JP2008516951A - 一成分自己エッチング接着材 - Google Patents
一成分自己エッチング接着材 Download PDFInfo
- Publication number
- JP2008516951A JP2008516951A JP2007536738A JP2007536738A JP2008516951A JP 2008516951 A JP2008516951 A JP 2008516951A JP 2007536738 A JP2007536738 A JP 2007536738A JP 2007536738 A JP2007536738 A JP 2007536738A JP 2008516951 A JP2008516951 A JP 2008516951A
- Authority
- JP
- Japan
- Prior art keywords
- adhesive
- etching
- self
- sea
- performance
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000853 adhesive Substances 0.000 title claims abstract description 31
- 230000001070 adhesive effect Effects 0.000 title claims abstract description 31
- 238000005530 etching Methods 0.000 title claims abstract description 31
- 239000000178 monomer Substances 0.000 claims abstract description 10
- 239000003479 dental cement Substances 0.000 claims abstract description 8
- 230000002378 acidificating effect Effects 0.000 claims abstract description 5
- 230000001588 bifunctional effect Effects 0.000 claims abstract description 5
- 239000002253 acid Substances 0.000 abstract description 12
- 230000037452 priming Effects 0.000 abstract description 4
- 238000004132 cross linking Methods 0.000 abstract description 3
- 238000002203 pretreatment Methods 0.000 abstract description 3
- 239000000203 mixture Substances 0.000 description 12
- 238000001723 curing Methods 0.000 description 10
- 238000000034 method Methods 0.000 description 8
- 239000002131 composite material Substances 0.000 description 6
- 210000004268 dentin Anatomy 0.000 description 6
- 210000003298 dental enamel Anatomy 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 239000003795 chemical substances by application Substances 0.000 description 4
- 238000009472 formulation Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 238000004806 packaging method and process Methods 0.000 description 4
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 3
- 239000012190 activator Substances 0.000 description 3
- JYMNQRQQBJIMCV-UHFFFAOYSA-N 4-(dimethylamino)benzonitrile Chemical compound CN(C)C1=CC=C(C#N)C=C1 JYMNQRQQBJIMCV-UHFFFAOYSA-N 0.000 description 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 241000183024 Populus tremula Species 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 230000002860 competitive effect Effects 0.000 description 2
- 238000006731 degradation reaction Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- FZUGPQWGEGAKET-UHFFFAOYSA-N parbenate Chemical compound CCOC(=O)C1=CC=C(N(C)C)C=C1 FZUGPQWGEGAKET-UHFFFAOYSA-N 0.000 description 2
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 150000004982 aromatic amines Chemical class 0.000 description 1
- 159000000007 calcium salts Chemical class 0.000 description 1
- 239000002521 compomer Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 208000002925 dental caries Diseases 0.000 description 1
- 239000011350 dental composite resin Substances 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 238000000338 in vitro Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 238000000016 photochemical curing Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000002504 physiological saline solution Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229910052573 porcelain Inorganic materials 0.000 description 1
- 239000003829 resin cement Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 230000002459 sustained effect Effects 0.000 description 1
- 238000005382 thermal cycling Methods 0.000 description 1
- 230000008646 thermal stress Effects 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- 239000002966 varnish Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K6/00—Preparations for dentistry
- A61K6/30—Compositions for temporarily or permanently fixing teeth or palates, e.g. primers for dental adhesives
Landscapes
- Health & Medical Sciences (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Epidemiology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Dental Preparations (AREA)
- Liquid Developers In Electrophotography (AREA)
- Developing Agents For Electrophotography (AREA)
- Reinforced Plastic Materials (AREA)
Abstract
Description
ボトル入りおよび単位付与量パッケージ入りの真の一成分自己エッチング接着材
施用前の混合またはリンス不要
1回塗り/1工程、簡単かつ健全な技法
VLC直接接着強度はXeno IIIおよび他の2成分競合品と同等またはそれ以上
間接接着強度(別々のSCA成分と共に使用した場合)はP&B NT/SCA Dual Cure接着材の強度と同等
薄いフィルム(<15μm)
フッ化物放出性
微小な漏洩、少なくとも現用のP&B NTの系およびXeno IIIの系と同様に良好
競合製品との比較
1P−SEAおよび他の歯科用接着材について、熱サイクル前後のIn Vitroのせん断接着強度を試験した。データは、表2、3、4および7に示す。7種類の歯科用接着材を選択した。1P−SEA(Dentsply)、Xeno III(Dentsply)、Prime & Bond NT(P&B NT、Dentsply)、Prompt L−Pop(L−Pop、3M ESPE)、ClearFil SE Bond(SE、クラレ)、One−up Bond F(OBF、Tokuyama)、i−Bond(1B、Heraeus Kulzer)。
SEAのための最低限の設計仕様は、現在Prime & Bond(登録商標)NTに使用されているシステムに類似の単位付与量パッケージフォーマットを必要とする。Dentsply Internationalは、米国特許第6372816号でこのシステム(パッケージ)の特許を取得している(Waltzら、2002年4月16日現在)。包装に対する理想的な要件は、「一体式ブラシ単位付与量」(IB単位付与量)と規定される。2003年9月23日出願のPiersonらの米国特許出願第10/668946号は、IB単位付与量包装に関してケース番号LDC−922−Eで提出されている。
Claims (3)
- 加水分解安定性で酸性の高強度接着材モノマーおよび安定で二官能性の親水性モノマーを含む単一要素自己エッチング歯科用接着材。
- 前記酸性モノマーがPENTAである、請求項1に記載の接着材。
- 前記二官能性の親水性モノマーがAHPMAである、請求項1に記載の接着材。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US61864904P | 2004-10-14 | 2004-10-14 | |
US60/618,649 | 2004-10-14 | ||
PCT/US2005/035991 WO2006044223A1 (en) | 2004-10-14 | 2005-10-06 | One-component self-etching adhesive |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2008516951A true JP2008516951A (ja) | 2008-05-22 |
JP5128950B2 JP5128950B2 (ja) | 2013-01-23 |
Family
ID=35708409
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2007536738A Active JP5128950B2 (ja) | 2004-10-14 | 2005-10-06 | 一成分自己エッチング接着材 |
Country Status (7)
Country | Link |
---|---|
US (2) | US20090043009A1 (ja) |
EP (2) | EP1799180B8 (ja) |
JP (1) | JP5128950B2 (ja) |
AT (1) | ATE429894T1 (ja) |
CA (1) | CA2584070C (ja) |
DE (1) | DE602005014253D1 (ja) |
WO (1) | WO2006044223A1 (ja) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20040229973A1 (en) | 2003-05-13 | 2004-11-18 | Junjie Sang | Dental adhesive compositions and methods |
ATE429894T1 (de) | 2004-10-14 | 2009-05-15 | Dentsply Int Inc | Aus nur einer komponente bestehendes selbstätzendes haftmittel |
WO2018181707A1 (ja) | 2017-03-31 | 2018-10-04 | 三井化学株式会社 | 歯科材料用接着性モノマー |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH09227324A (ja) * | 1995-11-30 | 1997-09-02 | Heraeus Kulzer Gmbh | 歯科用接着剤 |
JPH11322526A (ja) * | 1998-03-27 | 1999-11-24 | Dentsply Detrey Gmbh | 自己硬化性歯科用接着剤 |
WO2004100900A1 (en) * | 2003-05-13 | 2004-11-25 | Dentsply International Inc. | Dental adhesive compositions and methods |
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CH632667A5 (de) * | 1978-01-03 | 1982-10-29 | Espe Pharm Praep | Opakes, durch uv-licht polymerisierbares zahnfuellmaterial. |
US4389497A (en) * | 1979-11-22 | 1983-06-21 | Espe Fabrik Parmazeutischer Praparate Gmbh | Use of agglomerates of silicic acid as fillers in dental materials |
IE54502B1 (en) * | 1982-03-04 | 1989-10-25 | Ici Plc | Photopolymerisable compositions |
US4674980A (en) * | 1982-05-03 | 1987-06-23 | Den-Mat, Inc. | Dental composite and porcelain repair |
DE3300321A1 (de) | 1983-01-07 | 1984-07-12 | Ernst Mühlbauer KG, 2000 Hamburg | Verfahren zur herstellung oberflaechenverkleinerter kieselgele und deren verwendung als fuellstoff fuer dentalmassen |
DE3342601C1 (de) * | 1983-11-25 | 1985-03-14 | Blendax-Werke R. Schneider Gmbh & Co, 6500 Mainz | Verwendung von bromierten aromatischen Diacrylsaeure- bzw. Dimethacrylsaeureestern in dentalen Fuellungsmaterialien |
US4544359A (en) * | 1984-01-13 | 1985-10-01 | Pentron Corporation | Dental restorative material |
JPS60197609A (ja) | 1984-03-16 | 1985-10-07 | Kuraray Co Ltd | 歯科用組成物 |
DE3414164A1 (de) * | 1984-04-14 | 1985-10-17 | Kulzer & Co GmbH, 6393 Wehrheim | Photopolymerisierbarer dentaler haftvermittler-lack |
DE3414163A1 (de) * | 1984-04-14 | 1985-10-17 | Kulzer & Co GmbH, 6393 Wehrheim | Photopolymerisierbarer phosphathaltiger dentaler haftvermittler-lack |
US4503169A (en) * | 1984-04-19 | 1985-03-05 | Minnesota Mining And Manufacturing Company | Radiopaque, low visual opacity dental composites containing non-vitreous microparticles |
DE3430801A1 (de) * | 1984-08-22 | 1986-03-06 | Bayer Ag, 5090 Leverkusen | Verwendung von poroesen fuellstoffen in polymerisierbaren massen, solche massen und deren verwendung zur herstellung von formkoerpern |
US4966934A (en) * | 1984-11-29 | 1990-10-30 | Dentsply Research & Development Corp. | Biological compatible adhesive containing a phosphorous adhesion promoter and accelerator |
US4721735A (en) * | 1986-01-23 | 1988-01-26 | Dentsply Research And Development Corporation | Frangible light cured compositions |
DE3609038A1 (de) * | 1986-03-18 | 1987-09-24 | Espe Stiftung | Roentgenopake polymerisierbare dentalmassen |
JPH0653647B2 (ja) * | 1986-04-18 | 1994-07-20 | 而至歯科工業株式会社 | 歯科修復用組成物 |
US5033650A (en) * | 1987-03-09 | 1991-07-23 | Laurence Colin | Multiple barrel dispensing device |
US4746686A (en) * | 1987-04-17 | 1988-05-24 | Kerr Manufacturing Company | Visible light activated cavity liner |
US4959297A (en) * | 1987-12-09 | 1990-09-25 | Minnesota Mining And Manufacturing Company | Ternary photoinitiator system for addition polymerization |
IT1234978B (it) * | 1988-06-01 | 1992-06-09 | Tecres Spa | Miscela cementifera a due fasi, particolarmente adatta per usi ortopedici. |
JPH0667812B2 (ja) | 1988-07-13 | 1994-08-31 | 株式会社クラレ | 歯科用接着性組成物 |
EP0363903A3 (en) * | 1988-10-14 | 1991-03-20 | Dentsply International | Adhesive containing pit and fissure sealants |
DE3932989A1 (de) | 1989-10-03 | 1991-04-11 | Espe Stiftung | Polyalkylenoxidderivate enthaltende polyetherabformmassen |
JP2634276B2 (ja) | 1990-02-15 | 1997-07-23 | 株式会社松風 | プライマー組成物 |
US5525648A (en) * | 1991-12-31 | 1996-06-11 | Minnesota Mining And Manufacturing Company | Method for adhering to hard tissue |
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JP4305594B2 (ja) * | 2000-11-28 | 2009-07-29 | 株式会社トクヤマ | 歯科用接着キット |
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JP2004105351A (ja) | 2002-09-17 | 2004-04-08 | Dentsply Sankin Kk | 光硬化性歯科用接着組成物 |
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ATE429894T1 (de) | 2004-10-14 | 2009-05-15 | Dentsply Int Inc | Aus nur einer komponente bestehendes selbstätzendes haftmittel |
-
2005
- 2005-10-06 AT AT05808891T patent/ATE429894T1/de not_active IP Right Cessation
- 2005-10-06 CA CA2584070A patent/CA2584070C/en active Active
- 2005-10-06 EP EP05808891A patent/EP1799180B8/en active Active
- 2005-10-06 JP JP2007536738A patent/JP5128950B2/ja active Active
- 2005-10-06 EP EP09001527.2A patent/EP2062561B1/en active Active
- 2005-10-06 WO PCT/US2005/035991 patent/WO2006044223A1/en active Application Filing
- 2005-10-06 DE DE602005014253T patent/DE602005014253D1/de active Active
-
2008
- 2008-09-25 US US12/284,854 patent/US20090043009A1/en not_active Abandoned
-
2009
- 2009-11-30 US US12/592,603 patent/US8466211B2/en active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH09227324A (ja) * | 1995-11-30 | 1997-09-02 | Heraeus Kulzer Gmbh | 歯科用接着剤 |
JPH11322526A (ja) * | 1998-03-27 | 1999-11-24 | Dentsply Detrey Gmbh | 自己硬化性歯科用接着剤 |
WO2004100900A1 (en) * | 2003-05-13 | 2004-11-25 | Dentsply International Inc. | Dental adhesive compositions and methods |
Also Published As
Publication number | Publication date |
---|---|
EP2062561A2 (en) | 2009-05-27 |
JP5128950B2 (ja) | 2013-01-23 |
CA2584070A1 (en) | 2006-04-27 |
EP1799180B8 (en) | 2010-01-06 |
EP2062561A3 (en) | 2014-07-23 |
EP2062561B1 (en) | 2016-06-15 |
CA2584070C (en) | 2012-12-18 |
US20090043009A1 (en) | 2009-02-12 |
US20120172488A1 (en) | 2012-07-05 |
US8466211B2 (en) | 2013-06-18 |
DE602005014253D1 (de) | 2009-06-10 |
EP1799180A1 (en) | 2007-06-27 |
EP1799180B1 (en) | 2009-04-29 |
WO2006044223A1 (en) | 2006-04-27 |
ATE429894T1 (de) | 2009-05-15 |
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At | of Dental Sciences |
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