JP2006523141A5 - - Google Patents
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- Publication number
- JP2006523141A5 JP2006523141A5 JP2006509713A JP2006509713A JP2006523141A5 JP 2006523141 A5 JP2006523141 A5 JP 2006523141A5 JP 2006509713 A JP2006509713 A JP 2006509713A JP 2006509713 A JP2006509713 A JP 2006509713A JP 2006523141 A5 JP2006523141 A5 JP 2006523141A5
- Authority
- JP
- Japan
- Prior art keywords
- organic base
- reaction product
- nickel
- molar equivalents
- phase
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 150000007530 organic bases Chemical class 0.000 claims 7
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims 6
- 239000007795 chemical reaction product Substances 0.000 claims 6
- 239000003446 ligand Substances 0.000 claims 5
- 239000002904 solvent Substances 0.000 claims 5
- 150000003839 salts Chemical class 0.000 claims 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims 3
- 238000000034 method Methods 0.000 claims 3
- 229910052759 nickel Inorganic materials 0.000 claims 3
- 239000011347 resin Substances 0.000 claims 3
- 229920005989 resin Polymers 0.000 claims 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 2
- 229910021586 Nickel(II) chloride Inorganic materials 0.000 claims 2
- 125000003118 aryl group Chemical group 0.000 claims 2
- 239000003054 catalyst Substances 0.000 claims 2
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims 2
- 238000000622 liquid--liquid extraction Methods 0.000 claims 2
- 239000000203 mixture Substances 0.000 claims 2
- QMMRZOWCJAIUJA-UHFFFAOYSA-L nickel dichloride Chemical compound Cl[Ni]Cl QMMRZOWCJAIUJA-UHFFFAOYSA-L 0.000 claims 2
- 239000007787 solid Substances 0.000 claims 2
- 238000000638 solvent extraction Methods 0.000 claims 2
- FPPLREPCQJZDAQ-UHFFFAOYSA-N 2-methylpentanedinitrile Chemical compound N#CC(C)CCC#N FPPLREPCQJZDAQ-UHFFFAOYSA-N 0.000 claims 1
- 239000002841 Lewis acid Substances 0.000 claims 1
- 229910021536 Zeolite Inorganic materials 0.000 claims 1
- 230000002378 acidificating effect Effects 0.000 claims 1
- -1 acyclic hydrocarbons Chemical class 0.000 claims 1
- BTGRAWJCKBQKAO-UHFFFAOYSA-N adiponitrile Chemical compound N#CCCCCC#N BTGRAWJCKBQKAO-UHFFFAOYSA-N 0.000 claims 1
- 229910000323 aluminium silicate Inorganic materials 0.000 claims 1
- 125000004104 aryloxy group Chemical group 0.000 claims 1
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 125000004122 cyclic group Chemical group 0.000 claims 1
- 238000000605 extraction Methods 0.000 claims 1
- 238000001914 filtration Methods 0.000 claims 1
- 229930195733 hydrocarbon Natural products 0.000 claims 1
- 150000007517 lewis acids Chemical class 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 150000002825 nitriles Chemical class 0.000 claims 1
- FAIAAWCVCHQXDN-UHFFFAOYSA-N phosphorus trichloride Chemical compound ClP(Cl)Cl FAIAAWCVCHQXDN-UHFFFAOYSA-N 0.000 claims 1
- 239000000047 product Substances 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
- 239000010457 zeolite Substances 0.000 claims 1
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/409,482 US6844289B2 (en) | 2003-04-08 | 2003-04-08 | Process for the preparation of a nickel/phosphorous ligand catalyst |
| PCT/US2004/010472 WO2004091780A1 (en) | 2003-04-08 | 2004-04-06 | Process for the preparation of a nickel/phosphorous ligand catalyst |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2006523141A JP2006523141A (ja) | 2006-10-12 |
| JP2006523141A5 true JP2006523141A5 (enExample) | 2007-04-26 |
Family
ID=33130607
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2006509713A Ceased JP2006523141A (ja) | 2003-04-08 | 2004-04-06 | ニッケル/リン配位子触媒の製造方法 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US6844289B2 (enExample) |
| EP (1) | EP1610894B1 (enExample) |
| JP (1) | JP2006523141A (enExample) |
| CN (1) | CN100496725C (enExample) |
| AT (1) | ATE357972T1 (enExample) |
| DE (1) | DE602004005580T2 (enExample) |
| MY (1) | MY138457A (enExample) |
| SA (1) | SA04250241B1 (enExample) |
| TW (1) | TW200500372A (enExample) |
| WO (1) | WO2004091780A1 (enExample) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2849027B1 (fr) * | 2002-12-23 | 2005-01-21 | Rhodia Polyamide Intermediates | Procede de synthese de composes comprenant des fonctions nitriles a partir de composes a insaturations ethyleniques |
| FR2850966B1 (fr) | 2003-02-10 | 2005-03-18 | Rhodia Polyamide Intermediates | Procede de fabrication de composes dinitriles |
| FR2854892B1 (fr) * | 2003-05-12 | 2005-06-24 | Rhodia Polyamide Intermediates | Procede de fabrication de dinitriles |
| FR2854891B1 (fr) | 2003-05-12 | 2006-07-07 | Rhodia Polyamide Intermediates | Procede de preparation de dinitriles |
| DE102004049339A1 (de) * | 2004-10-08 | 2006-04-13 | Basf Ag | Verfahren zur Reinigung von phosphorhaltigen Chelat-Liganden |
| DE102004050935A1 (de) * | 2004-10-18 | 2006-04-20 | Basf Ag | Extraktion von Nickel(0)-Komplexen aus Nitrilgemischen mit verminderter Mulmbildung |
| US7211703B2 (en) * | 2005-04-27 | 2007-05-01 | Calgon Carbon Corporation | Method of separating E and Z isomers of an alkene alcohol and derivatives thereof |
| WO2007109005A2 (en) * | 2006-03-17 | 2007-09-27 | Invista Technologies S.A R.L. | Method for the purification of triorganophosphites by treatment with a basic additive |
| US7709674B2 (en) * | 2006-07-14 | 2010-05-04 | Invista North America S.A R.L | Hydrocyanation process with reduced yield losses |
| SG175182A1 (en) | 2009-04-21 | 2011-11-28 | Invista Tech Sarl | Highly selective process for producing organodiphosphites |
| CN102380353B (zh) * | 2011-09-19 | 2013-08-21 | 江苏大学 | 一种磁性氧化镁表面分子印迹固相萃取剂的制备方法 |
| WO2013076569A1 (en) | 2011-10-26 | 2013-05-30 | Invista Technologies S.A R.L. | Methods for producing organodi phosphites from phosphorochloridites characterized by measuring side- product levels to determine further additions |
| US9011691B2 (en) * | 2011-12-21 | 2015-04-21 | Invista North America S.A.R.L. | Extraction solvent control for reducing stable emulsions |
| CN103547349B (zh) * | 2011-12-21 | 2016-03-16 | 因温斯特北美公司 | 用于减少稳定乳液的萃取溶剂控制 |
| TWI709566B (zh) * | 2015-09-30 | 2020-11-11 | 美商陶氏科技投資公司 | 用於製造有機磷化合物的方法 |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3846461A (en) * | 1972-10-25 | 1974-11-05 | Du Pont | Process of preparing a zerovalent nickel complex with organic phosphorus compounds |
| US3903120A (en) * | 1973-06-19 | 1975-09-02 | Du Pont | Preparation of zerovalent nickel complexes from elemental nickel |
| US5747339A (en) * | 1990-06-25 | 1998-05-05 | Research Foundation For Microbial Diseases Of Osaka | Non-A, non-B hepatitis virus genomic CDNA and antigen polypeptide |
| DK0730574T3 (da) * | 1993-11-23 | 1999-05-25 | Du Pont | Fremgangsmåder og katalysatorsammensætninger til hydrocyanering af monoolefiner |
| EP0755302B1 (en) * | 1994-04-14 | 2000-10-04 | E.I. Du Pont De Nemours And Company | Bidentate phosphite and nickel catalyst compositions for hydrocyanation of monoolefins |
| US5512695A (en) * | 1994-04-14 | 1996-04-30 | E. I. Du Pont De Nemours And Company | Bidentate phosphite and nickel catalyst compositions for hydrocyanation of monoolefins |
| US5512696A (en) * | 1995-07-21 | 1996-04-30 | E. I. Du Pont De Nemours And Company | Hydrocyanation process and multidentate phosphite and nickel catalyst composition therefor |
| TW315370B (enExample) * | 1994-10-07 | 1997-09-11 | Du Pont | |
| US5523453A (en) * | 1995-03-22 | 1996-06-04 | E. I. Du Pont De Nemours And Company | Process for hydrocyanation |
| US5693843A (en) * | 1995-12-22 | 1997-12-02 | E. I. Du Pont De Nemours And Company | Process for hydrocyanation of diolefins and isomerization of nonconjugated 2 alkyl-3-monoalkenenitriles |
| ZA986374B (en) * | 1997-07-29 | 2000-01-17 | Du Pont | Hydrocyanation of diolefins and isomerization of nonconjugated 2-alkyl-3-monoalkenenitriles. |
| MY124170A (en) * | 1997-07-29 | 2006-06-30 | Invista Tech Sarl | Hydrocyanation processes and multidentate phosphite ligand and nickel catalyst compositions therefor |
| US5959135A (en) * | 1997-07-29 | 1999-09-28 | E. I. Du Pont De Nemours And Company | Hydrocyanation processes and multidentate phosphite ligand and nickel catalyst compositions thereof |
| US6031120A (en) * | 1997-07-29 | 2000-02-29 | E. I. Du Pont De Nemours And Company | Selective synthesis of organodiphosphite compounds |
| ZA986369B (en) * | 1997-07-29 | 2000-01-17 | Du Pont | Hydrocyanation of diolefins and isomerization of nonconjugated 2-alkyl-3-monoalkenenitriles. |
| US6307107B1 (en) * | 1999-09-20 | 2001-10-23 | E.I. Du Pont De Nemours And Company | Hydroformylation of acyclic monoethylenically unsaturated compounds to corresponding terminal aldehydes |
| US6660876B2 (en) * | 2001-11-26 | 2003-12-09 | E. I. Du Pont De Nemours And Company | Phosphorus-containing compositions and their use in hydrocyanation, isomerization and hydroformylation reactions |
-
2003
- 2003-04-08 US US10/409,482 patent/US6844289B2/en not_active Expired - Lifetime
-
2004
- 2004-04-06 EP EP04759127A patent/EP1610894B1/en not_active Expired - Lifetime
- 2004-04-06 DE DE602004005580T patent/DE602004005580T2/de not_active Expired - Lifetime
- 2004-04-06 CN CNB2004800157318A patent/CN100496725C/zh not_active Expired - Lifetime
- 2004-04-06 JP JP2006509713A patent/JP2006523141A/ja not_active Ceased
- 2004-04-06 WO PCT/US2004/010472 patent/WO2004091780A1/en not_active Ceased
- 2004-04-06 AT AT04759127T patent/ATE357972T1/de not_active IP Right Cessation
- 2004-04-07 MY MYPI20041274A patent/MY138457A/en unknown
- 2004-04-08 TW TW093109795A patent/TW200500372A/zh unknown
- 2004-08-04 SA SA4250241A patent/SA04250241B1/ar unknown
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