JP2001213821A - 不飽和のアルデヒドおよび酸を製造するための高炭化水素空間速度プロセス - Google Patents

不飽和のアルデヒドおよび酸を製造するための高炭化水素空間速度プロセス

Info

Publication number
JP2001213821A
JP2001213821A JP2000355843A JP2000355843A JP2001213821A JP 2001213821 A JP2001213821 A JP 2001213821A JP 2000355843 A JP2000355843 A JP 2000355843A JP 2000355843 A JP2000355843 A JP 2000355843A JP 2001213821 A JP2001213821 A JP 2001213821A
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JP
Japan
Prior art keywords
oxidation
reactor
temperature
heat transfer
contact
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2000355843A
Other languages
English (en)
Japanese (ja)
Other versions
JP2001213821A5 (https=
Inventor
Charles Michael Lonzetta
チャールズ・マイケル・ロンゼッタ
James Edward Elder
ジェームズ・エドワード・エルダー
David Kuruherutsu Peter
ピーター・デービッド・クルヘルツ
Allen Hale Timothy
ティモシー・アレン・ヘイル
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rohm and Haas Co
Original Assignee
Rohm and Haas Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rohm and Haas Co filed Critical Rohm and Haas Co
Publication of JP2001213821A publication Critical patent/JP2001213821A/ja
Publication of JP2001213821A5 publication Critical patent/JP2001213821A5/ja
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C57/03—Monocarboxylic acids
    • C07C57/04—Acrylic acid; Methacrylic acid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
    • C07C45/34—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds
    • C07C45/35—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds in propene or isobutene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/02—Processes carried out in the presence of solid particles; Reactors therefor with stationary particles
    • B01J2208/023—Details
    • B01J2208/024—Particulate material
    • B01J2208/025—Two or more types of catalyst
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
JP2000355843A 1999-11-23 2000-11-22 不飽和のアルデヒドおよび酸を製造するための高炭化水素空間速度プロセス Pending JP2001213821A (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US16707999P 1999-11-23 1999-11-23
US60/167079 1999-11-23

Publications (2)

Publication Number Publication Date
JP2001213821A true JP2001213821A (ja) 2001-08-07
JP2001213821A5 JP2001213821A5 (https=) 2008-01-17

Family

ID=22605843

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2000355843A Pending JP2001213821A (ja) 1999-11-23 2000-11-22 不飽和のアルデヒドおよび酸を製造するための高炭化水素空間速度プロセス

Country Status (7)

Country Link
US (2) US6620968B1 (https=)
EP (1) EP1106598A3 (https=)
JP (1) JP2001213821A (https=)
KR (1) KR100811510B1 (https=)
CN (1) CN1149184C (https=)
BR (1) BR0005544A (https=)
TW (1) TW581758B (https=)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006521314A (ja) * 2003-03-25 2006-09-21 ビーエーエスエフ　アクチェンゲゼルシャフト アクロレインからアクリル酸への不均一系接触部分気相酸化法
JP2008528683A (ja) * 2005-02-01 2008-07-31 エルジー・ケム・リミテッド 不飽和脂肪酸の製造法
JP4762899B2 (ja) * 2003-09-01 2011-08-31 エルジー・ケム・リミテッド 固定層触媒部分酸化反応器における改善された熱制御システムによる不飽和アルデヒド及び不飽和酸の製造方法
JP2014511343A (ja) * 2010-12-22 2014-05-15 エボニック デグサ ゲーエムベーハー アクロレインの製造および青酸の製造からの排ガスを熱的に後燃焼させるための方法
US9580376B2 (en) 2013-07-18 2017-02-28 Nippon Kayaku Kabushiki Kaisha Method for producing unsaturated aldehyde and/or unsaturated carboxylic acid

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US6620968B1 (en) * 1999-11-23 2003-09-16 Rohm And Haas Company High hydrocarbon space velocity process for preparing unsaturated aldehydes and acids
US20040104108A1 (en) 2002-12-03 2004-06-03 Mason Robert Michael High capacity purification of thermally unstable compounds
EP1611077B1 (de) 2003-03-25 2008-03-19 Basf Se Verfahren der heterogen katalysierten partiellen gasphasenoxidation von propen zu acrylsäure
TWI311131B (en) 2003-03-25 2009-06-21 Basf Ag Heterogeneously catalyzed partial gas phase oxidation of propene to acrolein
DE10313212A1 (de) 2003-03-25 2004-10-07 Basf Ag Verfahren der heterogen katalysierten partiellen Gasphasenoxidation von Propen zu Acrolein
DE10313214A1 (de) 2003-03-25 2004-10-07 Basf Ag Verfahren der heterogen katalysierten partiellen Gasphasenoxidation von Acrolein zu Acrylsäure
DE10313209A1 (de) 2003-03-25 2004-03-04 Basf Ag Verfahren der heterogen katalysierten partiellen Gasphasenoxidation von Propen zu Acrylsäure
DE10313208A1 (de) 2003-03-25 2004-10-07 Basf Ag Verfahren der heterogen katalysierten partiellen Gasphasenoxidation von Propen zu Acrylsäure
CN1819869A (zh) * 2003-07-31 2006-08-16 陶氏环球技术公司 氧化方法和具有改良进料系统的反应器
EP1687249B1 (de) 2003-08-06 2009-12-02 Basf Se Verfahren zum betreiben einer kontinuierlichen heterogen katalysierten gasphasen-partialoxidation wenigstens einer organischen verbindung
RU2361853C2 (ru) 2003-08-14 2009-07-20 Басф Акциенгезельшафт Способ получения (мет)акролеина и/или (мет)акриловой кислоты
US7019169B2 (en) 2003-09-23 2006-03-28 Basf Aktiengesellschaft Preparation of (meth)acrylic acid
US7012157B2 (en) 2003-09-23 2006-03-14 Basf Aktiengesellschaft Preparation of (meth)acrylic acid
WO2005047224A1 (de) 2003-10-29 2005-05-26 Basf Aktiengesellschaft Verfahren zum langzeitbetrieb einer heterogen katalysierten gasphasenpartialoxidation von propen zu acrolein
WO2005047226A1 (de) 2003-10-29 2005-05-26 Basf Aktiengesellschaft Verfahren zum langzeitbetrieb einer heterogen katalysierten gasphasenpartialoxidation von acrolein zu acrylsäure
DE10350812A1 (de) 2003-10-29 2005-06-02 Basf Ag Verfahren zum Langzeitbetrieb einer heterogen katalysierten Gasphasenpartialoxidation von Propen zu Acrolein
DE10351269A1 (de) 2003-10-31 2005-06-02 Basf Ag Verfahren zum Langzeitbetrieb einer heterogen katalysierten Gasphasenpartialoxidation von Propen zu Acrylsäure
IN2006KN00738A (https=) 2003-12-24 2007-08-03 Lg Chemical Ltd
BRPI0509632B1 (pt) 2004-05-07 2015-09-08 Basf Aktiengesellschaft processo para carregamento de tubos de contato de um feixe de tubos de contato de uma maneira estruturada
DE102004025445A1 (de) 2004-05-19 2005-02-10 Basf Ag Verfahren zum Langzeitbetrieb einer heterogen katalysierten Gasphasenpartialoxidation wenigstens einer organischen Verbindung
US7592483B2 (en) 2004-07-01 2009-09-22 Basf Aktiengesellschaft Preparation of acrolein or acrylic acid or a mixture thereof by heterogeneously catalyzed partial gas phase oxidation of propylene
US7439389B2 (en) 2005-03-01 2008-10-21 Basf Aktiengesellschaft Process for preparing at least one organic target compound by heterogeneously catalyzed gas phase partial oxidation
DE102005019911A1 (de) 2005-04-27 2006-11-02 Basf Ag Verfahren der rektifikativen Auftrennung einer Acrylsäure und/oder Methacrylsäure enthaltenden Flüssigkeit
DE102006000996A1 (de) 2006-01-05 2007-07-12 Basf Ag Verfahren der heterogen katalysierten Gasphasen-Partialoxidation wenigstens einer organischen Ausgangsverbindung
EP1734030A1 (de) 2006-01-18 2006-12-20 BASF Aktiengesellschaft Verfahren zum Langzeitbetrieb einer heterogen katalysierten partiellen Gasphasenoxidation einer organischen Ausgangsverbindung
DE102007004961A1 (de) 2007-01-26 2008-07-31 Basf Se Verfahren zur Herstellung von Katalysatorformkörpern, deren Aktivmasse ein Multielementoxid ist
DE102007010422A1 (de) 2007-03-01 2008-09-04 Basf Se Verfahren zur Herstellung eines Katalysators bestehend aus einem Trägerkörper und einer auf der Oberfläche des Trägerkörpers aufgebrachten katalytisch aktiven Masse
DE102007017080A1 (de) 2007-04-10 2008-10-16 Basf Se Verfahren zur Beschickung eines Längsabschnitts eines Kontaktrohres
DE102007025869A1 (de) 2007-06-01 2008-07-03 Basf Se Verfahren der Wiederbeschickung der Reaktionsrohre eines Rohrbündelreaktors mit einem neuen Katalysatorfestbett
DE102007028333A1 (de) 2007-06-15 2008-12-18 Basf Se Verfahren zum Einbringen einer wenigstens einer Produktionscharge von ringförmigen Schalenkatalysatoren K entnommenen Teilmenge in ein Reaktionsrohr eines Rohrbündelreaktors
DE102007028332A1 (de) 2007-06-15 2008-12-18 Basf Se Verfahren zum Beschicken eines Reaktors mit einem Katalysatorfestbett, das wenigstens ringförmige Katalysatorformkörper K umfasst
TW200948474A (en) 2008-04-09 2009-12-01 Basf Se Coated catalysts comprising a multimetal oxide comprising molybdenum
DE102008040093A1 (de) 2008-07-02 2008-12-18 Basf Se Verfahren zur Herstellung eines ringähnlichen oxidischen Formkörpers
DE102008040094A1 (de) 2008-07-02 2009-01-29 Basf Se Verfahren zur Herstellung eines oxidischen geometrischen Formkörpers
DE102008042060A1 (de) 2008-09-12 2009-06-18 Basf Se Verfahren zur Herstellung von geometrischen Katalysatorformkörpern
DE102008042061A1 (de) 2008-09-12 2010-03-18 Basf Se Verfahren zur Herstellung von geometrischen Katalysatorformkörpern
DE102008042064A1 (de) 2008-09-12 2010-03-18 Basf Se Verfahren zur Herstellung von geometrischen Katalysatorformkörpern
DE102008054586A1 (de) 2008-12-12 2010-06-17 Basf Se Verfahren zur kontinuierlichen Herstellung von geometrischen Katalysatorformkörpern K
DE102010048405A1 (de) 2010-10-15 2011-05-19 Basf Se Verfahren zum Langzeitbetrieb einer heterogen katalysierten partiellen Gasphasenoxidation von Proben zu Acrolein
DE102011076931A1 (de) 2011-06-03 2012-12-06 Basf Se Wässrige Lösung, enthaltend Acrylsäure und deren konjugierte Base
BR112014000343B1 (pt) 2011-07-12 2019-12-24 Basf Se composição de óxido multimetálico, catalisador revestido, corpo de catalisador formado todo ativo, processo para preparar unia composição de óxido multimetálico, e, uso de pelo menos um óxido multimetálico
DE102011084040A1 (de) 2011-10-05 2012-01-05 Basf Se Mo, Bi und Fe enthaltende Multimetalloxidmasse
DE102011079035A1 (de) 2011-07-12 2013-01-17 Basf Se Mo, Bi und Fe enthaltende Multimetalloxidmassen
DE102013202048A1 (de) 2013-02-07 2013-04-18 Basf Se Verfahren zur Herstellung einer katalytisch aktiven Masse, die ein Gemisch aus einem die Elemente Mo und V enthaltenden Multielementoxid und wenigstens einem Oxid des Molybdäns ist
EP3068754B1 (de) 2013-11-11 2018-01-31 Basf Se Verfahren zur herstellung eines ungesättigten aldehyds und/oder einer ungesättigten carbonsäure
CN105899480B (zh) 2013-11-11 2018-11-13 巴斯夫欧洲公司 用于烯烃气相氧化以获得不饱和醛和/或不饱和羧酸的机械上稳定的中空圆柱形模制催化剂体
DE102015209638A1 (de) 2015-05-27 2016-07-07 Basf Se Verfahren zur Herstellung eines Bismut und Wolfram enthaltenden Multielementoxids durch Co-Präzipitation
DE102018200841A1 (de) 2018-01-19 2019-07-25 Basf Se Mo, Bi, Fe und Cu enthaltende Multimetalloxidmassen
EP3770145A1 (en) 2019-07-24 2021-01-27 Basf Se A process for the continuous production of either acrolein or acrylic acid as the target product from propene
KR102705461B1 (ko) * 2019-08-23 2024-09-09 주식회사 엘지화학 (메트)아크릴산 제조용 복수의 반응관의 제조 방법
EP3805194A1 (en) 2020-09-25 2021-04-14 Basf Se Method for producing a multimetal oxide catalyst under gas-tight conditions
EP4572887A1 (de) 2022-08-16 2025-06-25 Basf Se Verfahren zur herstellung von vollkatalysatorformkörpern zur gasphasenoxidation eines alkens und/oder eines alkohols zu einem a,b-ungesättigtem aldehyd und/oder einer a,b-ungesättigten carbonsäure
WO2025172145A1 (de) 2024-02-16 2025-08-21 Basf Se Anorganische faser-haltiger multi-element-vollkatalysatorformkörper zur herstellung von ungesättigten aldehyden und ungesättigten carbonsäuren; dessen herstellungsverfahren sowie verwendung in der gasphasenoxidation
WO2025176520A1 (de) 2024-02-23 2025-08-28 Basf Se Verfahren zur herstellung eines ethylenisch ungesättigten aldehyds und/oder einer ethylenisch ungesättigten carbonsäure an einem katalysatorfestbett eines rohrbündelreaktors

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JPS6463543A (en) * 1987-05-27 1989-03-09 Nippon Catalytic Chem Ind Production of acrylic acid
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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006521314A (ja) * 2003-03-25 2006-09-21 ビーエーエスエフ　アクチェンゲゼルシャフト アクロレインからアクリル酸への不均一系接触部分気相酸化法
JP4762899B2 (ja) * 2003-09-01 2011-08-31 エルジー・ケム・リミテッド 固定層触媒部分酸化反応器における改善された熱制御システムによる不飽和アルデヒド及び不飽和酸の製造方法
JP2008528683A (ja) * 2005-02-01 2008-07-31 エルジー・ケム・リミテッド 不飽和脂肪酸の製造法
JP2014511343A (ja) * 2010-12-22 2014-05-15 エボニック デグサ ゲーエムベーハー アクロレインの製造および青酸の製造からの排ガスを熱的に後燃焼させるための方法
US9580376B2 (en) 2013-07-18 2017-02-28 Nippon Kayaku Kabushiki Kaisha Method for producing unsaturated aldehyde and/or unsaturated carboxylic acid
JPWO2015008814A1 (ja) * 2013-07-18 2017-03-02 日本化薬株式会社 不飽和アルデヒドおよび／または不飽和カルボン酸の製造方法

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EP1106598A3 (en) 2003-01-29
CN1149184C (zh) 2004-05-12
CN1311177A (zh) 2001-09-05
US20040059155A1 (en) 2004-03-25
BR0005544A (pt) 2001-07-03
KR20010051867A (ko) 2001-06-25
TW581758B (en) 2004-04-01
KR100811510B1 (ko) 2008-03-07
US6620968B1 (en) 2003-09-16

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