JP2002275155A5 - - Google Patents
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- Publication number
- JP2002275155A5 JP2002275155A5 JP2002000313A JP2002000313A JP2002275155A5 JP 2002275155 A5 JP2002275155 A5 JP 2002275155A5 JP 2002000313 A JP2002000313 A JP 2002000313A JP 2002000313 A JP2002000313 A JP 2002000313A JP 2002275155 A5 JP2002275155 A5 JP 2002275155A5
- Authority
- JP
- Japan
- Prior art keywords
- methylene chloride
- methanol
- cdcl
- mhz
- ppm
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 9
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- WQDUMFSSJAZKTM-UHFFFAOYSA-N Sodium methoxide Chemical compound [Na+].[O-]C WQDUMFSSJAZKTM-UHFFFAOYSA-N 0.000 description 2
- 238000000655 nuclear magnetic resonance spectrum Methods 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- GGPNYXIOFZLNKW-UHFFFAOYSA-N piperidin-3-amine;dihydrochloride Chemical compound Cl.Cl.NC1CCCNC1 GGPNYXIOFZLNKW-UHFFFAOYSA-N 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- DYHSDKLCOJIUFX-UHFFFAOYSA-N tert-butoxycarbonyl anhydride Chemical compound CC(C)(C)OC(=O)OC(=O)OC(C)(C)C DYHSDKLCOJIUFX-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2002000313A JP2002275155A (ja) | 2001-01-11 | 2002-01-07 | 環状アミン誘導体の製造方法 |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2001-3272 | 2001-01-11 | ||
| JP2001003272 | 2001-01-11 | ||
| JP2002000313A JP2002275155A (ja) | 2001-01-11 | 2002-01-07 | 環状アミン誘導体の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2002275155A JP2002275155A (ja) | 2002-09-25 |
| JP2002275155A5 true JP2002275155A5 (enExample) | 2006-01-12 |
Family
ID=26607506
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2002000313A Pending JP2002275155A (ja) | 2001-01-11 | 2002-01-07 | 環状アミン誘導体の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP2002275155A (enExample) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006022045A (ja) * | 2004-07-08 | 2006-01-26 | Kaneka Corp | 光学活性１−ｔ−ブトキシカルボニル−３−アミノピロリジン塩の単離精製方法 |
| JP2006219382A (ja) * | 2005-02-08 | 2006-08-24 | Toray Fine Chemicals Co Ltd | 環状ジアミノ化合物誘導体の製造方法 |
-
2002
- 2002-01-07 JP JP2002000313A patent/JP2002275155A/ja active Pending
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