JP2007514259A - 標識ポリマーの認証方法 - Google Patents
標識ポリマーの認証方法 Download PDFInfo
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- JP2007514259A JP2007514259A JP2006541264A JP2006541264A JP2007514259A JP 2007514259 A JP2007514259 A JP 2007514259A JP 2006541264 A JP2006541264 A JP 2006541264A JP 2006541264 A JP2006541264 A JP 2006541264A JP 2007514259 A JP2007514259 A JP 2007514259A
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Abstract
【選択図】 図3
Description
次に、例示的であって限定的ではない図面について説明する。
開示された方法に従って製造した、法的認証マーカー及び動的応答認証マーカーを共に含むマルチレベル標識系を有する例示的なポリカーボネート組成物を表1に示す。この特定の実施例では、17700単位の平均分子量を有する光学品質のポリカーボネートを基材樹脂として使用し、さらに、ジメチルビスフェノールシクロヘキサン(DMBPC)及びビスフェノールAに基づくポリカーボネートからなるGeneral Electric社の特許コポリマーを、法的認証マーカーを含む化合物として使用する。電磁スペクトルの緑色領域で発光するUV励起可能なロングストークスシフト蛍光物質をHoneywell社(ゼールツェ、ドイツ)から入手し、動的応答認証マーカーとして使用した。
30mm二軸押出機を用いて、配合物A及びBを290℃の溶融温度で押し出した。次いで、ペレットから0.6mm及び1.2mmの段階厚さを有する色プラークを成形した。2種の配合物の流れ挙動を比較するため、剪断粘度対剪断速度曲線を作成した。すべての流動学的データは毛管レオメーターを用いて300℃で測定し、剪断速度に対して剪断粘度を示すグラフとして表す(図1)。2種の材料の粘度は重なり合い、剪断減粘は同じ剪断速度で開始するが、これは法的認証マーカー及び動的応答認証マーカーの添加がポリカーボネートの材料特性に影響を及ぼさないことを表している。同じ結論は、2種の配合物の溶融流れが約7%未満しか違わないという事実からも引き出すことができる。即ち、250℃での配合物Aのメルト・ボリューム・レート(ASTM D1238)は9.72g/10分である一方、250℃での配合物Bのメルト・ボリューム・レート(ASTM D1238)は10.39g/10分であり、これは有意差に該当しない。
開示された方法に従って法的認証マーカーを確認した結果を図2に示す。溶液状態プロトン核磁気共鳴(NMR)分光法を用いて、配合物Bの法的認証マーカー(即ち、DMBPCコポリマー)の種類及び量を測定した。ペレット試料を約1.5mlの重水素化クロロホルム(純度99%)中に溶解し、次いでVarian Mercury−400分光計で分析した。
開示された方法に従って動的応答認証マーカーを確認した結果を図3に示す。小形レーザー光源(Nanolase社、フランス、355nm発光波長)及びポータブル分光蛍光計(Ocean Optics,Inc.、ダニーディン、米国フロリダ州、モデルST2000)を含む装置を用いて、UV蛍光物質の蛍光発光スペクトルを測定した。分光蛍光計には、200μmのスリット、400nmのブレーズ波長を有すると共に30%を超える効率で250〜800nmのスペクトル範囲をカバーする600本/mmの回折格子、及び線形CCDアレイ検出器が備わっていた。レーザーからの光は、「シックス・アラウンド・ワン」二分岐型光ファイバー反射プローブ(Ocean Optics,Inc.、モデルR400−7−UV/VIS)の一方のアームに集束させた。試料からプローブに直接反射される光の量を最小限に抑えるため、光ファイバープローブの共通端を一定の角度で試料の近くに配置した場合に試料からの発光が捕集された。プローブの第二のアームは分光蛍光計に結合した。図3は、配合物Aの平坦なスペクトルに対し、配合物B中に混入されたロングストークスシフトUV蛍光物質の蛍光発光を明確に示している。
表2から、2種の配合物が互いに2.5ΔE単位の範囲内にあることがわかり、これはD65光源及び10°観測者の下で有意な視覚差は存在しないことを表している。650nm及び780nm(CD及びDVDプレイヤーで使用される主レーザ波長)での%透過率の値も、法的認証マーカーを含む化合物及び動的応答認証マーカー(c)の添加による影響を受けない。実際、蛍光物質の添加は、図4a及び4bに示すように吸収/透過スペクトルの(450nmまでの)UV領域のみに影響を及ぼす。
Claims (13)
- 標識ポリマーが基板ポリマー、法的認証マーカーを含む化合物、及び動的応答認証マーカーを含み、前記法的認証マーカーが法的分析技術で検出するのに十分な量で標識ポリマー中に存在し、前記動的応答認証マーカーが動的応答分析技術で検出するのに十分な量で存在する場合において、試験ポリマーが標識ポリマーであることを認証する方法であって、
試験ポリマーが標識ポリマーであることを認証する方法であって、標識ポリマーが基板ポリマー、法的認証マーカーを含む化合物、及び動的応答認証マーカーを含み、前記法的認証マーカーが法的分析技術で検出するのに十分な量で標識ポリマー中に存在し、前記動的応答認証マーカーが動的応答分析技術で検出するのに十分な量で存在する場合において、
法的分析技術を用いて試験ポリマーを法的認証マーカーについて試験し、
動的応答分析技術を用いて試験ポリマーを動的応答認証マーカーについて試験し、
法的認証マーカー及び動的応答認証マーカーが検出されれば試験ポリマーが標識ポリマーであると認証する
ことを含んでなる方法。 - 法的認証マーカーを含む化合物が、基板ポリマーの光学的又は流動学的性質に影響を及ぼさない量で標識ポリマー中に存在する、請求項1記載の方法。
- 法的分析技術がNMRであり、動的応答分析技術がルミネセンス分光法及び蛍光分光法からなる群から選択される、請求項1記載の方法。
- 法的認証マーカーが、標識ポリマーの全重量を基準にして約10重量%以下の量で標識ポリマー中に存在する、請求項1記載の方法。
- 法的認証マーカーが、標識ポリマーの全重量を基準にして0.005重量%以上の量で標識ポリマー中に存在する、請求項1記載の方法。
- 法的認証マーカーが、炭素原子数2以上のアルキル基、炭素原子数3以上の脂環式基、−OCH3基、−CH3Si基、アリール部分に結合したメチル基、二価置換フェノール基、及び末端置換フェノール基の1種以上である、請求項1記載の方法。
- 法的認証マーカーが、−(CH2)n−基(式中、nは4〜14の数である。)からなる群から選択される、請求項6記載の方法。
- 法的認証マーカーが、ポリカーボネートとの混和性を有すると共に、DMBPCコポリマー、DDDAコポリマー、オイゲノールシロキサン−PCコポリマー、ITR−PCコポリマー、ポリ(1,4−シクロヘキサンジメチル−1,4−シクロヘキサンジカルボキシレート)、ポリ(エチレンナフタレート)、ポリ(ブチレンナフタレート)、ポリ(シクロヘキサンジメタノール−コ−エチレンテレフタレート)、及び上述の混和性ポリマーの1種以上を含む組合せからなる群から選択されるポリマー中に存在する、請求項6記載の方法。
- 動的応答認証マーカーが、有機蛍光物質、無機蛍光物質、有機金属蛍光物質、半導体発光ナノ粒子及びこれらの混合物からなる群から選択される1種からなる、請求項1記載の方法。
- 動的応答認証マーカーが、標識ポリマーの全重量を基準にして約10−18〜約2重量%の量で標識ポリマー中に存在する、請求項1記載の方法。
- 試験ポリマーが成形物品であり、情報記憶媒体である、請求項1記載の方法。
- 物品の認証方法であって、
ポリマー及び法的認証マーカーを含む化合物を合体させることで、法的認証マーカーが法的分析技術で検出するのに十分な量で標識ポリマー中に存在するようにして標識ポリマーを製造し、
標識ポリマーから標識物品を形成し、
法的分析技術を用いて法的認証マーカーを検出することで、物品が標識物品であると認証する
ことを含んでなる方法。 - 物品の認証方法であって、
基板ポリマー、法的認証マーカーを含む化合物、及び動的応答認証マーカーを合体させて標識ポリマーを製造し、
前記標識ポリマーから標識物品を形成し、
法的分析技術を用いて法的認証マーカーを検出すると共に、動的応答分析技術を用いて動的応答認証マーカーを検出することで、物品が標識物品であると認証する
ことを含んでなり、前記法的認証マーカーが法的分析技術で検出するのに十分な量で標識ポリマー中に存在し、前記動的応答認証マーカーが動的応答分析技術で検出するのに十分な量で存在する、方法。
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2004
- 2004-11-10 DE DE602004020814T patent/DE602004020814D1/de active Active
- 2004-11-10 JP JP2006541264A patent/JP2007514259A/ja not_active Ceased
- 2004-11-10 WO PCT/US2004/037687 patent/WO2005055236A1/en not_active Application Discontinuation
- 2004-11-10 AT AT04800998T patent/ATE429702T1/de not_active IP Right Cessation
- 2004-11-10 EP EP04800998A patent/EP1820193B1/en not_active Not-in-force
- 2004-11-23 TW TW093135998A patent/TW200526940A/zh unknown
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JP2009300985A (ja) * | 2008-05-13 | 2009-12-24 | Toyobo Co Ltd | 温度時間経歴を表示する製造工程チェックラベル |
JP2009300986A (ja) * | 2008-05-13 | 2009-12-24 | Toyobo Co Ltd | 温度時間経歴を表示する流通履歴表示ラベル |
JP2014502340A (ja) * | 2010-09-21 | 2014-01-30 | ダウ グローバル テクノロジーズ エルエルシー | オンライン分析とトレーサー技術との関連付け法 |
JP2014527621A (ja) * | 2011-07-15 | 2014-10-16 | ハネウェル・インターナショナル・インコーポレーテッド | 発光蛍光体化合物を有する物品を認証するための方法および装置 |
JP2017095724A (ja) * | 2011-11-30 | 2017-06-01 | シクパ ホルディング ソシエテ アノニムSicpa Holding Sa | マーキングされた塗料組成物およびその認証法 |
JP2015505111A (ja) * | 2012-01-17 | 2015-02-16 | ハネウェル・インターナショナル・インコーポレーテッド | サーモグラフィ蛍光体を組み込む物品、ならびにそのような物品を認証するための方法および装置 |
JP2017111119A (ja) * | 2015-11-09 | 2017-06-22 | ザ・ボーイング・カンパニーThe Boeing Company | 接合コンポーネントの構造健全性を監視するシステム及び方法 |
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Also Published As
Publication number | Publication date |
---|---|
US20050112768A1 (en) | 2005-05-26 |
WO2005055236A1 (en) | 2005-06-16 |
ATE429702T1 (de) | 2009-05-15 |
TW200526940A (en) | 2005-08-16 |
EP1820193B1 (en) | 2009-04-22 |
DE602004020814D1 (de) | 2009-06-04 |
EP1820193A1 (en) | 2007-08-22 |
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