、目視での観察および輝度を測定した。
輝度は、図3に示す、(1)乃至(9)の箇所について測定し、下記式により面内均一性を評価した。
面内均一性(輝度:cd/cm2)=((2)+(4)+(6)+(8))/4−((1)+(3)+(5)+(7)+(9))/5
偏光板の端部において、偏光子と透明保護フィルムとの間にカッターの刃先を挿入した。当該挿入部において、偏光子と透明保護フィルムとを掴み、それぞれ反対方向に引っ張った。このとき、偏光子および/または透明保護フィルムが破断して剥離できなかった場合は、密着性が良好:「○」と判断した。一方、偏光子と透明保護フィルムとの間で一部または全部は剥離した場合は、密着性に乏しい:「×」と判断した。
偏光板を、偏光子の吸収軸方向に50mm、吸収軸に直交する方向に25mmになるように切り出してサンプルを調製した。当該サンプルを、60℃の温水に浸漬し、時間経過とともにサンプルの端部の剥がれ量(mm)を測定した。剥がれ量(mm)の測定は、ノギスにより行なった。5時間経過後の剥がれ量(mm)を表1に示す。
偏光板を1000mm×1000mmになるように切り出してサンプルを調製した。サンプルの偏光板を、蛍光灯下に置いた。サンプルの偏光板の光源側に別の偏光板を、それぞれの吸収軸が直行するように設置し、この状態で、光抜けする箇所(クニック欠陥)の個数をカウントした。
11 偏光子
12、12’ 接着剤層
13 積層フィルム
A、B 透明保護フィルム
D 液晶光学補償層
20 液晶セル
Claims (8)
- 偏光子の片面に、接着剤層、透明保護フィルムAおよび液晶光学補償層をこの順で有し、他の片面に接着剤層、透明保護フィルムBをこの順で有する偏光板であって、
前記液晶光学補償層は、液晶の光軸を傾斜配向させて得られる液晶光学補償層であり、かつ、
前記透明保護フィルムAおよび透明保護フィルムBのいずれか少なくとも一方は、ラクトン環構造を有する(メタ)アクリル系樹脂を含有することを特徴とする偏光板。 - 前記接着剤層は、ポリビニルアルコール系樹脂、架橋剤および平均粒子径が1〜100nmの金属化合物コロイドを含有してなる樹脂溶液であって、かつ、
金属化合物コロイドは、ポリビニルアルコール系樹脂100重量部に対して、200重量部以下の割合で配合されている偏光板用接着剤から形成されたものであることを特徴とする請求項1記載の偏光板。 - 金属化合物コロイドが、アルミナコロイド、シリカコロイド、ジルコニアコロイド、チタニアコロイドおよび酸化スズコロイドから選ばれるいずれか少なくとも1種であることを特徴とする請求項2記載の偏光板。
- 金属化合物コロイドが、正電荷を有することを特徴とする請求項2または3記載の偏光板。
- 金属化合物コロイドが、アルミナコロイドであることを特徴とする請求項4記載の偏光板。
- 前記液晶光学補償層が、ディスコティック液晶層であることを特徴とする請求項1〜5のいずれかに記載の偏光板。
- 請求項1〜6のいずれかに記載の偏光板が、少なくとも1枚積層されていることを特徴とする光学フィルム。
- 請求項1〜6のいずれかに記載の偏光板または請求項7記載の光学フィルムが用いられていることを特徴とする画像表示装置。
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