HRP20120861T1 - Postupak pripreme triamida iz amonijaka i amidodiklorida - Google Patents
Postupak pripreme triamida iz amonijaka i amidodiklorida Download PDFInfo
- Publication number
- HRP20120861T1 HRP20120861T1 HRP20120861AT HRP20120861T HRP20120861T1 HR P20120861 T1 HRP20120861 T1 HR P20120861T1 HR P20120861A T HRP20120861A T HR P20120861AT HR P20120861 T HRP20120861 T HR P20120861T HR P20120861 T1 HRP20120861 T1 HR P20120861T1
- Authority
- HR
- Croatia
- Prior art keywords
- process according
- mixing
- triamide
- starting materials
- tubular reactor
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims 11
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 title claims 6
- 229910021529 ammonia Inorganic materials 0.000 title claims 3
- 238000002360 preparation method Methods 0.000 title claims 2
- 239000007858 starting material Substances 0.000 claims 4
- 239000011541 reaction mixture Substances 0.000 claims 2
- 239000000203 mixture Substances 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/22—Amides of acids of phosphorus
- C07F9/222—Amides of phosphoric acids
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/90—Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting the nitrification of ammonium compounds or urea in the soil
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Soil Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Claims (10)
1. Postupak pripreme triamida iz amonijaka i amido-diklorida, gdje se početni materijali međusobno miješaju i reagiraju, na način slobodnog povratnog miješanja (eng. back-mixing-free), i koncentracija amido-diklorida u miješalici je uvijek ispod 0.2 (mol/mol)% reakcijske smjese na temelju volumena reakcijske smjese.
2. Postupak prema zahtjevu 1, gdje je vrijeme miješanja početnih materijala manje od jedne sekunde.
3. Postupak prema jednom od zahtjeva 1 do 2, gdje se miješanje početnih materijala odvija pomoću mlaznice, rotor-stator miješalice, pumpe za miješanje reakcije ili mlazne miješalice s mlaznicom.
4. Postupak prema zahtjevu 3, gdje se smjesa prenosi u cijevni reaktor.
5. Postupak prema zahtjevu 4, gdje je cijevni reaktor izmjenjivač topline.
6. Postupak prema zahtjevu 4 ili 5, gdje se početni materijali hlade do ispod prije miješanja.
7. Postupak prema bilo kojem od zahtjeva 4 ili 5, gdje se, u cijevnom reaktoru, toplina reakcije gubi (disipira) isparavanjem amonijaka.
8. Postupak prema zahtjevu 4 ili 5, gdje se reakcijsko pražnjenje cijevnog reaktora prenosi na kolonu.
9. Postupak prema zahtjevu 7, gdje se triamid izvlači s dna kolone.
10. Postupak prema zahtjevu 8, gdje je triamid N-alkiltiofosforni triamid.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP08153960A EP2107064A1 (de) | 2008-04-02 | 2008-04-02 | Verfahren zur Herstellung von Triamiden aus Ammoniak und Amido-Dichloriden |
| PCT/EP2009/053577 WO2009121786A1 (de) | 2008-04-02 | 2009-03-26 | Verfahren zur herstellung von triamiden aus ammoniak und amido-dichloriden |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| HRP20120861T1 true HRP20120861T1 (hr) | 2012-11-30 |
Family
ID=39473390
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| HRP20120861AT HRP20120861T1 (hr) | 2008-04-02 | 2012-10-23 | Postupak pripreme triamida iz amonijaka i amidodiklorida |
Country Status (23)
| Country | Link |
|---|---|
| US (1) | US8088950B2 (hr) |
| EP (2) | EP2107064A1 (hr) |
| JP (1) | JP5562323B2 (hr) |
| CN (1) | CN101981040B (hr) |
| AU (1) | AU2009231421B2 (hr) |
| BR (1) | BRPI0909391B1 (hr) |
| CA (1) | CA2719304C (hr) |
| DK (1) | DK2262819T3 (hr) |
| EG (1) | EG26578A (hr) |
| ES (1) | ES2388710T3 (hr) |
| HR (1) | HRP20120861T1 (hr) |
| IL (1) | IL208288A (hr) |
| MA (1) | MA32255B1 (hr) |
| MX (1) | MX2010010644A (hr) |
| MY (1) | MY150292A (hr) |
| NZ (1) | NZ588244A (hr) |
| PL (1) | PL2262819T3 (hr) |
| PT (1) | PT2262819E (hr) |
| RU (1) | RU2491287C2 (hr) |
| SI (1) | SI2262819T1 (hr) |
| UA (1) | UA100153C2 (hr) |
| WO (1) | WO2009121786A1 (hr) |
| ZA (1) | ZA201007787B (hr) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8901344B2 (en) | 2008-12-16 | 2014-12-02 | Basf Se | Production of carboxylic acid esters by stripping with alcohol vapor |
| DE102009056566B4 (de) | 2009-12-03 | 2021-11-04 | Skw Stickstoffwerke Piesteritz Gmbh | Verfahren zur Herstellung von Phosphorsäuretriamiden in einer Eintopfreaktion |
| US8680323B2 (en) | 2010-01-19 | 2014-03-25 | Basf Se | Process for preparing isocyanates by thermal dissociation of carbamates |
| PL2687536T3 (pl) | 2012-07-18 | 2016-05-31 | Saltigo Gmbh | Sposób otrzymywania asymetrycznych triamidów kwasu (tio)fosforowego |
| EP2885261B1 (en) | 2012-08-15 | 2019-05-22 | Koch Agronomic Services, LLC | Liquid compositions containing urease inhibitors and glycol alkyl ethers |
| CN104736500A (zh) | 2012-08-15 | 2015-06-24 | 科氏农艺服务有限责任公司 | 含有脲酶抑制剂和芳基烷基醇的液体组合物 |
| EA031909B1 (ru) * | 2013-08-19 | 2019-03-29 | ДЖОРДЖИЯ-ПЭСИФИК КЕМИКАЛЗ ЭлЭлСи | Способы получения эмульгатора и буровой текучей среды |
| CN103524551B (zh) * | 2013-10-31 | 2014-06-18 | 江西吉翔医药化工有限公司 | 一种n-正丁基硫代磷酰三胺的连续化生产工艺 |
| CN104370957A (zh) * | 2014-10-28 | 2015-02-25 | 浙江奥复托化工有限公司 | 一种正丁基硫代磷酰三胺的微通道合成工艺 |
| EP3212592A1 (en) | 2014-10-31 | 2017-09-06 | Koch Agronomic Services, LLC | Nitrification inhibitor compositions and methods of making thereof |
| PL3356375T3 (pl) | 2015-10-01 | 2023-06-26 | Basf Se | Sposób odzyskiwania mieszaniny zawierającej pochodną kwasu (tio)fosforowego |
| CN105399767B (zh) * | 2015-11-20 | 2018-04-17 | 江西吉翔医药化工有限公司 | 一种n‑烃基取代磷酰三胺的生产方法 |
| CN105440073B (zh) * | 2015-11-20 | 2018-02-27 | 江西吉翔医药化工有限公司 | 一种n‑烃基硫代磷酰三胺的生产方法 |
| CN108290909B (zh) * | 2015-12-01 | 2021-06-01 | 巴斯夫欧洲公司 | 分离(硫代)磷酸衍生物的方法 |
| US10242994B2 (en) * | 2016-03-16 | 2019-03-26 | Sandisk Technologies Llc | Three-dimensional memory device containing annular etch-stop spacer and method of making thereof |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS512454B2 (hr) * | 1971-08-11 | 1976-01-26 | ||
| SU1839443A1 (ru) * | 1988-10-18 | 1995-07-09 | Институт Органической Химии Ан Усср | N`-бис-(этиленимино)фосфонил-n``-арилмочевины, обладающие антибластической активностью, n`-дихлорфосфонил-n``-арилмочевины для синтеза n`-бис-(этиленимино)фосфонил-n``-арилмочевин- и фторсодержащие анилины для синтеза n`-дихлорфосфонил-n``-арилмочевин |
| HUT64077A (en) * | 1990-02-08 | 1993-11-29 | Sapos Sa | Process for producing pyrimidinetrione derivatives |
| US5770771A (en) | 1997-01-21 | 1998-06-23 | Albemarle Corporation | Preparation of N-hydrocarbylthiophosphoric triamides |
| US5883297A (en) * | 1997-01-21 | 1999-03-16 | Albemarle Corporation | Preparation and recovery of N-hydrocarbylthiophosphoric triamides or N-hydrocarbylphosphoric triamides |
| US5955630A (en) | 1997-01-21 | 1999-09-21 | Albemarle Corporation | Recovery of N-hydrocarbylthiophosphoric triamides and N-hydrocarbylphosphoric triamides from reaction mixtures |
| CN1583767A (zh) * | 2004-06-08 | 2005-02-23 | 张雪崧 | 一种化学合成脂肪胺基磷酰三胺的方法 |
| DE102004035742A1 (de) * | 2004-07-23 | 2006-03-16 | Skw Stickstoffwerke Piesteritz Gmbh | N-Phenylphosphorsäuretriamide, Verfahren zu ihrer Herstellung und deren Verwendung als Mittel zur Regulierung bzw. Hemmung der enzymatischen Harnstoff-Hydrolyse |
| DE102005053541A1 (de) * | 2005-11-08 | 2007-05-10 | Basf Ag | Verfahren zur Herstellung von Thiophosphorsäuretriamiden |
| DE102005053540A1 (de) | 2005-11-08 | 2007-05-10 | Basf Ag | Verfahren zur Abtrennung von Säuren aus chemischen Reaktionsgemischen mit Hilfe unpolarer Amine |
| EP2056889A1 (de) | 2006-08-24 | 2009-05-13 | Basf Se | Verwendung von phosphorsäuretriamiden in toiletten |
| BRPI0716057A2 (pt) | 2006-08-24 | 2013-08-06 | Basf Se | composiÇço, dispositivo de dosagem, kit de partes, dispositivo de limpeza, e, uso dos mesmos |
-
2008
- 2008-04-02 EP EP08153960A patent/EP2107064A1/de not_active Withdrawn
-
2009
- 2009-03-26 MY MYPI2010004431A patent/MY150292A/en unknown
- 2009-03-26 ES ES09726930T patent/ES2388710T3/es active Active
- 2009-03-26 UA UAA201012979A patent/UA100153C2/ru unknown
- 2009-03-26 PT PT09726930T patent/PT2262819E/pt unknown
- 2009-03-26 RU RU2010144598/04A patent/RU2491287C2/ru active
- 2009-03-26 US US12/935,934 patent/US8088950B2/en active Active
- 2009-03-26 CN CN200980111468.5A patent/CN101981040B/zh active Active
- 2009-03-26 EP EP09726930A patent/EP2262819B1/de active Active
- 2009-03-26 JP JP2011502346A patent/JP5562323B2/ja active Active
- 2009-03-26 AU AU2009231421A patent/AU2009231421B2/en active Active
- 2009-03-26 BR BRPI0909391-5A patent/BRPI0909391B1/pt active IP Right Grant
- 2009-03-26 SI SI200930376T patent/SI2262819T1/sl unknown
- 2009-03-26 MX MX2010010644A patent/MX2010010644A/es active IP Right Grant
- 2009-03-26 CA CA2719304A patent/CA2719304C/en active Active
- 2009-03-26 PL PL09726930T patent/PL2262819T3/pl unknown
- 2009-03-26 DK DK09726930.2T patent/DK2262819T3/da active
- 2009-03-26 WO PCT/EP2009/053577 patent/WO2009121786A1/de active Application Filing
- 2009-03-26 NZ NZ588244A patent/NZ588244A/en unknown
-
2010
- 2010-09-21 IL IL208288A patent/IL208288A/en active IP Right Grant
- 2010-09-30 EG EG2010091653A patent/EG26578A/en active
- 2010-10-28 MA MA33289A patent/MA32255B1/fr unknown
- 2010-11-01 ZA ZA2010/07787A patent/ZA201007787B/en unknown
-
2012
- 2012-10-23 HR HRP20120861AT patent/HRP20120861T1/hr unknown
Also Published As
| Publication number | Publication date |
|---|---|
| MA32255B1 (fr) | 2011-04-01 |
| ZA201007787B (en) | 2012-01-25 |
| ES2388710T3 (es) | 2012-10-17 |
| WO2009121786A1 (de) | 2009-10-08 |
| EG26578A (en) | 2014-03-10 |
| PL2262819T3 (pl) | 2013-01-31 |
| MX2010010644A (es) | 2010-11-05 |
| EP2262819B1 (de) | 2012-08-08 |
| AU2009231421A1 (en) | 2009-10-08 |
| RU2491287C2 (ru) | 2013-08-27 |
| UA100153C2 (ru) | 2012-11-26 |
| BRPI0909391A2 (pt) | 2015-12-15 |
| NZ588244A (en) | 2012-03-30 |
| PT2262819E (pt) | 2012-09-06 |
| US8088950B2 (en) | 2012-01-03 |
| CN101981040B (zh) | 2014-07-02 |
| IL208288A (en) | 2013-11-28 |
| AU2009231421B2 (en) | 2014-03-13 |
| CA2719304C (en) | 2016-09-06 |
| DK2262819T3 (da) | 2012-11-19 |
| BRPI0909391B1 (pt) | 2017-11-14 |
| JP2011516446A (ja) | 2011-05-26 |
| RU2010144598A (ru) | 2012-05-10 |
| CN101981040A (zh) | 2011-02-23 |
| SI2262819T1 (sl) | 2012-12-31 |
| IL208288A0 (en) | 2010-12-30 |
| MY150292A (en) | 2013-12-31 |
| EP2107064A1 (de) | 2009-10-07 |
| CA2719304A1 (en) | 2009-10-08 |
| EP2262819A1 (de) | 2010-12-22 |
| US20110028761A1 (en) | 2011-02-03 |
| JP5562323B2 (ja) | 2014-07-30 |
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