CN100496725C - 用于制备镍/亚磷配体催化剂的方法 - Google Patents

用于制备镍/亚磷配体催化剂的方法 Download PDF

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Publication number
CN100496725C
CN100496725C CNB2004800157318A CN200480015731A CN100496725C CN 100496725 C CN100496725 C CN 100496725C CN B2004800157318 A CNB2004800157318 A CN B2004800157318A CN 200480015731 A CN200480015731 A CN 200480015731A CN 100496725 C CN100496725 C CN 100496725C
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CN
China
Prior art keywords
ligand
alkyl
nickel
vial
solution
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Expired - Lifetime
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CNB2004800157318A
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English (en)
Chinese (zh)
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CN1802213A (zh
Inventor
S·C·杰克逊
R·J·麦金尼
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INVISTA TECHNOLOGIES Sarl
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INVISTA TECHNOLOGIES Sarl
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/18—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms
    • B01J31/1845—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms the ligands containing phosphorus
    • B01J31/185—Phosphites ((RO)3P), their isomeric phosphonates (R(RO)2P=O) and RO-substitution derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/06—Phosphorus compounds without P—C bonds
    • C07F9/08—Esters of oxyacids of phosphorus
    • C07F9/141—Esters of phosphorous acids
    • C07F9/145—Esters of phosphorous acids with hydroxyaryl compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/30—Addition reactions at carbon centres, i.e. to either C-C or C-X multiple bonds
    • B01J2231/32—Addition reactions to C=C or C-C triple bonds
    • B01J2231/323—Hydrometalation, e.g. bor-, alumin-, silyl-, zirconation or analoguous reactions like carbometalation, hydrocarbation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/84—Metals of the iron group
    • B01J2531/847—Nickel

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CNB2004800157318A 2003-04-08 2004-04-06 用于制备镍/亚磷配体催化剂的方法 Expired - Lifetime CN100496725C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US10/409,482 US6844289B2 (en) 2003-04-08 2003-04-08 Process for the preparation of a nickel/phosphorous ligand catalyst
US10/409,482 2003-04-08

Publications (2)

Publication Number Publication Date
CN1802213A CN1802213A (zh) 2006-07-12
CN100496725C true CN100496725C (zh) 2009-06-10

Family

ID=33130607

Family Applications (1)

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CNB2004800157318A Expired - Lifetime CN100496725C (zh) 2003-04-08 2004-04-06 用于制备镍/亚磷配体催化剂的方法

Country Status (10)

Country Link
US (1) US6844289B2 (enExample)
EP (1) EP1610894B1 (enExample)
JP (1) JP2006523141A (enExample)
CN (1) CN100496725C (enExample)
AT (1) ATE357972T1 (enExample)
DE (1) DE602004005580T2 (enExample)
MY (1) MY138457A (enExample)
SA (1) SA04250241B1 (enExample)
TW (1) TW200500372A (enExample)
WO (1) WO2004091780A1 (enExample)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2849027B1 (fr) * 2002-12-23 2005-01-21 Rhodia Polyamide Intermediates Procede de synthese de composes comprenant des fonctions nitriles a partir de composes a insaturations ethyleniques
FR2850966B1 (fr) 2003-02-10 2005-03-18 Rhodia Polyamide Intermediates Procede de fabrication de composes dinitriles
FR2854892B1 (fr) * 2003-05-12 2005-06-24 Rhodia Polyamide Intermediates Procede de fabrication de dinitriles
FR2854891B1 (fr) 2003-05-12 2006-07-07 Rhodia Polyamide Intermediates Procede de preparation de dinitriles
DE102004049339A1 (de) * 2004-10-08 2006-04-13 Basf Ag Verfahren zur Reinigung von phosphorhaltigen Chelat-Liganden
DE102004050935A1 (de) * 2004-10-18 2006-04-20 Basf Ag Extraktion von Nickel(0)-Komplexen aus Nitrilgemischen mit verminderter Mulmbildung
US7211703B2 (en) * 2005-04-27 2007-05-01 Calgon Carbon Corporation Method of separating E and Z isomers of an alkene alcohol and derivatives thereof
MX2008011640A (es) * 2006-03-17 2008-09-22 Invista Tech Sarl Metodo para la purificacion de triorganofosfitos por tratamiento con un aditivo basico.
US7709674B2 (en) * 2006-07-14 2010-05-04 Invista North America S.A R.L Hydrocyanation process with reduced yield losses
WO2010123743A1 (en) 2009-04-21 2010-10-28 Invista Technologies S.A R.L. Highly selective process for producing organodiphosphites
CN102380353B (zh) * 2011-09-19 2013-08-21 江苏大学 一种磁性氧化镁表面分子印迹固相萃取剂的制备方法
CN103889991B (zh) 2011-10-26 2017-12-05 英威达纺织（英国）有限公司 特征在于测量副产物水平以确定进一步添加的由氯代亚磷酸酯制备有机二亚磷酸酯的方法
CN103402595B (zh) * 2011-12-21 2016-02-03 因温斯特技术公司 用于减少稳定乳液的萃取溶剂控制
KR20140127218A (ko) * 2011-12-21 2014-11-03 인비스타 테크놀러지스 에스.에이 알.엘. 안정한 에멀젼을 감소시키기 위한 추출 용매 제어
TWI709566B (zh) * 2015-09-30 2020-11-11 美商陶氏科技投資公司 用於製造有機磷化合物的方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1146166A (zh) * 1994-04-14 1997-03-26 纳幕尔杜邦公司 用于单烯烃氢氰化的双配位亚磷酸酯和镍的催化剂复合物
CN1159799A (zh) * 1994-10-07 1997-09-17 纳幕尔杜邦公司 氢氰化方法及所用多配位亚磷酸酯和镍催化剂复合物

Family Cites Families (15)

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Publication number Priority date Publication date Assignee Title
US3846461A (en) 1972-10-25 1974-11-05 Du Pont Process of preparing a zerovalent nickel complex with organic phosphorus compounds
US3903120A (en) 1973-06-19 1975-09-02 Du Pont Preparation of zerovalent nickel complexes from elemental nickel
US5747339A (en) * 1990-06-25 1998-05-05 Research Foundation For Microbial Diseases Of Osaka Non-A, non-B hepatitis virus genomic CDNA and antigen polypeptide
KR100263138B1 (ko) 1993-11-23 2000-08-01 이.아이,듀우판드네모아앤드캄파니 모노올레핀의 하이드로시안화 방법 및 이를 위한 촉매 조성물
US5512695A (en) 1994-04-14 1996-04-30 E. I. Du Pont De Nemours And Company Bidentate phosphite and nickel catalyst compositions for hydrocyanation of monoolefins
US5512696A (en) 1995-07-21 1996-04-30 E. I. Du Pont De Nemours And Company Hydrocyanation process and multidentate phosphite and nickel catalyst composition therefor
US5523453A (en) 1995-03-22 1996-06-04 E. I. Du Pont De Nemours And Company Process for hydrocyanation
US5693843A (en) 1995-12-22 1997-12-02 E. I. Du Pont De Nemours And Company Process for hydrocyanation of diolefins and isomerization of nonconjugated 2 alkyl-3-monoalkenenitriles
US6031120A (en) 1997-07-29 2000-02-29 E. I. Du Pont De Nemours And Company Selective synthesis of organodiphosphite compounds
ZA986374B (en) 1997-07-29 2000-01-17 Du Pont Hydrocyanation of diolefins and isomerization of nonconjugated 2-alkyl-3-monoalkenenitriles.
ZA986369B (en) 1997-07-29 2000-01-17 Du Pont Hydrocyanation of diolefins and isomerization of nonconjugated 2-alkyl-3-monoalkenenitriles.
US5959135A (en) 1997-07-29 1999-09-28 E. I. Du Pont De Nemours And Company Hydrocyanation processes and multidentate phosphite ligand and nickel catalyst compositions thereof
MY124170A (en) 1997-07-29 2006-06-30 Invista Tech Sarl Hydrocyanation processes and multidentate phosphite ligand and nickel catalyst compositions therefor
US6307107B1 (en) * 1999-09-20 2001-10-23 E.I. Du Pont De Nemours And Company Hydroformylation of acyclic monoethylenically unsaturated compounds to corresponding terminal aldehydes
US6660876B2 (en) * 2001-11-26 2003-12-09 E. I. Du Pont De Nemours And Company Phosphorus-containing compositions and their use in hydrocyanation, isomerization and hydroformylation reactions

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1146166A (zh) * 1994-04-14 1997-03-26 纳幕尔杜邦公司 用于单烯烃氢氰化的双配位亚磷酸酯和镍的催化剂复合物
CN1159799A (zh) * 1994-10-07 1997-09-17 纳幕尔杜邦公司 氢氰化方法及所用多配位亚磷酸酯和镍催化剂复合物

Also Published As

Publication number Publication date
DE602004005580T2 (de) 2008-01-24
ATE357972T1 (de) 2007-04-15
TW200500372A (en) 2005-01-01
DE602004005580D1 (de) 2007-05-10
EP1610894B1 (en) 2007-03-28
US6844289B2 (en) 2005-01-18
EP1610894A1 (en) 2006-01-04
SA04250241B1 (ar) 2007-07-31
CN1802213A (zh) 2006-07-12
MY138457A (en) 2009-06-30
JP2006523141A (ja) 2006-10-12
US20040204312A1 (en) 2004-10-14
WO2004091780A1 (en) 2004-10-28

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