JP2004517071A5 - - Google Patents

Download PDF

Info

Publication number
JP2004517071A5
JP2004517071A5 JP2002543503A JP2002543503A JP2004517071A5 JP 2004517071 A5 JP2004517071 A5 JP 2004517071A5 JP 2002543503 A JP2002543503 A JP 2002543503A JP 2002543503 A JP2002543503 A JP 2002543503A JP 2004517071 A5 JP2004517071 A5 JP 2004517071A5
Authority
JP
Japan
Prior art keywords
during crystallization
stability
adjusting
results
product
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP2002543503A
Other languages
English (en)
Other versions
JP2004517071A (ja
JP4560637B2 (ja
Filing date
Publication date
Application filed filed Critical
Priority claimed from PCT/US2001/043491 external-priority patent/WO2002040495A2/en
Publication of JP2004517071A publication Critical patent/JP2004517071A/ja
Publication of JP2004517071A5 publication Critical patent/JP2004517071A5/ja
Application granted granted Critical
Publication of JP4560637B2 publication Critical patent/JP4560637B2/ja
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Description

実施例２
結晶化中の生成物の安定性に対するｐＨの影響
結晶化中に存在するアセテートまたは他の緩衝物質の量に関わらず、母液のｐＨは時間が経つと下降する傾向がある。従来から、ｐＨは約３乃至約４の範囲を有する。我々は結晶化中にｐＨを中性付近に調整すると、最終生成物の安定性が極めて高くなることを発見した。次の表は、結晶化中にｐＨを変化させた種々のバッチの安定性の結果を示す。
Figure 2004517071
 中性付近（約６乃至約８）にｐＨを調整することによって、安定化を促進した試験環境の下で平均的な安定性を著しく高めることができることがデータから明らかである。
JP2002543503A 2000-11-17 2001-11-16 改良されたスクラロース組成物およびその結晶化の方法 Expired - Fee Related JP4560637B2 (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US24978200P 2000-11-17 2000-11-17
PCT/US2001/043491 WO2002040495A2 (en) 2000-11-17 2001-11-16 Improved sucralose composition and process for the crystallization thereof

Related Child Applications (1)

Application Number Title Priority Date Filing Date
JP2009188092A Division JP2009298803A (ja) 2000-11-17 2009-08-14 改良されたスクラロース組成物およびその結晶化の方法

Publications (3)

Publication Number Publication Date
JP2004517071A JP2004517071A (ja) 2004-06-10
JP2004517071A5 true JP2004517071A5 (ja) 2009-11-05
JP4560637B2 JP4560637B2 (ja) 2010-10-13

Family

ID=22944966

Family Applications (2)

Application Number Title Priority Date Filing Date
JP2002543503A Expired - Fee Related JP4560637B2 (ja) 2000-11-17 2001-11-16 改良されたスクラロース組成物およびその結晶化の方法
JP2009188092A Pending JP2009298803A (ja) 2000-11-17 2009-08-14 改良されたスクラロース組成物およびその結晶化の方法

Family Applications After (1)

Application Number Title Priority Date Filing Date
JP2009188092A Pending JP2009298803A (ja) 2000-11-17 2009-08-14 改良されたスクラロース組成物およびその結晶化の方法

Country Status (11)

Country Link
US (4) US6646121B2 (ja)
EP (1) EP1339728B1 (ja)
JP (2) JP4560637B2 (ja)
KR (1) KR100854528B1 (ja)
CN (1) CN1294139C (ja)
AU (2) AU2691802A (ja)
BR (1) BR0115482B1 (ja)
CA (1) CA2429228C (ja)
MX (1) MXPA03004402A (ja)
RU (1) RU2279437C2 (ja)
WO (1) WO2002040495A2 (ja)

Families Citing this family (54)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4614541B2 (ja) * 1999-04-16 2011-01-19 三栄源エフ・エフ・アイ株式会社 スクラロース含有組成物及び該組成物を含む可食性製品
US6921026B2 (en) * 2002-02-05 2005-07-26 Albert L. Saari Preservation of intermediate moisture foods by controlling humidity and inhibition of mold growth
US6998480B2 (en) * 2002-03-08 2006-02-14 Tate & Lyle Public Limited Company Process for improving sucralose purity and yield
US6984732B2 (en) * 2003-03-31 2006-01-10 Mcneil-Ppc, Inc. High-intensity sweetener composition and delivery of same
US6943248B2 (en) * 2003-04-30 2005-09-13 Tate & Lyle Public Limited Company Crystalline form of sucralose, and method for producing it
US20040258822A1 (en) * 2003-06-16 2004-12-23 Shyhyuan Liao Chilsonated sucralose product
US20040258818A1 (en) * 2003-06-20 2004-12-23 Kraft Foods Holdings, Inc. Reduced acidic flavor in acidified starch products
MXPA06010665A (es) * 2004-03-19 2007-03-28 Pharmed Medicare Pvt Ltd Un proceso mejorado para producir sacarosa clorada.
US20070020330A1 (en) 2004-11-24 2007-01-25 Medpointe Healthcare Inc. Compositions comprising azelastine and methods of use thereof
US8758816B2 (en) 2004-11-24 2014-06-24 Meda Pharmaceuticals Inc. Compositions comprising azelastine and methods of use thereof
LT2486942T (lt) 2004-11-24 2019-01-25 Meda Pharmaceuticals Inc. Kompozicijos, apimančios azelastiną ir jų panaudojimo būdai
JP4737977B2 (ja) * 2004-11-30 2011-08-03 株式会社ケーヒン 燃料電池用弁装置
CN101090906B (zh) * 2004-12-28 2012-07-04 日本甜菜制糖株式会社 二果糖二酐ⅲ晶体的制备方法
US7750146B2 (en) * 2005-03-18 2010-07-06 Tate & Lyle Plc Granular sucralose
US20060247180A1 (en) * 2005-04-29 2006-11-02 Bergey James L Purgative composition and uses thereof
US20060276639A1 (en) * 2005-06-01 2006-12-07 Healthy Brands, Llc Conversion of sucralose-6-ester to sucralose
DE202005019910U1 (de) * 2005-12-19 2007-04-19 Mann + Hummel Gmbh Filter
US7741477B2 (en) * 2006-01-10 2010-06-22 Alembic Limited Process for purification of sucralose
US20070264403A1 (en) * 2006-05-11 2007-11-15 Nehmer Warren L Sparkling agglomerated sweetener, and method of making it
US8791253B2 (en) * 2006-06-19 2014-07-29 The Coca-Cola Company Rebaudioside A composition and method for purifying rebaudioside A
US9012626B2 (en) * 2006-06-19 2015-04-21 The Coca-Cola Company Rebaudioside a composition and method for purifying rebaudioside a
BRPI0621844A2 (pt) * 2006-07-06 2013-03-19 Alembic Ltd processo aperfeiÇoado para a preparaÇço de sucralose de alta pureza
GB0702857D0 (en) * 2007-01-19 2007-03-28 Tate & Lyle Plc Improved sucralose production method
CN101260127B (zh) * 2007-03-06 2011-04-20 盐城捷康三氯蔗糖制造有限公司 由三氯蔗糖-6-乙酯脱乙酰基合成三氯蔗糖的方法
US8030481B2 (en) 2007-05-21 2011-10-04 The Coca-Cola Company Stevioside polymorphic and amorphous forms, methods for their formulation, and uses
US20080299277A1 (en) * 2007-06-01 2008-12-04 Yaohai Chao Sweetening Compositions
AR070082A1 (es) * 2008-01-04 2010-03-10 Tate & Lyle Technology Ltd Metodo para la produccion de sucralosa
US8476424B2 (en) * 2008-03-20 2013-07-02 Tate & Lyle Technology Limited Removal of acids from tertiary amide solvents
US8436157B2 (en) * 2008-03-26 2013-05-07 Tate & Lyle Technology Limited Method for the production of sucralose
US20090259036A1 (en) * 2008-04-03 2009-10-15 Tate & Lyle Technology Limited Extraction of less polar impurities from sucralose containing aqueous feed streams
US8212022B2 (en) * 2008-04-03 2012-07-03 Tate & Lyle Technology Limited Effect of carbohydrate concentration on sucralose extraction efficiency
US8497367B2 (en) * 2008-04-03 2013-07-30 Tate & Lyle Technology Limited Sucralose purification process
AR071134A1 (es) * 2008-04-03 2010-05-26 Tate & Lyle Technology Ltd Cristalizacion de sucralosa a partir de chorros que contienen sucralosa
WO2009140345A2 (en) * 2008-05-15 2009-11-19 Tate & Lyle Technology Ltd Buffer rinsed sucralose crystals
GB2468936B (en) 2009-03-27 2011-09-07 Mohamad Rami Radwan Jaber Chlorination of sucrose-6-esters
GB2469157B (en) 2009-03-30 2011-07-06 John Kerr Process for removing dimethylamine during sucralose production
GB2469158B (en) 2009-03-31 2011-09-28 Peter J Seaberg Base-assisted formation of tin-sucrose adducts
US20130045314A1 (en) * 2009-08-25 2013-02-21 Pratima N. Shastri Liquid sucralose sweetener composition
GB2474310B (en) 2009-10-12 2012-02-29 Tate & Lyle Technology Ltd Process for the production of sucrose-6-ester
GB2474311B (en) 2009-10-12 2012-10-17 Tate & Lyle Technology Ltd Low temperature, single solvent process for the production of sucrose-6-ester
GB201110520D0 (en) 2011-05-10 2011-08-03 Tate & Lyle Technology Ltd Extraction of carboxylic acids with tin compounds
CN102391319B (zh) * 2011-10-14 2015-01-07 山东三和维信生物科技有限公司 三氯蔗糖的结晶方法
CN102391320B (zh) * 2011-12-23 2014-03-19 盐城捷康三氯蔗糖制造有限公司 溶剂热回流纯化三氯蔗糖的方法
GB2503644A (en) * 2012-05-03 2014-01-08 British American Tobacco Co Filter
CN102977157A (zh) * 2012-12-05 2013-03-20 溧阳维信生物科技有限公司 一种三氯蔗糖的结晶方法
CN103242384B (zh) * 2013-05-27 2015-12-02 南通市常海食品添加剂有限公司 三氯蔗糖母液萃取工艺
US10227367B2 (en) 2013-12-16 2019-03-12 Tate & Lyle Technology Limited Chlorination of sucrose-6-esters
WO2016020635A1 (en) 2014-08-08 2016-02-11 Tate & Lyle Technology Limited Chlorination of sucrose-6-esters
GB2536480B (en) 2015-03-17 2019-09-04 Tate & Lyle Tech Ltd DMF Distillation
US9750811B2 (en) 2015-09-15 2017-09-05 Boveda, Inc. Devices and methods for controlling headspace humidity and oxygen levels
GB2551591B (en) 2016-06-23 2019-08-07 Tate & Lyle Tech Ltd Liquid-liquid extraction of DMF
AU2017342433B2 (en) 2016-10-12 2019-07-11 Boveda, Inc. Container and closure assembly with predetermined humidity and related method
CN109762030A (zh) * 2019-03-06 2019-05-17 福州大学 一种三氯蔗糖的结晶方法
CN112574258A (zh) * 2020-12-02 2021-03-30 安徽金禾实业股份有限公司 一种控制三氯蔗糖酸味的方法

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ZA807578B (en) * 1979-12-18 1981-11-25 Tate & Lyle Patent Holdings Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
GB2065646B (en) 1979-12-18 1983-10-05 Tate & Lyle Ltd Crystalline 4,1',6'-trichloro-4,1',6'-trideoxygalactosucrose
EP0030804B1 (en) * 1979-12-18 1983-10-19 TATE & LYLE PUBLIC LIMITED COMPANY Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
DE3062467D1 (en) 1979-12-20 1983-04-28 Tate & Lyle Plc Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
DE3165986D1 (en) 1980-07-08 1984-10-18 Tate & Lyle Plc Process for the preparation of 4, 1',6'-trichloro-4,1',6'-trideoxygalactosucrose (tgs)
GB8500862D0 (en) * 1985-01-14 1985-02-20 Tate & Lyle Plc Composition
GB8525953D0 (en) 1985-10-21 1985-11-27 Mcneilab Inc Preparation of galactopyranoside
GB8525954D0 (en) 1985-10-21 1985-11-27 Mcneilab Inc Chlorination of carbohydrates &c alcohols
DE3602090A1 (de) 1986-01-24 1987-07-30 Basf Ag Verfahren zur herstellung von aromatischen block-copolyethern
GB8617222D0 (en) 1986-07-15 1986-08-20 Tate & Lyle Plc Sweetener
GB8627139D0 (en) 1986-11-13 1986-12-10 Tate & Lyle Plc Sweetening composition
US4950746A (en) 1988-07-18 1990-08-21 Noramco, Inc. Process for synthesizing sucrose derivatives by regioselective reaction
GB8818430D0 (en) 1988-08-03 1988-09-07 Tate & Lyle Plc Process
GB8822674D0 (en) 1988-09-27 1988-11-02 Tate & Lyle Plc Preparation of acylated sucrose derivatives
US4980463A (en) * 1989-07-18 1990-12-25 Noramco, Inc. Sucrose-6-ester chlorination
US5034551A (en) * 1990-04-23 1991-07-23 Noramco, Inc. Process for recovery of organotin esters from reaction mixtures containing the same and re-use of the recovered organotin compounds
US5470969A (en) 1990-08-27 1995-11-28 Mcneil-Ppc, Inc. Catalyzed sucrose-6-ester process
JPH06155682A (ja) * 1992-11-25 1994-06-03 Kumagaya:Kk 包装体
US5298611A (en) 1993-03-12 1994-03-29 Mcneil-Ppc, Inc. Sucralose pentaester production
US5498709A (en) 1994-10-17 1996-03-12 Mcneil-Ppc, Inc. Production of sucralose without intermediate isolation of crystalline sucralose-6-ester
US5874155A (en) * 1995-06-07 1999-02-23 American National Can Company Easy-opening flexible packaging laminates and packaging materials made therefrom
GB9517281D0 (en) * 1995-08-23 1995-10-25 Tate & Lyle Plc Solid sucralose
JP2000142799A (ja) * 1998-11-12 2000-05-23 Ma Packaging:Kk 易開封袋
JP2000272060A (ja) * 1999-03-25 2000-10-03 Toyo Aluminium Kk 化学製品包装用積層体と蓋材および袋

Similar Documents

Publication Publication Date Title
JP2004517071A5 (ja)
CA2056066A1 (en) A physical form of n-[4-[5-(cyclopentyloxycarbony)amino-1-methylindol-3yl-methy1]-3-methoxybenzoy1]-2-methlbenzenesulphonamide, processes for its preparation and compositions containing it
CA2448954A1 (en) Fatty acid compositions having superior stability and flavor properties
JP2006528706A5 (ja)
RU93054180A (ru) Абразивное изделие и способ абразивной обработки
NO934271L (no) Anvendelse av rensede overflatemodifiseringsmidler for å hindre partikkelaggregering under sterilisering
RU94046268A (ru) Микрогранулы омепразола и способ их получения
JP2001093837A5 (ja)
ES2105951A1 (es) Procedimiento de obtencion por aglomeracion de agentes filtrantes diatomiticos.
WO2007017895A3 (en) Stabilized oral pharmaceutical compositions of cephalosporins
WO2015141516A1 (ja) オルガノシラン水溶液及びその保存方法
JP2005529145A5 (ja)
AU2018240412B2 (en) Remoistening of thermally inhibited starch and/or flour
JP2006070024A (ja) 顆粒状製剤及びその製造方法
HUT47374A (en) Fungicide compositions containing /2-cyano-2-oximino-acetyl/-aminoacid derivatives as active components and process for producing the active components
ITMI20040498A1 (it) Composizioni granulari
SU1608212A1 (ru) Полировальна паста
CA2482017A1 (en) Magnetic embryo transfer
US10239121B2 (en) Clay-like composition for sintered precious metal body
JP2008193902A (ja) 無塩梅干の製造方法
CA2100099A1 (en) Isothiazole Derivatives and Processes for Preparing the Same as Well as Termite Controlling Agents Comprising the Same as Active Ingredient
JP2004215522A (ja) 米粒中のγ−アミノ酪酸を富化させる方法及びその方法によって得られた米粒
JP2000128777A5 (ja)
JP3497892B2 (ja) 早茹麺類の製造法
JP2005538705A5 (ja)