JP2009102309A5 - - Google Patents

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Publication number
JP2009102309A5
JP2009102309A5 JP2008249197A JP2008249197A JP2009102309A5 JP 2009102309 A5 JP2009102309 A5 JP 2009102309A5 JP 2008249197 A JP2008249197 A JP 2008249197A JP 2008249197 A JP2008249197 A JP 2008249197A JP 2009102309 A5 JP2009102309 A5 JP 2009102309A5
Authority
JP
Japan
Prior art keywords
monomethylhydrazine
methylation
reaction mixture
low
hydrazinium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP2008249197A
Other languages
English (en)
Japanese (ja)
Other versions
JP5322564B2 (ja
JP2009102309A (ja
Filing date
Publication date
Priority claimed from DE102007046467A external-priority patent/DE102007046467A1/de
Application filed filed Critical
Publication of JP2009102309A publication Critical patent/JP2009102309A/ja
Publication of JP2009102309A5 publication Critical patent/JP2009102309A5/ja
Application granted granted Critical
Publication of JP5322564B2 publication Critical patent/JP5322564B2/ja
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

JP2008249197A 2007-09-28 2008-09-26 モノメチルヒドラジンの製造方法 Expired - Fee Related JP5322564B2 (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102007046467.5 2007-09-28
DE102007046467A DE102007046467A1 (de) 2007-09-28 2007-09-28 Verfahren zur Herstellung von Monomethylhydrazin

Publications (3)

Publication Number Publication Date
JP2009102309A JP2009102309A (ja) 2009-05-14
JP2009102309A5 true JP2009102309A5 (enExample) 2011-09-29
JP5322564B2 JP5322564B2 (ja) 2013-10-23

Family

ID=40263014

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2008249197A Expired - Fee Related JP5322564B2 (ja) 2007-09-28 2008-09-26 モノメチルヒドラジンの製造方法

Country Status (6)

Country Link
US (1) US7683217B2 (enExample)
EP (1) EP2042483B1 (enExample)
JP (1) JP5322564B2 (enExample)
CN (1) CN101397264B (enExample)
DE (1) DE102007046467A1 (enExample)
ES (1) ES2432575T3 (enExample)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SE426607B (sv) 1982-03-29 1983-01-31 Kamyr Ab Sett att behandla en massasuspension som er i rorelse lengs en bana medelst fortrengning av massans suspensionsvetska med en eller flera ersettningsvetskor
CN104151190B (zh) * 2014-08-07 2016-01-20 山东汇海医药化工有限公司 一种从甲基氨基硫脲合成母液中回收甲基肼的方法
CN104628595B (zh) * 2015-02-03 2017-05-17 西安近代化学研究所 一种42％甲基肼水溶液的制备方法
CN104628594B (zh) * 2015-02-03 2017-04-12 西安近代化学研究所 一种高纯度甲基肼的制备方法
CN105037196B (zh) * 2015-08-10 2017-03-29 济南大学 一种常压下催化合成甲基肼的新方法
CN109180522B (zh) * 2018-09-28 2021-01-29 吉林化工学院 一种去除叔丁基肼盐酸盐中盐酸肼的工艺
CN110590595A (zh) * 2019-09-26 2019-12-20 河北合佳医药科技集团股份有限公司 一种绿色高效的甲基肼粗品溶液精馏方法
CN111320554A (zh) * 2019-12-11 2020-06-23 东力（南通）化工有限公司 一种一甲基肼生产工艺改进技术
CN114133339A (zh) * 2021-11-12 2022-03-04 东力（南通）化工有限公司 一种甲基肼连续流微通道烷基化方法
CN114292208B (zh) * 2021-12-27 2023-11-28 杭州新本立医药有限公司 一种固体酸催化制备甲基肼的方法
CN117384063B (zh) * 2023-08-29 2025-11-07 东力（南通）化工有限公司 一种三甲基肼的合成工艺及产品
CN117160060B (zh) * 2023-08-30 2025-10-31 湖北三峰透平装备股份有限公司 一种甲基联氨联合制备装置及制备方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2954283A (en) 1957-12-02 1960-09-27 Nat Distillers Chem Corp Fuel mixtures
FR1260474A (fr) * 1960-06-22 1961-05-05 Olin Mathieson Production de monométhylhydrazine anhydre par distillation extractive
US3423464A (en) * 1966-08-25 1969-01-21 Olin Mathieson Process for the manufacture of monomethylhydrazine
JPS5399099A (en) * 1977-02-09 1978-08-30 Osuboogu Hansu Method of making hydrazine
JPS5615257A (en) * 1979-07-17 1981-02-14 Nippon Hidorajin Kogyo Kk Preparation of methylhydrazine
JPS5829296B2 (ja) * 1980-12-10 1983-06-22 日本ヒドラジン工業株式会社 モノメチルヒドラジンの製造方法
JPH0239502B2 (ja) 1982-03-15 1990-09-05 Nippon Hydrogene Kogyo Monomechiruhidorajinnokaishuhoho
JPS60237059A (ja) 1984-05-09 1985-11-25 Nippon Carbide Ind Co Ltd モノアルキルヒドラジンの製法

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