GB975914A - Sulphonation of organic compounds - Google Patents
Sulphonation of organic compoundsInfo
- Publication number
- GB975914A GB975914A GB19157/61A GB1915761A GB975914A GB 975914 A GB975914 A GB 975914A GB 19157/61 A GB19157/61 A GB 19157/61A GB 1915761 A GB1915761 A GB 1915761A GB 975914 A GB975914 A GB 975914A
- Authority
- GB
- United Kingdom
- Prior art keywords
- zone
- orifice
- mixture
- sulphonation
- lower pressure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000002894 organic compounds Chemical class 0.000 title abstract 3
- -1 aliphatic alcohols Chemical class 0.000 abstract 6
- AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Chemical compound O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 abstract 6
- 239000000203 mixture Substances 0.000 abstract 4
- 239000011261 inert gas Substances 0.000 abstract 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 abstract 2
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 abstract 2
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 abstract 2
- 235000014113 dietary fatty acids Nutrition 0.000 abstract 2
- KWKXNDCHNDYVRT-UHFFFAOYSA-N dodecylbenzene Chemical compound CCCCCCCCCCCCC1=CC=CC=C1 KWKXNDCHNDYVRT-UHFFFAOYSA-N 0.000 abstract 2
- 229930195729 fatty acid Natural products 0.000 abstract 2
- 239000000194 fatty acid Substances 0.000 abstract 2
- 150000004665 fatty acids Chemical class 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 125000000913 palmityl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 abstract 2
- XFRVVPUIAFSTFO-UHFFFAOYSA-N 1-Tridecanol Chemical compound CCCCCCCCCCCCCO XFRVVPUIAFSTFO-UHFFFAOYSA-N 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 abstract 1
- 239000005977 Ethylene Substances 0.000 abstract 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 abstract 1
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 abstract 1
- 239000003570 air Substances 0.000 abstract 1
- 125000003118 aryl group Chemical group 0.000 abstract 1
- 239000001569 carbon dioxide Substances 0.000 abstract 1
- 229910002092 carbon dioxide Inorganic materials 0.000 abstract 1
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 239000007859 condensation product Substances 0.000 abstract 1
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 abstract 1
- 239000007789 gas Substances 0.000 abstract 1
- 239000008246 gaseous mixture Substances 0.000 abstract 1
- 229930195733 hydrocarbon Natural products 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 abstract 1
- 239000006193 liquid solution Substances 0.000 abstract 1
- 239000006194 liquid suspension Substances 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 229910052757 nitrogen Inorganic materials 0.000 abstract 1
- 150000004671 saturated fatty acids Chemical class 0.000 abstract 1
- 235000003441 saturated fatty acids Nutrition 0.000 abstract 1
- 239000002002 slurry Substances 0.000 abstract 1
- 239000004291 sulphur dioxide Substances 0.000 abstract 1
- 235000010269 sulphur dioxide Nutrition 0.000 abstract 1
- 229940087291 tridecyl alcohol Drugs 0.000 abstract 1
- 239000008096 xylene Substances 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B45/00—Formation or introduction of functional groups containing sulfur
- C07B45/02—Formation or introduction of functional groups containing sulfur of sulfo or sulfonyldioxy groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
- C07C303/04—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups
- C07C303/06—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups by reaction with sulfuric acid or sulfur trioxide
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00162—Controlling or regulating processes controlling the pressure
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (10)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
NL278901D NL278901A (enrdf_load_stackoverflow) | 1961-05-26 | ||
BE617968D BE617968A (enrdf_load_stackoverflow) | 1961-05-26 | ||
GB19157/61A GB975914A (en) | 1961-05-26 | 1961-05-26 | Sulphonation of organic compounds |
ES277408A ES277408A1 (es) | 1961-05-26 | 1962-05-17 | Un procedimiento para sulfonar un compuesto orgánico |
DEC27021A DE1179196B (de) | 1961-05-26 | 1962-05-18 | Verfahren und Vorrichtung zum Sulfonieren und Sulfatieren von organischen Verbindungen |
CH623762A CH401031A (de) | 1961-05-26 | 1962-05-23 | Verfahren zum Sulfonieren organischer Verbindungen und Vorrichtung zur Durchführung des Verfahrens |
US197508A US3270038A (en) | 1961-05-26 | 1962-05-24 | Sulphonation of organic compounds |
FR898594A FR1330937A (fr) | 1961-05-26 | 1962-05-24 | Procédé et appareil pour la sulfonation des composés organiques |
DK238262AA DK117825B (da) | 1961-05-26 | 1962-05-26 | Fremgangsmåde og apparat til sulfonering eller sulfatering af en organisk forbindelse. |
ES280186A ES280186A1 (es) | 1961-05-26 | 1962-08-22 | Un aparato para sulforar un compuesto orgánico |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB19157/61A GB975914A (en) | 1961-05-26 | 1961-05-26 | Sulphonation of organic compounds |
Publications (1)
Publication Number | Publication Date |
---|---|
GB975914A true GB975914A (en) | 1964-11-25 |
Family
ID=10124710
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB19157/61A Expired GB975914A (en) | 1961-05-26 | 1961-05-26 | Sulphonation of organic compounds |
Country Status (9)
Country | Link |
---|---|
US (1) | US3270038A (enrdf_load_stackoverflow) |
BE (1) | BE617968A (enrdf_load_stackoverflow) |
CH (1) | CH401031A (enrdf_load_stackoverflow) |
DE (1) | DE1179196B (enrdf_load_stackoverflow) |
DK (1) | DK117825B (enrdf_load_stackoverflow) |
ES (2) | ES277408A1 (enrdf_load_stackoverflow) |
FR (1) | FR1330937A (enrdf_load_stackoverflow) |
GB (1) | GB975914A (enrdf_load_stackoverflow) |
NL (1) | NL278901A (enrdf_load_stackoverflow) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2155474A (en) * | 1984-03-13 | 1985-09-25 | Procter & Gamble | Process for the continuous reaction of organic compounds with sulfur trioxide |
US5085846A (en) * | 1990-04-12 | 1992-02-04 | Albright & Wilson Limited | Process for producing phosphorous acid |
Families Citing this family (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3412143A (en) * | 1965-06-21 | 1968-11-19 | Pillsbury Co | Process for the production of amine salts of sulfamic acid |
US3535339A (en) * | 1965-12-17 | 1970-10-20 | Procter & Gamble | Process and apparatus for the continuous reaction of organic compounds with undiluted sulfur trioxide |
US3482947A (en) * | 1966-07-14 | 1969-12-09 | Procter & Gamble | Feed device for a film reactor |
GB1223255A (en) * | 1967-04-25 | 1971-02-24 | Marchon Products Ltd | Sulphation process |
GB1229477A (enrdf_load_stackoverflow) * | 1967-06-26 | 1971-04-21 | ||
US3931273A (en) * | 1970-02-23 | 1976-01-06 | Costruzioni Meccaniche G. Mazzoni S.P.A. | Method for sulphonatizing and sulphatizing organic compounds with sulphur trioxide and apparatus therefor |
GB1434020A (en) * | 1972-10-30 | 1976-04-28 | Koebner A | Sulphonation of aromatic compounds in the presence of solvents |
US4144266A (en) * | 1973-07-05 | 1979-03-13 | Marathon Oil Company | Sulfonation of crude oils to produce petroleum sulfonates |
US4614623A (en) * | 1974-01-04 | 1986-09-30 | Marathon Oil Company | Sulfonation of crude oils with gaseous SO3 to produce petroleum sulfonates |
US4390474A (en) * | 1974-10-16 | 1983-06-28 | Stepan Chemical Company | Sulfonation petroleum composition |
DE2502254C2 (de) * | 1975-01-17 | 1983-08-04 | Marathon Oil Co., 45840 Findlay, Ohio | Verfahren zur Herstellung einwertige Kationen enthaltender Erdölsulfonate |
GB1563994A (en) * | 1975-05-15 | 1980-04-02 | Albright & Wilson | Sulph(on)ation process and mixer |
US4097242A (en) * | 1975-07-21 | 1978-06-27 | Kao Soap Co., Ltd. | Sulfonation apparatus |
US4002431A (en) * | 1975-12-19 | 1977-01-11 | United Technologies Corporation | Nitrous oxide decomposition reactor |
US4113438A (en) * | 1976-05-27 | 1978-09-12 | The Chemithon Corporation | Sulfonating apparatus |
JPS6045185B2 (ja) * | 1976-11-17 | 1985-10-08 | 丸善石油株式会社 | 芳香族化合物のスルホン化方法 |
US4560517A (en) * | 1979-03-22 | 1985-12-24 | Marathon Oil Company | Sulfonation of crude oils with gaseous SO3 to produce petroleum sulfonates |
JPS6033382B2 (ja) * | 1979-07-06 | 1985-08-02 | ライオン株式会社 | アルキルベンゼンの薄膜式スルホン化法 |
US4980087A (en) * | 1986-01-15 | 1990-12-25 | Sandoz Ltd. | Ether sulfates of a mixture of branched 1-decanols |
US4879399A (en) * | 1986-01-15 | 1989-11-07 | Sandoz Ltd. | Ether sulfates of a mixture of branched 1-decanols |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2371284A (en) * | 1945-03-13 | Preparation of sulphated fatty | ||
NL27274C (enrdf_load_stackoverflow) * | ||||
US2174760A (en) * | 1934-04-19 | 1939-10-03 | Ig Farbenindustrie Ag | Condensation products derived from carboxylic acids and method of producing them |
US2290167A (en) * | 1939-08-14 | 1942-07-21 | Solvay Process Co | Preparation of sulphonation derivatives |
US2634287A (en) * | 1948-04-01 | 1953-04-07 | Monsanto Chemicals | Process for sulfation of aliphatic alcohols |
DE834245C (de) * | 1948-07-17 | 1952-03-17 | Innovations Chimiques Sinnova | Verfahren und Vorrichtung zur kontinuierlichen Sulfonierung bzw. Veresterung organischer Verbindungen mittels Chlorsulfonsaeure |
US2665197A (en) * | 1950-08-03 | 1954-01-05 | Rowland Ernest Edward | Polymerization control apparatus |
US2730433A (en) * | 1954-11-02 | 1956-01-10 | Du Pont | Spray mixer |
US2872297A (en) * | 1955-01-11 | 1959-02-03 | Flo Mix Fertilizers Corp | Apparatus for converting liquid anhydrous ammonia to aqua ammonia |
GB791995A (en) * | 1956-07-17 | 1958-03-19 | Shell Res Ltd | Sulphonation of organic liquids |
DE1095817B (de) * | 1956-07-17 | 1960-12-29 | Iashellia Res Ltd | Kontinuierliches Verfahren und Vorrichtung zum Sulfonieren von mit Schwefeltrioxyd sulfonierbaren organischen Fluessigkeiten |
US2828331A (en) * | 1956-09-26 | 1958-03-25 | Pure Oil Co | Sulfonation of petroleum oils |
US2923728A (en) * | 1957-11-19 | 1960-02-02 | Du Pont | Process of reacting organic compounds with sulfur trioxide |
-
0
- BE BE617968D patent/BE617968A/xx unknown
- NL NL278901D patent/NL278901A/xx unknown
-
1961
- 1961-05-26 GB GB19157/61A patent/GB975914A/en not_active Expired
-
1962
- 1962-05-17 ES ES277408A patent/ES277408A1/es not_active Expired
- 1962-05-18 DE DEC27021A patent/DE1179196B/de active Pending
- 1962-05-23 CH CH623762A patent/CH401031A/de unknown
- 1962-05-24 FR FR898594A patent/FR1330937A/fr not_active Expired
- 1962-05-24 US US197508A patent/US3270038A/en not_active Expired - Lifetime
- 1962-05-26 DK DK238262AA patent/DK117825B/da unknown
- 1962-08-22 ES ES280186A patent/ES280186A1/es not_active Expired
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2155474A (en) * | 1984-03-13 | 1985-09-25 | Procter & Gamble | Process for the continuous reaction of organic compounds with sulfur trioxide |
US5085846A (en) * | 1990-04-12 | 1992-02-04 | Albright & Wilson Limited | Process for producing phosphorous acid |
Also Published As
Publication number | Publication date |
---|---|
ES280186A1 (es) | 1962-11-16 |
CH401031A (de) | 1965-10-31 |
ES277408A1 (es) | 1962-12-01 |
DK117825B (da) | 1970-06-08 |
NL278901A (enrdf_load_stackoverflow) | |
FR1330937A (fr) | 1963-06-28 |
BE617968A (enrdf_load_stackoverflow) | |
DE1179196B (de) | 1964-10-08 |
US3270038A (en) | 1966-08-30 |
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