JP2002107874A

JP2002107874A - 熱現像感光材料

熱現像感光材料

Info

Publication number: JP2002107874A
Authority: JP; Japan
Prior art keywords: group; photothermographic material; image forming; silver; layer
Prior art date: 2000-09-27
Legal status : Pending

Application number

JP2000293879A

Other languages

English (en)

Japanese (ja)

Other versions

JP2002107874A5 (cg-RX-API-DMAC7.html

Inventor

Tokuki Oikawa

徳樹及川

Current Assignee

Fujifilm Holdings Corp

Original Assignee

Fuji Photo Film Co Ltd

Priority date

2000-09-27

Filing date

2000-09-27

Publication date

2002-04-10

2000-09-27 Application filed by Fuji Photo Film Co Ltd filed Critical Fuji Photo Film Co Ltd

2000-09-27 Priority to JP2000293879A priority Critical patent/JP2002107874A/ja

2001-08-14 Priority to US09/928,339 priority patent/US20020055068A1/en

2002-04-10 Publication of JP2002107874A publication Critical patent/JP2002107874A/ja

2005-11-10 Publication of JP2002107874A5 publication Critical patent/JP2002107874A5/ja

Status Pending legal-status Critical Current

Links

239000000463 material Substances 0.000 title claims abstract description 139
-1 silver halide Chemical class 0.000 claims abstract description 206
239000010410 layer Substances 0.000 claims abstract description 202
238000000034 method Methods 0.000 claims abstract description 95
229910052709 silver Inorganic materials 0.000 claims abstract description 89
239000004332 silver Substances 0.000 claims abstract description 85
150000001875 compounds Chemical class 0.000 claims abstract description 74
238000011161 development Methods 0.000 claims abstract description 66
GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 claims abstract description 52
125000001424 substituent group Chemical group 0.000 claims abstract description 46
239000011230 binding agent Substances 0.000 claims abstract description 33
239000011241 protective layer Substances 0.000 claims abstract description 25
125000003545 alkoxy group Chemical group 0.000 claims abstract description 24
125000006575 electron-withdrawing group Chemical group 0.000 claims abstract description 20
125000004104 aryloxy group Chemical group 0.000 claims abstract description 16
125000004414 alkyl thio group Chemical group 0.000 claims abstract description 13
230000008569 process Effects 0.000 claims abstract description 12
125000005110 aryl thio group Chemical group 0.000 claims abstract description 11
125000004122 cyclic group Chemical group 0.000 claims abstract description 11
125000003282 alkyl amino group Chemical group 0.000 claims abstract description 7
125000002490 anilino group Chemical group [H]N(*)C1=C([H])C([H])=C([H])C([H])=C1[H] 0.000 claims abstract description 6
238000000576 coating method Methods 0.000 claims description 90
239000011248 coating agent Substances 0.000 claims description 88
150000003839 salts Chemical class 0.000 claims description 51
125000000623 heterocyclic group Chemical group 0.000 claims description 48
239000002253 acid Substances 0.000 claims description 16
125000003277 amino group Chemical group 0.000 claims description 15
125000004149 thio group Chemical group *S* 0.000 claims description 11
125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 10
125000001820 oxy group Chemical group [*:1]O[*:2] 0.000 claims description 10
230000036571 hydration Effects 0.000 claims description 7
238000006703 hydration reaction Methods 0.000 claims description 7
125000005647 linker group Chemical group 0.000 claims description 7
DLYUQMMRRRQYAE-UHFFFAOYSA-N tetraphosphorus decaoxide Chemical compound O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 claims description 7
238000003860 storage Methods 0.000 abstract description 9
QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract description 4
239000000243 solution Substances 0.000 description 83
125000004432 carbon atom Chemical group C* 0.000 description 73
239000002245 particle Substances 0.000 description 69
239000006185 dispersion Substances 0.000 description 68
229920000642 polymer Polymers 0.000 description 58
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 58
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239000004816 latex Substances 0.000 description 53
238000001035 drying Methods 0.000 description 46
239000007787 solid Substances 0.000 description 46
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 45
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 36
239000007864 aqueous solution Substances 0.000 description 36
238000002360 preparation method Methods 0.000 description 36
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239000000975 dye Substances 0.000 description 31
239000007788 liquid Substances 0.000 description 31
125000003118 aryl group Chemical group 0.000 description 29
238000010438 heat treatment Methods 0.000 description 29
108010010803 Gelatin Proteins 0.000 description 28
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239000008273 gelatin Substances 0.000 description 27
229920002451 polyvinyl alcohol Polymers 0.000 description 25
239000000203 mixture Substances 0.000 description 24
SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 description 24
239000002904 solvent Substances 0.000 description 20
239000000126 substance Substances 0.000 description 20
239000004372 Polyvinyl alcohol Substances 0.000 description 19
239000003638 chemical reducing agent Substances 0.000 description 19
238000012545 processing Methods 0.000 description 19
ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 18
125000001841 imino group Chemical group [H]N=* 0.000 description 18
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 17
239000004094 surface-active agent Substances 0.000 description 16
125000000217 alkyl group Chemical group 0.000 description 15
125000003917 carbamoyl group Chemical group [H]N([H])C(*)=O 0.000 description 14
125000004093 cyano group Chemical group *C#N 0.000 description 14
239000000839 emulsion Substances 0.000 description 14
150000007524 organic acids Chemical class 0.000 description 14
AQRYNYUOKMNDDV-UHFFFAOYSA-M silver behenate Chemical compound [Ag+].CCCCCCCCCCCCCCCCCCCCCC([O-])=O AQRYNYUOKMNDDV-UHFFFAOYSA-M 0.000 description 14
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 13
125000002252 acyl group Chemical group 0.000 description 13
239000003795 chemical substances by application Substances 0.000 description 13
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 12
125000004442 acylamino group Chemical group 0.000 description 12
125000004453 alkoxycarbonyl group Chemical group 0.000 description 12
230000009477 glass transition Effects 0.000 description 12
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229920000139 polyethylene terephthalate Polymers 0.000 description 12
229910001961 silver nitrate Inorganic materials 0.000 description 12
VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 description 11
WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 11
229910052799 carbon Inorganic materials 0.000 description 11
125000002485 formyl group Chemical group [H]C(*)=O 0.000 description 11
230000002829 reductive effect Effects 0.000 description 11
229940126062 Compound A Drugs 0.000 description 10
NLDMNSXOCDLTTB-UHFFFAOYSA-N Heterophylliin A Natural products O1C2COC(=O)C3=CC(O)=C(O)C(O)=C3C3=C(O)C(O)=C(O)C=C3C(=O)OC2C(OC(=O)C=2C=C(O)C(O)=C(O)C=2)C(O)C1OC(=O)C1=CC(O)=C(O)C(O)=C1 NLDMNSXOCDLTTB-UHFFFAOYSA-N 0.000 description 10
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 10
MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 10
125000004397 aminosulfonyl group Chemical group NS(=O)(=O)* 0.000 description 10
229910052751 metal Inorganic materials 0.000 description 10
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125000004433 nitrogen atom Chemical group N* 0.000 description 10
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238000003756 stirring Methods 0.000 description 10
238000004804 winding Methods 0.000 description 10
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 9
125000004390 alkyl sulfonyl group Chemical group 0.000 description 9
125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 9
239000000428 dust Substances 0.000 description 9
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239000002667 nucleating agent Substances 0.000 description 9
150000003378 silver Chemical class 0.000 description 9
OEPOKWHJYJXUGD-UHFFFAOYSA-N 2-(3-phenylmethoxyphenyl)-1,3-thiazole-4-carbaldehyde Chemical compound O=CC1=CSC(C=2C=C(OCC=3C=CC=CC=3)C=CC=2)=N1 OEPOKWHJYJXUGD-UHFFFAOYSA-N 0.000 description 8
NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 8
229920003171 Poly (ethylene oxide) Polymers 0.000 description 8
DKGAVHZHDRPRBM-UHFFFAOYSA-N Tert-Butanol Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 description 8
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230000015572 biosynthetic process Effects 0.000 description 8
239000011575 calcium Substances 0.000 description 8
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235000019441 ethanol Nutrition 0.000 description 8
239000000194 fatty acid Substances 0.000 description 8
229930195729 fatty acid Natural products 0.000 description 8
KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 description 8
239000000178 monomer Substances 0.000 description 8
125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 description 8
239000003960 organic solvent Substances 0.000 description 8
125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 8
IOLCXVTUBQKXJR-UHFFFAOYSA-M potassium bromide Chemical compound [K+].[Br-] IOLCXVTUBQKXJR-UHFFFAOYSA-M 0.000 description 8
230000001235 sensitizing effect Effects 0.000 description 8
SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 7
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CVYDEWKUJFCYJO-UHFFFAOYSA-M sodium;docosanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCCCCCC([O-])=O CVYDEWKUJFCYJO-UHFFFAOYSA-M 0.000 description 7
125000002813 thiocarbonyl group Chemical group *C(*)=S 0.000 description 7
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229910052783 alkali metal Inorganic materials 0.000 description 6
239000000084 colloidal system Substances 0.000 description 6
235000019646 color tone Nutrition 0.000 description 6
230000000694 effects Effects 0.000 description 6
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PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 description 5
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ARENMZZMCSLORU-UHFFFAOYSA-N propan-2-yl naphthalene-1-sulfonate Chemical compound C1=CC=C2C(S(=O)(=O)OC(C)C)=CC=CC2=C1 ARENMZZMCSLORU-UHFFFAOYSA-N 0.000 description 1
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NDGRWYRVNANFNB-UHFFFAOYSA-N pyrazolidin-3-one Chemical compound O=C1CCNN1 NDGRWYRVNANFNB-UHFFFAOYSA-N 0.000 description 1
MCSKRVKAXABJLX-UHFFFAOYSA-N pyrazolo[3,4-d]triazole Chemical group N1=NN=C2N=NC=C21 MCSKRVKAXABJLX-UHFFFAOYSA-N 0.000 description 1
PBMFSQRYOILNGV-UHFFFAOYSA-N pyridazine Chemical compound C1=CC=NN=C1 PBMFSQRYOILNGV-UHFFFAOYSA-N 0.000 description 1
UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
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JWVCLYRUEFBMGU-UHFFFAOYSA-N quinazoline Chemical compound N1=CN=CC2=CC=CC=C21 JWVCLYRUEFBMGU-UHFFFAOYSA-N 0.000 description 1
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VXNYVYJABGOSBX-UHFFFAOYSA-N rhodium(3+);trinitrate Chemical compound [Rh+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O VXNYVYJABGOSBX-UHFFFAOYSA-N 0.000 description 1
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238000000926 separation method Methods 0.000 description 1
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IZXSLAZMYLIILP-ODZAUARKSA-M silver (Z)-4-hydroxy-4-oxobut-2-enoate Chemical compound [Ag+].OC(=O)\C=C/C([O-])=O IZXSLAZMYLIILP-ODZAUARKSA-M 0.000 description 1
ZUNKMNLKJXRCDM-UHFFFAOYSA-N silver bromoiodide Chemical compound [Ag].IBr ZUNKMNLKJXRCDM-UHFFFAOYSA-N 0.000 description 1
YRSQDSCQMOUOKO-KVVVOXFISA-M silver;(z)-octadec-9-enoate Chemical compound [Ag+].CCCCCCCC\C=C/CCCCCCCC([O-])=O YRSQDSCQMOUOKO-KVVVOXFISA-M 0.000 description 1
JKOCEVIXVMBKJA-UHFFFAOYSA-M silver;butanoate Chemical compound [Ag+].CCCC([O-])=O JKOCEVIXVMBKJA-UHFFFAOYSA-M 0.000 description 1
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AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 description 1
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238000010998 test method Methods 0.000 description 1
238000012360 testing method Methods 0.000 description 1
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BRWIZMBXBAOCCF-UHFFFAOYSA-N thiosemicarbazide group Chemical group NNC(=S)N BRWIZMBXBAOCCF-UHFFFAOYSA-N 0.000 description 1
UMGDCJDMYOKAJW-UHFFFAOYSA-N thiourea Chemical class NC(N)=S UMGDCJDMYOKAJW-UHFFFAOYSA-N 0.000 description 1
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125000002088 tosyl group Chemical group [H]C1=C([H])C(=C([H])C([H])=C1C([H])([H])[H])S(*)(=O)=O 0.000 description 1
150000003918 triazines Chemical class 0.000 description 1
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UNXRWKVEANCORM-UHFFFAOYSA-N triphosphoric acid Chemical compound OP(O)(=O)OP(O)(=O)OP(O)(O)=O UNXRWKVEANCORM-UHFFFAOYSA-N 0.000 description 1
229940048102 triphosphoric acid Drugs 0.000 description 1
OTOHACXAQUCHJO-UHFFFAOYSA-H tripotassium;hexachlororhodium(3-) Chemical compound [Cl-].[Cl-].[Cl-].[Cl-].[Cl-].[Cl-].[K+].[K+].[K+].[Rh+3] OTOHACXAQUCHJO-UHFFFAOYSA-H 0.000 description 1
RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
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GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 description 1