IL37976A - Crystalline hydrate of trisodium d-fructose-1,6-diphosphoric acid and process for the preparation thereof - Google Patents
Crystalline hydrate of trisodium d-fructose-1,6-diphosphoric acid and process for the preparation thereofInfo
- Publication number
- IL37976A IL37976A IL37976A IL3797671A IL37976A IL 37976 A IL37976 A IL 37976A IL 37976 A IL37976 A IL 37976A IL 3797671 A IL3797671 A IL 3797671A IL 37976 A IL37976 A IL 37976A
- Authority
- IL
- Israel
- Prior art keywords
- aqueous solution
- acid
- fructose
- process according
- preparation
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 14
- SOBHUZYZLFQYFK-UHFFFAOYSA-K trisodium;hydroxy-[[phosphonatomethyl(phosphonomethyl)amino]methyl]phosphinate Chemical compound [Na+].[Na+].[Na+].OP(O)(=O)CN(CP(O)([O-])=O)CP([O-])([O-])=O SOBHUZYZLFQYFK-UHFFFAOYSA-K 0.000 title claims description 8
- 238000002360 preparation method Methods 0.000 title claims description 7
- 239000013078 crystal Substances 0.000 claims description 14
- 239000002253 acid Substances 0.000 claims description 12
- 239000007864 aqueous solution Substances 0.000 claims description 9
- 239000000243 solution Substances 0.000 claims description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 6
- 159000000000 sodium salts Chemical class 0.000 claims description 5
- 230000015572 biosynthetic process Effects 0.000 claims description 4
- 150000004689 octahydrates Chemical class 0.000 claims description 3
- 229910052698 phosphorus Inorganic materials 0.000 claims description 3
- XPYBSIWDXQFNMH-UHFFFAOYSA-N D-Fructose 1 Chemical compound OP(=O)(O)OCC(O)C(O)C(O)C(=O)COP(O)(O)=O XPYBSIWDXQFNMH-UHFFFAOYSA-N 0.000 claims 1
- BJHIKXHVCXFQLS-UYFOZJQFSA-N keto-D-fructose Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)C(=O)CO BJHIKXHVCXFQLS-UYFOZJQFSA-N 0.000 claims 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 4
- 239000011734 sodium Substances 0.000 description 4
- 229910052708 sodium Inorganic materials 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 238000002425 crystallisation Methods 0.000 description 3
- XPPKVPWEQAFLFU-UHFFFAOYSA-N diphosphoric acid Chemical compound OP(O)(=O)OP(O)(O)=O XPPKVPWEQAFLFU-UHFFFAOYSA-N 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
- 239000011574 phosphorus Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000007983 Tris buffer Substances 0.000 description 1
- XTUNVEMVWFXFGV-UHFFFAOYSA-N [C].CCO Chemical compound [C].CCO XTUNVEMVWFXFGV-UHFFFAOYSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 239000002274 desiccant Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 230000002503 metabolic effect Effects 0.000 description 1
- 239000012452 mother liquor Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- HRXKRNGNAMMEHJ-UHFFFAOYSA-K trisodium citrate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O HRXKRNGNAMMEHJ-UHFFFAOYSA-K 0.000 description 1
- -1 trisodium diphosphoric acid Chemical compound 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H11/00—Compounds containing saccharide radicals esterified by inorganic acids; Metal salts thereof
- C07H11/04—Phosphates; Phosphites; Polyphosphates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Saccharide Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19702061731 DE2061731C (de) | 1970-12-15 | Monoklines Trinatrium-D-fructose-1,6diphosphorsäure-Octahydrat und Verfahren zu seiner Herstellung |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| IL37976A0 IL37976A0 (en) | 1971-12-29 |
| IL37976A true IL37976A (en) | 1974-06-30 |
Family
ID=5791050
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IL37976A IL37976A (en) | 1970-12-15 | 1971-10-20 | Crystalline hydrate of trisodium d-fructose-1,6-diphosphoric acid and process for the preparation thereof |
Country Status (7)
| Country | Link |
|---|---|
| JP (1) | JPS5126417B1 (enExample) |
| FR (1) | FR2118103B1 (enExample) |
| GB (1) | GB1313720A (enExample) |
| HU (1) | HU163084B (enExample) |
| IL (1) | IL37976A (enExample) |
| NL (1) | NL7115376A (enExample) |
| SU (1) | SU452964A3 (enExample) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102127426A (zh) * | 2011-01-11 | 2011-07-20 | 宁波大学 | 一种具有紫色发光性能的荧光材料及其制备方法 |
-
1971
- 1971-10-20 IL IL37976A patent/IL37976A/en unknown
- 1971-11-09 NL NL7115376A patent/NL7115376A/xx not_active Application Discontinuation
- 1971-12-13 GB GB5769571A patent/GB1313720A/en not_active Expired
- 1971-12-14 HU HUBO1336A patent/HU163084B/hu unknown
- 1971-12-14 JP JP46101346A patent/JPS5126417B1/ja active Pending
- 1971-12-15 SU SU1726546A patent/SU452964A3/ru active
- 1971-12-15 FR FR7145113A patent/FR2118103B1/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| FR2118103A1 (enExample) | 1972-07-28 |
| IL37976A0 (en) | 1971-12-29 |
| GB1313720A (en) | 1973-04-18 |
| HU163084B (enExample) | 1973-06-28 |
| NL7115376A (enExample) | 1972-06-19 |
| DE2061731A1 (enExample) | 1972-03-16 |
| JPS5126417B1 (enExample) | 1976-08-06 |
| SU452964A3 (ru) | 1974-12-05 |
| FR2118103B1 (enExample) | 1975-06-13 |
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