HUP0100191A2 - Eljárás poliamid folytonos extrakciójára - Google Patents

Eljárás poliamid folytonos extrakciójára

Info

Publication number
HUP0100191A2
HUP0100191A2 HU0100191A HUP0100191A HUP0100191A2 HU P0100191 A2 HUP0100191 A2 HU P0100191A2 HU 0100191 A HU0100191 A HU 0100191A HU P0100191 A HUP0100191 A HU P0100191A HU P0100191 A2 HUP0100191 A2 HU P0100191A2
Authority
HU
Hungary
Prior art keywords
extraction
extraction process
zone
carried out
continuous
Prior art date
Application number
HU0100191A
Other languages
English (en)
Inventor
Peter Hildenbrand
Reinhard Lang
Alfons Ludwig
Gunter Pipper
Original Assignee
Basf Aktiengesellschaft
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Aktiengesellschaft filed Critical Basf Aktiengesellschaft
Publication of HUP0100191A2 publication Critical patent/HUP0100191A2/hu
Publication of HUP0100191A3 publication Critical patent/HUP0100191A3/hu

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/46—Post-polymerisation treatment
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/08—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
    • C08G69/14—Lactams
    • C08G69/16—Preparatory processes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/08—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
    • C08G69/14—Lactams

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Polyamides (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

A találmány tárgya eljárás poliamid-részecskék folytonos, ellenáramúextrakciójára. A találmány szerint az extrakciót körfolyamatbanvezetett vizes extrahálószerrel, egy lényegileg függőleges, két zónáraosztott extrakciós toronyban végezik. Az első zónában 15-40 tömeg%-osvizes kaprolaktám-oldattal végezik az extrakciót 100-140 °C-on majd amásodik zónában vízzel, a fentinél 5-40 °C-kal alacsonyabbhőmérsékleten. Az eljárás lehetővé teszi poliamid gazdaságosextrakcióját, ahol a kapott termék csekély monomer- ésoligomertartalmú. Ó
HU0100191A 1997-11-25 1998-11-24 Continuous polyamide extraction process HUP0100191A3 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19752182A DE19752182A1 (de) 1997-11-25 1997-11-25 Verfahren zur kontinuierlichen Extraktion von Polyamid
PCT/EP1998/007576 WO1999026998A1 (de) 1997-11-25 1998-11-24 Verfahren zur kontinuierlichen extraktion von polyamid

Publications (2)

Publication Number Publication Date
HUP0100191A2 true HUP0100191A2 (hu) 2001-05-28
HUP0100191A3 HUP0100191A3 (en) 2004-09-28

Family

ID=7849758

Family Applications (1)

Application Number Title Priority Date Filing Date
HU0100191A HUP0100191A3 (en) 1997-11-25 1998-11-24 Continuous polyamide extraction process

Country Status (22)

Country Link
US (1) US6320021B1 (hu)
EP (1) EP1030872B1 (hu)
JP (1) JP4233215B2 (hu)
KR (1) KR100548108B1 (hu)
CN (1) CN1175030C (hu)
AU (1) AU1963899A (hu)
BG (1) BG64318B1 (hu)
BR (1) BR9815006A (hu)
CA (1) CA2310848A1 (hu)
CO (1) CO5040145A1 (hu)
CZ (1) CZ290277B6 (hu)
DE (2) DE19752182A1 (hu)
ES (1) ES2172958T3 (hu)
HU (1) HUP0100191A3 (hu)
ID (1) ID24217A (hu)
IL (1) IL136057A (hu)
MY (1) MY129533A (hu)
PL (1) PL192671B1 (hu)
SK (1) SK6972000A3 (hu)
TR (1) TR200001511T2 (hu)
TW (1) TW393497B (hu)
WO (1) WO1999026998A1 (hu)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL1010161C2 (nl) * 1998-09-23 2000-03-24 Dsm Nv Proces voor de productie van polyamide-6 uitgaande èpsilon-caprolactam.
DE19957663A1 (de) * 1999-11-30 2001-05-31 Basf Ag Verfahren zur kontinuierlichen Herstellung von Copolyamiden, die auf einem Lactam (I), einem Diamin (II) und einer Dicarbonsäure (III) basieren
DE10047657B4 (de) * 2000-09-26 2005-02-10 Basf Ag Verfahren zur Herstellung von Polycaprolactam, ein Polycaprolactam und dessen Verwendung
DE10146932B4 (de) * 2000-09-26 2005-03-31 Basf Aktiengesellschaft Verfahren zur Verminderung des Caprolactamgehaltes von Polyamid 6, ein Polyamid 6 und dessen Verwendung
DE10124580A1 (de) * 2001-05-21 2002-12-05 Bayer Ag Verfahren zur Behandlung von Oligoamiden und zur Herstellung von Polyamid
US6479620B1 (en) * 2001-06-01 2002-11-12 E. I. Du Pont De Nemours And Company Process for converting caprolactam to nylon 6
DE10251798A1 (de) * 2002-11-07 2004-05-19 Bayer Ag Verfahren zur Herstellung von Polyamid 6 mit geringem Dimergehalt
JP3912311B2 (ja) 2003-03-28 2007-05-09 ブラザー工業株式会社 情報処理システム
DE102007057189A1 (de) * 2007-11-28 2009-06-04 Automatik Plastics Machinery Gmbh Verfahren und Vorrichtung zur Herstellung von Polyamid
FR2930251A1 (fr) * 2008-08-11 2009-10-23 Arkema France Procede de reduction de la teneur en oligomeres et en monomeres d'un copolyamide
EP2532698B1 (de) 2011-06-08 2016-04-20 Uhde Inventa-Fischer GmbH Verfahren und Vorrichtung zur direkten, kontinuierlichen Modifizierung von Polymerschmelzen
EP2682417A1 (de) 2012-07-06 2014-01-08 Basf Se Verfahren zur Reinigung von Polyamidteilchen
EP2725051B1 (de) * 2012-10-23 2015-03-11 Uhde Inventa-Fischer GmbH Kontinuierliches Verfahren zur Herstellung von Polyamid 6 und Vorrichtungen hierzu
EP2727637B1 (de) * 2012-11-06 2019-08-28 Uhde Inventa-Fischer GmbH Extraktionsreaktor sowie verfahren zur extraktion von granulärem material
US9708271B2 (en) 2012-11-06 2017-07-18 Uhde Inventa-Fischer Gmbh Extraction reactor and also method for extraction from granular material
CN103083936B (zh) * 2013-01-11 2015-07-01 南京海洋高压容器制造有限公司 一种可调塔盘的萃取塔及其用途
CN108211422B (zh) * 2018-04-16 2024-04-26 阳煤集团太原化工新材料有限公司 一种降低苯萃残液中己内酰胺的装置及方法
PL4065330T3 (pl) 2021-02-15 2023-10-23 T.EN Zimmer GmbH Sposób i urządzenie do wytwarzania peletek poliamidu 6

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE289471C (hu)
US3245964A (en) * 1962-11-13 1966-04-12 Allied Chem Continuous extraction of poly-e-caproamide
US3374207A (en) * 1964-11-12 1968-03-19 Inventa Ag Continuous process for the extraction of monomers and oligomers from highly polymerized caprolactam granules
DE1519936B2 (de) 1966-04-06 1973-09-27 Davy-Ashmore Ag, 6000 Frankfurt Extraktionsrohr zum kontinuierlichen Entfernen niedermolekularer Bestandteile aus granulierten Polyamiden
JPS4525519B1 (hu) * 1967-04-27 1970-08-24
DE1770097B2 (de) 1968-03-30 1974-04-18 Basf Ag, 6700 Ludwigshafen Verfahren zum kontinuierlichen Extrahieren von körnigen Polyamiden
JPS497359B1 (hu) 1970-01-30 1974-02-20
DE2242641C3 (de) * 1972-08-30 1980-06-19 Basf Ag, 6700 Ludwigshafen Verfahren zum kontinuierlichen Extrahieren von Polylactamen
DE2242642C3 (de) * 1972-08-30 1980-06-19 Basf Ag, 6700 Ludwigshafen Verfahren zum kontinuierlichen Extrahieren von Polylactamen
DE2404510C3 (de) * 1974-01-31 1985-02-21 Basf Ag, 6700 Ludwigshafen Extraktionsrohr für Polyamide
DE2501348C3 (de) 1975-01-15 1988-02-11 Basf Ag, 6700 Ludwigshafen Kontinuierliches Verfahren zur Herstellung von Polyamiden aus epsilon-Caprolactam
JPS51149397A (en) * 1975-02-12 1976-12-22 Unitika Ltd Scouring of polycaprolamide chip
JPS5371196A (en) 1976-12-06 1978-06-24 Mitsubishi Chem Ind Ltd Preparation of purified polyamide
DE2732328A1 (de) 1977-07-16 1979-02-01 Basf Ag Verfahren zur herstellung von polycaprolactam
IT1100787B (it) 1978-12-06 1985-09-28 Snia Viscosa Processo e apparecchiatura per demonomerizzazione di policaproammide
JPS60166324A (ja) 1984-02-09 1985-08-29 Teijin Ltd ポリアミドチツプの連続式洗浄装置
DE3710803A1 (de) 1987-03-31 1988-10-20 Basf Ag Verfahren zur entfernung von caprolactam und dessen oligomeren aus solches enthaltendem polyamidgranulat
DE3732170C1 (de) * 1987-09-24 1989-02-16 Bayer Ag Verfahren zur kontinuierlichen Extraktion von Polyamiden sowie dafuer geeignetes Extraktionsrohr
DD289471A5 (de) * 1988-08-03 1991-05-02 Veb Chemieanlagenbau Erfurt-Rudisleben,De Verfahren zur intensivierung der gegenstromextraktion von polyamid-6-granulat
DE4324616A1 (de) * 1993-07-22 1995-01-26 Bayer Ag Extraktion von Polyamid 6
DE19505150A1 (de) 1995-02-16 1996-08-22 Bayer Ag Verfahren zur Extraktion von Polyamid-6 oder Copolyamiden mit epsilon-Caprolactam

Also Published As

Publication number Publication date
US6320021B1 (en) 2001-11-20
DE19752182A1 (de) 1999-05-27
KR100548108B1 (ko) 2006-02-02
JP4233215B2 (ja) 2009-03-04
CZ20001930A3 (cs) 2000-11-15
JP2001524562A (ja) 2001-12-04
AU1963899A (en) 1999-06-15
CA2310848A1 (en) 1999-06-03
TW393497B (en) 2000-06-11
CZ290277B6 (cs) 2002-06-12
CO5040145A1 (es) 2001-05-29
KR20010032403A (ko) 2001-04-16
ID24217A (id) 2000-07-13
CN1175030C (zh) 2004-11-10
PL341572A1 (en) 2001-04-23
EP1030872B1 (de) 2002-02-06
HUP0100191A3 (en) 2004-09-28
WO1999026998A1 (de) 1999-06-03
BR9815006A (pt) 2002-09-24
MY129533A (en) 2007-04-30
IL136057A (en) 2005-08-31
EP1030872A1 (de) 2000-08-30
PL192671B1 (pl) 2006-11-30
CN1284096A (zh) 2001-02-14
ES2172958T3 (es) 2002-10-01
SK6972000A3 (en) 2000-11-07
BG64318B1 (bg) 2004-09-30
DE59803036D1 (de) 2002-03-21
BG104459A (en) 2001-01-31
IL136057A0 (en) 2001-05-20
TR200001511T2 (tr) 2002-07-22

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Legal Events

Date Code Title Description
FD9A Lapse of provisional protection due to non-payment of fees