HRP20120927T1 - Postupak destiliranja polaznog materijala i pogon za provedbu istog postupka - Google Patents
Postupak destiliranja polaznog materijala i pogon za provedbu istog postupka Download PDFInfo
- Publication number
- HRP20120927T1 HRP20120927T1 HRP20120927AT HRP20120927T HRP20120927T1 HR P20120927 T1 HRP20120927 T1 HR P20120927T1 HR P20120927A T HRP20120927A T HR P20120927AT HR P20120927 T HRP20120927 T HR P20120927T HR P20120927 T1 HRP20120927 T1 HR P20120927T1
- Authority
- HR
- Croatia
- Prior art keywords
- pressure
- condenser
- evaporator
- temperature
- tank
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims 19
- 238000009434 installation Methods 0.000 title 1
- 239000007858 starting material Substances 0.000 title 1
- 238000002156 mixing Methods 0.000 claims 11
- 238000004821 distillation Methods 0.000 claims 7
- 239000000463 material Substances 0.000 claims 6
- FGUUSXIOTUKUDN-IBGZPJMESA-N C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 Chemical compound C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 FGUUSXIOTUKUDN-IBGZPJMESA-N 0.000 claims 3
- 239000007789 gas Substances 0.000 claims 3
- 239000007788 liquid Substances 0.000 claims 3
- 229920006395 saturated elastomer Polymers 0.000 claims 3
- 238000009833 condensation Methods 0.000 claims 1
- 230000005494 condensation Effects 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 238000012423 maintenance Methods 0.000 claims 1
- 238000012544 monitoring process Methods 0.000 claims 1
- 239000003507 refrigerant Substances 0.000 claims 1
- 238000005507 spraying Methods 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/16—Evaporating by spraying
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/28—Evaporating with vapour compression
- B01D1/2881—Compression specifications (e.g. pressure, temperature, processes)
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/28—Evaporating with vapour compression
- B01D1/2887—The compressor is integrated in the evaporation apparatus
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/28—Evaporating with vapour compression
- B01D1/2896—Control, regulation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/001—Processes specially adapted for distillation or rectification of fermented solutions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/06—Flash distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/10—Vacuum distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/42—Regulation; Control
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0027—Condensation of vapours; Recovering volatile solvents by condensation by direct contact between vapours or gases and the cooling medium
- B01D5/003—Condensation of vapours; Recovering volatile solvents by condensation by direct contact between vapours or gases and the cooling medium within column(s)
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0057—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
- B01D5/006—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with evaporation or distillation
Claims (16)
1. Postupak destiliranja osnovnog materijala (4) koji sadrži tekućinu Fd koju treba destilirati uz pomoć plinski nepropusnog sustava spremnika (1) otpornog na pretlak i/ili potlak, koji sadrži otparivač (2) s osnovnim materijalom (4), kojem se može kontrolirati temperaturu, kondenzator (3) za kondenziranje tekućine Fd kojoj se može kontrolirati temperaturu, koju se pretvori u paru, u kondenzat (5), kao i parnu komoru (6), koja povezuje otparivač (2) s kondenzatorom (3) i miješajući kombinira njihove pare, gdje parna komora (6) ima senzor za tlak (7), za mjerenje tlaka miješanja pm prisutnog u miješanoj pari u parnoj komori (6), senzor za temperaturu (8), za mjerenje temperature miješanja Tm prisutne u miješanoj pari u parnoj komori (6), te regulator tlaka (9), kojeg treba provesti u koracima postupka gdje
a) otparivač (2) s osnovnim materijalom (4) se dovede na prvu temperaturu T1, a kondenzator (3) na drugu, nižu temperaturu T2;
b) mjeri se tlak miješanja pm i temperatura miješanja Tm;
c) tlak zasićene pare ps tekućine Fd se odredi na izmjerenoj temperaturi miješanja Tm;
d) referentni raspon tlaka (11) se odredi, koju ograničava donja granica tlaka p1, koja je u najmanju ruku 0,1% iznad tlaka zasićene pare ps, i donja granica tlaka p2, koja je najviše 6% iznad tlaka zasićene pare ps;
e) tlak miješanja pm se uspoređuje s referentnim rasponom tlaka (11);
f) tlak miješanja pm se precizno smanjuje regulatorom tlaka (9) dok ne dosegne nižu granicu tlaka p1;
g) korake a) do e) se ponavlja dok tlak miješanja pm ne dosegne višu granicu tlaka p2;
h) korake f) i g) se ponavlja dok destiliranje ne treba prekinuti;
naznačen time što se uz smanjivanje tlaka u koraku f) plinove u kondenzatoru (3) na kraju puta kondenziranja ekstrahira isisavanjem, kako bi se uklonilo čim je više moguće stranog plina iz sustava spremnika (1).
2. Postupak u skladu s patentnim zahtjevom 1, naznačen time što je razlika u temperaturi T1 – T2 između otparivača (2) i kondenzator (3) između 1 i 10 K, po mogućnosti između 1 i 3 K.
3. Postupak u skladu s bilo kojim od prethodnih patentnih zahtjeva, naznačen time što se površine osnovnog materijala (4) u otparivaču (2) i/ili površina kondenzata (5) u kondenzatoru (3) povećava, po mogućnosti raspršivanjem osnovnog materijala (4) ili kondenzata (5).
4. Postupak u skladu s patentnim zahtjevom 3, naznačen time što se povećavanje površine postiže uvođenjem poroznog umetka za povećavanje površine.
5. Postupak u skladu s bilo kojim od prethodnih patentnih zahtjeva, naznačen time što se raspodjelu pare u parnoj komori (6) pomno miješa ventilatorom (16), gdje je ventilator (16) po mogućnosti pogonjen volumnim protokom uštrcanog medija kojeg treba ispariti ili uštrcanog kondenzata.
6. Postupak u skladu s bilo kojim od prethodnih patentnih zahtjeva uz referiranje na patentni zahtjev 3, naznačen time što se uklanjanje stranog plina u koraku f) provodi vakuumskom mlaznom pumpom, koju pogoni bilo kondenzat (5) kojeg treba raspršiti iz istog stupnja ili iz stupnja hladila, para iz drugog stupnja, ili okolni zrak.
7. Postupak u skladu s bilo kojim od prethodnih patentnih zahtjeva, naznačen time što se postupak provodi u dva ili više takvih sustava spremnika (1, 1', …), gdje se rasponi temperature T1, T2 u pojedinačnim sustavima spremnika (1, 1', …) međusobno nadovezuju.
8. Postupak u skladu s patentnim zahtjevom 7, naznačen time što se energiju za grijanje otparivača (2) ili kondenzator (3) dobiva u najmanju ruku dijelom izravno ili posredno preko izmjenjivača topline iz energije iz drugog otparivača (2) ili kondenzatora (3), čiju temperaturu treba promijeniti.
9. Postupak u skladu s bilo kojim od patentnih zahtjeva 7 ili 8, naznačen time što se otparivač (2) i/ili kondenzatori (3) različitih sustava spremnika (1, 1', …) nalaze jedan iznad drugog.
10. Postupak u skladu s bilo kojim od prethodnih patentnih zahtjeva, naznačen time što sustav spremnika (1) i/ili cijevi su načinjeni u potpunosti ili pretežno od plastike.
11. Postupak u skladu s bilo kojim od prethodnih patentnih zahtjeva, naznačen time što cijeli sustav, ili njegovi dijelovi, osobito stjenke sustava spremnika (1), na koje su vezani povezujući dijelovi, i/ili pumpe, ventili, senzori, prirubnice i/ili drugi komponente relevantne za tlak, rade kao potopljeni.
12. Postupak u skladu s bilo kojim od prethodnih patentnih zahtjeva, naznačen time što regulator tlaka (9) u koraku f) radi najviše 50%, po mogućnosti najviše 3% trajanja destiliranja.
13. Postupak u skladu s bilo kojim od prethodnih patentnih zahtjeva, naznačen time što se destiliranje provodi u spremniku, osobito u ISO spremniku.
14. Destilacijski sustav koji se sastoji od sustava spremnika (1) s kondenzator (3), otparivač (2) i parna komora (6) koja povezuje otparivač (2) i kondenzator (3) i miješanjem kombinira njihove pare, gdje parna komora (6) ima senzor za tlak (7), za mjerenje tlaka miješanja pm prisutnog u miješanoj pari u parnoj komori (6), senzor za temperaturu (8), za mjerenje temperature miješanja Tm prisutne u miješanoj pari u parnoj komori (6), a također i regulator tlaka (9), za destiliranje osnovnog materijala (4) postupkom u skladu s bilo kojim od prethodnih patentnih zahtjeva, gdje se sustav nalazi u spremniku (21), osobito u ISO spremniku, naznačen time što je destilacijski sustav integriran u spremnik (21) na takav način da dijelovi spremnika, osobito njegove stjenke, djeluju kao dijelovi sustava spremnika (1).
15. Destilacijski sustav u skladu s patentnim zahtjevom 14, naznačen time što spremnik (21) ima reaktorsko područje (22), u kojem se nalaze otparivač (2) i kondenzator (3), iznad potopljenog područja (23), u kojem se nalaze komponente relevantne za tlak, poput pumpi (9), ventila, senzora (7, 8) i prirubnica, kao i nadzorno područje (24) za elektronske komponente (25), koja je dostupno za rad i održavanje sustava.
16. Destilacijski sustav u skladu s bilo kojim od patentnih zahtjeva 14 ili 15, naznačen time što se više otparivača (2) i kondenzatora (3) stupnjeva s različitim tlakom i temperaturom nalazi u spremniku (21) i međusobno su povezani na
način koji omogućuje provođenje postupka.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH5472007 | 2007-04-04 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| HRP20120927T1 true HRP20120927T1 (hr) | 2012-12-31 |
Family
ID=38330229
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| HRP20120927AT HRP20120927T1 (hr) | 2007-04-04 | 2012-11-16 | Postupak destiliranja polaznog materijala i pogon za provedbu istog postupka |
Country Status (17)
| Country | Link |
|---|---|
| US (1) | US8617359B2 (hr) |
| EP (2) | EP2361659B1 (hr) |
| JP (1) | JP5589834B2 (hr) |
| KR (1) | KR101346401B1 (hr) |
| CN (1) | CN101663075B (hr) |
| AU (1) | AU2008235231B2 (hr) |
| BR (1) | BRPI0809444B1 (hr) |
| CY (1) | CY1113952T1 (hr) |
| ES (1) | ES2393286T3 (hr) |
| HK (1) | HK1141751A1 (hr) |
| HR (1) | HRP20120927T1 (hr) |
| IL (1) | IL200843A (hr) |
| MA (1) | MA31357B1 (hr) |
| MY (1) | MY148581A (hr) |
| PT (1) | PT2361659E (hr) |
| RU (1) | RU2459651C2 (hr) |
| WO (1) | WO2008122136A1 (hr) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2766170A1 (en) * | 2009-06-26 | 2010-12-29 | Gevo, Inc. | Recovery of higher alcohols from dilute aqueous solutions |
| CN104192925A (zh) * | 2014-07-30 | 2014-12-10 | 江苏河海新能源有限公司 | 蒸发冷凝系统及其应用 |
| CH710735A1 (de) | 2015-02-13 | 2016-08-15 | Thermal Purification Tech Ltd | Mehrstufige Destillationsanlage, Verfahren zum Betreiben einer solchen und Steuerung dafür. |
| CH712029A1 (de) | 2016-01-12 | 2017-07-14 | Thermal Purification Tech Ltd | Nieder-Temperatur-Destillationsanlage. |
| CN108046362B (zh) * | 2017-12-15 | 2021-03-26 | 鲁西化工集团股份有限公司煤化工分公司 | 一种高效耐蚀闪蒸分离设备 |
| CN110873622B (zh) * | 2018-09-03 | 2021-09-24 | 中国石油化工股份有限公司 | 测定固体物质饱和蒸气压的方法 |
| CN110170177A (zh) * | 2019-06-17 | 2019-08-27 | 江阴市欧姆机械设备有限公司 | 蒸发冷凝器 |
| WO2021105822A1 (en) * | 2019-11-25 | 2021-06-03 | King Abdullah University Of Science And Technology | Tubeless, multi-effect distillation system and method |
| CN112337123A (zh) * | 2021-01-04 | 2021-02-09 | 郑州长城科工贸有限公司 | 基于溶液饱和温度-压强关系自动蒸馏的方法及系统 |
| CN114890603A (zh) * | 2022-06-06 | 2022-08-12 | 嘉兴市中新医疗仪器有限公司 | 一种化工生产用高效蒸馏水装置 |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3218241A (en) * | 1960-01-26 | 1965-11-16 | Singmaster & Breyer Inc | Inhibiting scale formation in fresh water recovery |
| US4053368A (en) * | 1973-11-07 | 1977-10-11 | Battelle Memorial Institute | Process for the purification of water |
| US4302297A (en) * | 1977-05-24 | 1981-11-24 | Humiston Gerald F | Desalination apparatus with power generation |
| SU990247A1 (ru) * | 1980-11-26 | 1983-01-23 | Предприятие П/Я А-7815 | Устройство дл очистки жидкостей дистилл цией |
| SU1337108A1 (ru) * | 1985-09-12 | 1987-09-15 | Предприятие П/Я Г-4937 | Циркул ционный аппарат дл молекул рной дистилл ции |
| EP0563628B1 (de) | 1992-03-30 | 1996-09-11 | MEIER, René | Verfahren und Einrichtung zum Aufbereiten von Prozessabwasser mittels Vakuumdestillation mit indirekter Wärmerückgewinnung |
| DE4226487C1 (de) * | 1992-08-11 | 1994-01-27 | Noell Dbi Energie Entsorgung | Verfahren und Vorrichtung zur Zuführung von Klärschlamm in einen Reaktor zur thermischen Entsorgung |
| RU2082787C1 (ru) * | 1994-06-10 | 1997-06-27 | Государственный научный центр вирусологии и биотехнологии "Вектор" | Аппарат для разделения металлов дистилляцией в вакууме |
| US6004433A (en) * | 1997-02-03 | 1999-12-21 | L'air Liquide Societe Anonyme Pour L'etude Et L'exploitation Des Procedes George Claude | Purification of electronic specialty gases by vapor phase transfilling |
| AT409421B (de) | 1999-02-23 | 2002-08-26 | Wolf Systembau Gmbh & Co Kg | Verfahren und vorrichtung zum trocknen von feuchtigkeit enthaltenden produkten |
| DE19940992A1 (de) * | 1999-08-28 | 2001-03-01 | Joerg Korb | Frischwassererzeugungsanlage |
| JP2001276808A (ja) * | 2000-03-31 | 2001-10-09 | Onodera Kozaburo | 水の分離方法および水の分離装置 |
| JP2002023388A (ja) * | 2000-07-04 | 2002-01-23 | Casio Comput Co Ltd | 有機溶剤回収装置およびその装置を用いたパターン形成方法 |
| IL154139A0 (en) | 2000-07-27 | 2003-07-31 | Ips Gmbh | Device for distilling a medium |
| DE10100666A1 (de) | 2001-01-09 | 2002-07-11 | Alexander Von Poswik | Einrichtung zur dezentralen Gewinnung von Trinkwasser oder Brauchwasser |
| US7431806B2 (en) * | 2002-09-20 | 2008-10-07 | Lev Group, Llc | Low energy vacuum distillation method and apparatus |
| WO2004069370A1 (ja) | 2003-02-10 | 2004-08-19 | Sato, Chisato | 液体封止装置、液体封止減圧装置、この液体封止減圧装置を用いた蒸発装置、凝縮装置、不凝縮ガス除去装置、蒸発凝縮装置、熱エネルギ源分離装置、冷水製造装置、淡水化装置、および発電装置 |
| US7431805B2 (en) | 2003-12-03 | 2008-10-07 | Arizona Board Of Regents | Method and apparatus for simultaneous heat and mass transfer utilizing a carrier-gas at various absolute pressures |
| RU55766U1 (ru) * | 2006-04-20 | 2006-08-27 | Юрий Леопольдович Яковлев | Дистиллятор |
| HUE035231T2 (hu) * | 2007-04-04 | 2018-05-02 | Markus Lehmann | Eljárás nedves anyag kiszárítására |
-
2008
- 2008-04-01 ES ES11164665T patent/ES2393286T3/es active Active
- 2008-04-01 EP EP11164665A patent/EP2361659B1/de active Active
- 2008-04-01 JP JP2010501348A patent/JP5589834B2/ja not_active Expired - Fee Related
- 2008-04-01 AU AU2008235231A patent/AU2008235231B2/en active Active
- 2008-04-01 RU RU2009140746/05A patent/RU2459651C2/ru active
- 2008-04-01 CN CN2008800097391A patent/CN101663075B/zh active Active
- 2008-04-01 BR BRPI0809444-6A patent/BRPI0809444B1/pt active IP Right Grant
- 2008-04-01 KR KR1020097020236A patent/KR101346401B1/ko active IP Right Grant
- 2008-04-01 PT PT111646659T patent/PT2361659E/pt unknown
- 2008-04-01 EP EP08714793A patent/EP2139571A1/de not_active Withdrawn
- 2008-04-01 WO PCT/CH2008/000143 patent/WO2008122136A1/de active Application Filing
- 2008-04-01 MY MYPI20093967A patent/MY148581A/en unknown
- 2008-04-01 US US12/594,684 patent/US8617359B2/en active Active
-
2009
- 2009-09-10 IL IL200843A patent/IL200843A/en active IP Right Revival
- 2009-11-02 MA MA32317A patent/MA31357B1/fr unknown
-
2010
- 2010-09-02 HK HK10108330.0A patent/HK1141751A1/xx unknown
-
2012
- 2012-11-16 HR HRP20120927AT patent/HRP20120927T1/hr unknown
- 2012-11-21 CY CY20121101119T patent/CY1113952T1/el unknown
Also Published As
| Publication number | Publication date |
|---|---|
| JP5589834B2 (ja) | 2014-09-17 |
| IL200843A (en) | 2014-01-30 |
| IL200843A0 (en) | 2010-05-17 |
| PT2361659E (pt) | 2012-12-03 |
| CY1113952T1 (el) | 2016-07-27 |
| EP2361659A1 (de) | 2011-08-31 |
| JP2010523303A (ja) | 2010-07-15 |
| RU2459651C2 (ru) | 2012-08-27 |
| MA31357B1 (fr) | 2010-05-03 |
| KR101346401B1 (ko) | 2014-01-02 |
| US8617359B2 (en) | 2013-12-31 |
| WO2008122136A8 (de) | 2008-12-04 |
| EP2139571A1 (de) | 2010-01-06 |
| AU2008235231B2 (en) | 2012-08-30 |
| HK1141751A1 (en) | 2010-11-19 |
| ES2393286T3 (es) | 2012-12-20 |
| MY148581A (en) | 2013-04-30 |
| EP2361659B1 (de) | 2012-08-22 |
| RU2009140746A (ru) | 2011-05-10 |
| CN101663075A (zh) | 2010-03-03 |
| US20100163398A1 (en) | 2010-07-01 |
| BRPI0809444B1 (pt) | 2019-04-24 |
| CN101663075B (zh) | 2013-03-20 |
| BRPI0809444A2 (pt) | 2014-09-09 |
| WO2008122136A1 (de) | 2008-10-16 |
| AU2008235231A1 (en) | 2008-10-16 |
| KR20100014636A (ko) | 2010-02-10 |
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