JP2002543255A5 - - Google Patents
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- Publication number
- JP2002543255A5 JP2002543255A5 JP2000615675A JP2000615675A JP2002543255A5 JP 2002543255 A5 JP2002543255 A5 JP 2002543255A5 JP 2000615675 A JP2000615675 A JP 2000615675A JP 2000615675 A JP2000615675 A JP 2000615675A JP 2002543255 A5 JP2002543255 A5 JP 2002543255A5
- Authority
- JP
- Japan
- Prior art keywords
- polyether polyol
- crystallized
- propylene oxide
- parts
- molecular weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229920005862 polyol Polymers 0.000 description 41
- 150000003077 polyols Chemical class 0.000 description 41
- 229920000570 polyether Polymers 0.000 description 35
- 239000004721 Polyphenylene oxide Substances 0.000 description 34
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 24
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 18
- 239000003054 catalyst Substances 0.000 description 16
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 15
- 150000002924 oxiranes Chemical class 0.000 description 9
- 229920002635 polyurethane Polymers 0.000 description 8
- 239000004814 polyurethane Substances 0.000 description 8
- -1 alkoxy compound Chemical class 0.000 description 7
- 238000002425 crystallisation Methods 0.000 description 7
- 230000008025 crystallization Effects 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 7
- 239000000047 product Substances 0.000 description 7
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 6
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical group [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 229910052751 metal Inorganic materials 0.000 description 6
- 239000002184 metal Substances 0.000 description 6
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical group [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 5
- 150000001875 compounds Chemical class 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 230000000707 stereoselective effect Effects 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 239000000543 intermediate Substances 0.000 description 4
- 239000011541 reaction mixture Substances 0.000 description 4
- 229910052725 zinc Inorganic materials 0.000 description 4
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 description 3
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 229910001854 alkali hydroxide Inorganic materials 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 239000012043 crude product Substances 0.000 description 3
- 238000010992 reflux Methods 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- XTHFKEDIFFGKHM-UHFFFAOYSA-N Dimethoxyethane Chemical compound COCCOC XTHFKEDIFFGKHM-UHFFFAOYSA-N 0.000 description 2
- 229920005830 Polyurethane Foam Polymers 0.000 description 2
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 description 2
- 238000007259 addition reaction Methods 0.000 description 2
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 229920003225 polyurethane elastomer Polymers 0.000 description 2
- 239000011496 polyurethane foam Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000012721 stereospecific polymerization Methods 0.000 description 2
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 description 2
- TURGQPDWYFJEDY-UHFFFAOYSA-N 1-hydroperoxypropane Chemical compound CCCOO TURGQPDWYFJEDY-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- AWMVMTVKBNGEAK-UHFFFAOYSA-N Styrene oxide Chemical compound C1OC1C1=CC=CC=C1 AWMVMTVKBNGEAK-UHFFFAOYSA-N 0.000 description 1
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 1
- 238000012644 addition polymerization Methods 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical group [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 229910052792 caesium Inorganic materials 0.000 description 1
- TVFDJXOCXUVLDH-UHFFFAOYSA-N caesium atom Chemical compound [Cs] TVFDJXOCXUVLDH-UHFFFAOYSA-N 0.000 description 1
- RKBAPHPQTADBIK-UHFFFAOYSA-N cobalt;hexacyanide Chemical compound [Co].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-] RKBAPHPQTADBIK-UHFFFAOYSA-N 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000000536 complexating effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- UZZWBUYVTBPQIV-UHFFFAOYSA-N dme dimethoxyethane Chemical compound COCCOC.COCCOC UZZWBUYVTBPQIV-UHFFFAOYSA-N 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 229910021505 gold(III) hydroxide Inorganic materials 0.000 description 1
- WDZVNNYQBQRJRX-UHFFFAOYSA-K gold(iii) hydroxide Chemical compound O[Au](O)O WDZVNNYQBQRJRX-UHFFFAOYSA-K 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 239000003446 ligand Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 150000002825 nitriles Chemical class 0.000 description 1
- 239000012074 organic phase Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 239000011527 polyurethane coating Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- UUCCCPNEFXQJEL-UHFFFAOYSA-L strontium dihydroxide Chemical compound [OH-].[OH-].[Sr+2] UUCCCPNEFXQJEL-UHFFFAOYSA-L 0.000 description 1
- 229910001866 strontium hydroxide Inorganic materials 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 239000012855 volatile organic compound Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 235000005074 zinc chloride Nutrition 0.000 description 1
- 239000011592 zinc chloride Substances 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19919267.7 | 1999-04-28 | ||
| DE19919267A DE19919267A1 (de) | 1999-04-28 | 1999-04-28 | Kristallisierende Polyetherpolyole, ein Verfahren zu deren Herstellung sowie deren Verwendung |
| PCT/EP2000/003495 WO2000066648A1 (de) | 1999-04-28 | 2000-04-18 | Kristallisierende polyetherpolyole, ein verfahren zu deren herstellung sowie deren verwendung |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2002543255A JP2002543255A (ja) | 2002-12-17 |
| JP2002543255A5 true JP2002543255A5 (https=) | 2007-06-07 |
| JP4896296B2 JP4896296B2 (ja) | 2012-03-14 |
Family
ID=7906131
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2000615675A Expired - Fee Related JP4896296B2 (ja) | 1999-04-28 | 2000-04-18 | 結晶化ポリエーテルポリオール |
Country Status (20)
| Country | Link |
|---|---|
| US (1) | US6569981B1 (https=) |
| EP (1) | EP1177237B1 (https=) |
| JP (1) | JP4896296B2 (https=) |
| KR (1) | KR100558233B1 (https=) |
| CN (1) | CN1117789C (https=) |
| AT (1) | ATE274015T1 (https=) |
| AU (1) | AU4296300A (https=) |
| BR (1) | BR0010066B1 (https=) |
| CA (1) | CA2371540C (https=) |
| CZ (1) | CZ20013850A3 (https=) |
| DE (2) | DE19919267A1 (https=) |
| ES (1) | ES2226820T3 (https=) |
| HK (1) | HK1046418B (https=) |
| HU (1) | HUP0200943A2 (https=) |
| ID (1) | ID30442A (https=) |
| MX (1) | MXPA01010932A (https=) |
| PL (1) | PL351610A1 (https=) |
| RU (1) | RU2001132153A (https=) |
| TW (1) | TW527376B (https=) |
| WO (1) | WO2000066648A1 (https=) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ATE532811T1 (de) | 2006-08-31 | 2011-11-15 | Asahi Glass Co Ltd | Verfahren zur reinigung einer polyetherverbindung |
| SG191340A1 (en) * | 2010-12-27 | 2013-08-30 | Dow Global Technologies Llc | Alkylene oxide polymerization using a double metal cyanide catalyst complex and a magnesium, group 3-group 15 metal or lanthanide series metal compound |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE566583A (https=) | 1957-04-08 | |||
| DE1720337A1 (de) | 1967-12-27 | 1971-06-09 | Basf Ag | Verfahren zur Herstellung von hochmolekularen Polyaethern aus Epoxyden |
| JPS4812080B1 (https=) * | 1969-10-20 | 1973-04-18 | ||
| JPS495237B1 (https=) * | 1970-01-07 | 1974-02-06 | ||
| JPS495637B1 (https=) * | 1970-03-19 | 1974-02-08 | ||
| JPS4917440B1 (https=) * | 1970-09-08 | 1974-04-30 | ||
| US4962281A (en) | 1985-12-13 | 1990-10-09 | The Dow Chemical Company | Synthesis of stereoregular poly(propylene oxide) |
| DE19709031A1 (de) | 1997-03-06 | 1998-09-10 | Basf Ag | Verfahren zur Herstellung von Doppelmetallcyanidkatalysatoren |
| DE19748359A1 (de) * | 1997-11-03 | 1999-05-06 | Bayer Ag | Verfahren zur Herstellung teilkristalliner Polyetherpolyole |
-
1999
- 1999-04-28 DE DE19919267A patent/DE19919267A1/de not_active Withdrawn
-
2000
- 2000-04-18 EP EP00922645A patent/EP1177237B1/de not_active Expired - Lifetime
- 2000-04-18 PL PL00351610A patent/PL351610A1/xx not_active Application Discontinuation
- 2000-04-18 RU RU2001132153/04A patent/RU2001132153A/ru not_active Application Discontinuation
- 2000-04-18 BR BRPI0010066-8A patent/BR0010066B1/pt not_active IP Right Cessation
- 2000-04-18 AT AT00922645T patent/ATE274015T1/de not_active IP Right Cessation
- 2000-04-18 CA CA002371540A patent/CA2371540C/en not_active Expired - Fee Related
- 2000-04-18 MX MXPA01010932A patent/MXPA01010932A/es unknown
- 2000-04-18 DE DE50007496T patent/DE50007496D1/de not_active Expired - Lifetime
- 2000-04-18 ES ES00922645T patent/ES2226820T3/es not_active Expired - Lifetime
- 2000-04-18 HU HU0200943A patent/HUP0200943A2/hu unknown
- 2000-04-18 AU AU42963/00A patent/AU4296300A/en not_active Abandoned
- 2000-04-18 ID IDW00200102350A patent/ID30442A/id unknown
- 2000-04-18 HK HK02107962.7A patent/HK1046418B/zh not_active IP Right Cessation
- 2000-04-18 US US10/030,489 patent/US6569981B1/en not_active Expired - Lifetime
- 2000-04-18 WO PCT/EP2000/003495 patent/WO2000066648A1/de not_active Ceased
- 2000-04-18 KR KR1020017013782A patent/KR100558233B1/ko not_active Expired - Fee Related
- 2000-04-18 CN CN00806680A patent/CN1117789C/zh not_active Expired - Lifetime
- 2000-04-18 CZ CZ20013850A patent/CZ20013850A3/cs unknown
- 2000-04-18 JP JP2000615675A patent/JP4896296B2/ja not_active Expired - Fee Related
- 2000-04-21 TW TW089107513A patent/TW527376B/zh not_active IP Right Cessation
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