GB858058A - Method and apparatus for accomplishing exothermic reactions in continuous manner as,but not exclusively for sulphonations, nitrations and the like - Google Patents
Method and apparatus for accomplishing exothermic reactions in continuous manner as,but not exclusively for sulphonations, nitrations and the likeInfo
- Publication number
- GB858058A GB858058A GB11555/57A GB1155557A GB858058A GB 858058 A GB858058 A GB 858058A GB 11555/57 A GB11555/57 A GB 11555/57A GB 1155557 A GB1155557 A GB 1155557A GB 858058 A GB858058 A GB 858058A
- Authority
- GB
- United Kingdom
- Prior art keywords
- mixture
- pipes
- reaction
- main body
- mixed
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
- B01F23/43—Mixing liquids with liquids; Emulsifying using driven stirrers
- B01F23/431—Mixing liquids with liquids; Emulsifying using driven stirrers the liquids being introduced from the outside through or along the axis of a rotating stirrer, e.g. the stirrer rotating due to the reaction of the introduced liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/80—Mixing plants; Combinations of mixers
- B01F33/81—Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
- B01J19/1881—Stationary reactors having moving elements inside resulting in a loop-type movement externally, i.e. the mixture leaving the vessel and subsequently re-entering it
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00083—Coils
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/18—Details relating to the spatial orientation of the reactor
- B01J2219/185—Details relating to the spatial orientation of the reactor vertical
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
In the sulphonation of hydrocarbons, alcohols, acids and phenols in a continuous process using oleum or SO3, the two reactants are separately pre-mixed with a part of the reaction product, and the reagent mixture then admitted to the main body of the reactant mixture at spaced points and rapidly dispersed therein. By this means the heat of reaction is limited and controlled. Suitable apparatus is described.ALSO:In exothermic reactions, e.g. the nitration or sulphonation of organic compounds, two reagents are separately pre-mixed with a part of the reaction product before admission at two spaced points in the main body of the reaction mixture. A vessel 1, Fig. 1, having a cooling jacket 2 is connected to two premixing vessels 6, 7, to which reaction product <PICT:0858058/III/1> from vessel 1 is pumped through pipes 10, 11 to the pre-mixers, and to which two proportioned reagents are added through pipes 8, 9. The pre-mixed diluted reagents flow through pipes 4, 5 and impinge on inclined blades 20 of a rotating dispersing element 16. Dispersion is assisted by a stirrer 17, and circulation is guided by a cooling coil 3. An annula ring 23 maintains the surface of the liquid mixture quiescent at the level of the discharge 22. In a modification (not shown) of the apparatus where one reactant is a gas, the pre-mixing chamber forms a cup-shaped chamber in the upper part of the reactor in which a dispersing member similar to element 16 above is mounted, above which a fan forces the gas into admixture with the reaction mixture fed to the dispersing element. The mixture is drawn down a central tube into the main body of the reaction mixture and unabsorbed gas is recirculated.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT858058X | 1956-09-04 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB858058A true GB858058A (en) | 1961-01-04 |
Family
ID=11329798
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB11555/57A Expired GB858058A (en) | 1956-09-04 | 1957-04-09 | Method and apparatus for accomplishing exothermic reactions in continuous manner as,but not exclusively for sulphonations, nitrations and the like |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB858058A (en) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4640832A (en) * | 1984-10-06 | 1987-02-03 | Degussa Aktiengesellschaft | Process for the production of sodium polysulfides from the elements sodium and sulfur |
| US4891207A (en) * | 1983-12-10 | 1990-01-02 | Broome Andrew D J | Manufacture of arsenic acid |
| CN104399398A (en) * | 2014-11-30 | 2015-03-11 | 南京威安新材料科技有限公司 | Catalyst processing emulsifying machine capable of improving homogenizing uniformity |
| CN104984707A (en) * | 2015-06-16 | 2015-10-21 | 镇江港和新型建材有限公司 | Material reaction device |
| CN110449103A (en) * | 2019-07-29 | 2019-11-15 | 浙江迪邦化工有限公司 | A kind of integration system of band premix for diazonium salt method and apparatus |
| CN112853365A (en) * | 2020-12-31 | 2021-05-28 | 苏州博睿特环保科技有限公司 | Novel oil removing material and preparation equipment thereof |
| CN113578178A (en) * | 2021-09-29 | 2021-11-02 | 山东淇水环保科技有限公司 | Seawater chemical dosing premixing device for marine ecological management |
| GB2599890A (en) * | 2020-08-18 | 2022-04-20 | Ashe Robert | Improved loop reactor |
| CN116586023A (en) * | 2023-07-19 | 2023-08-15 | 山东齐发化工有限公司 | Alkylation reaction device and method thereof |
| CN118122191A (en) * | 2024-05-06 | 2024-06-04 | 安徽理士新能源发展有限公司 | Lithium ion battery slurry processing and conveying integrated system and use method |
-
1957
- 1957-04-09 GB GB11555/57A patent/GB858058A/en not_active Expired
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4891207A (en) * | 1983-12-10 | 1990-01-02 | Broome Andrew D J | Manufacture of arsenic acid |
| US4640832A (en) * | 1984-10-06 | 1987-02-03 | Degussa Aktiengesellschaft | Process for the production of sodium polysulfides from the elements sodium and sulfur |
| CN104399398A (en) * | 2014-11-30 | 2015-03-11 | 南京威安新材料科技有限公司 | Catalyst processing emulsifying machine capable of improving homogenizing uniformity |
| CN104984707A (en) * | 2015-06-16 | 2015-10-21 | 镇江港和新型建材有限公司 | Material reaction device |
| CN110449103A (en) * | 2019-07-29 | 2019-11-15 | 浙江迪邦化工有限公司 | A kind of integration system of band premix for diazonium salt method and apparatus |
| CN110449103B (en) * | 2019-07-29 | 2021-06-01 | 浙江迪邦化工有限公司 | Method and device for integrally preparing diazonium salt with premixing function |
| GB2599890A (en) * | 2020-08-18 | 2022-04-20 | Ashe Robert | Improved loop reactor |
| CN112853365A (en) * | 2020-12-31 | 2021-05-28 | 苏州博睿特环保科技有限公司 | Novel oil removing material and preparation equipment thereof |
| CN113578178A (en) * | 2021-09-29 | 2021-11-02 | 山东淇水环保科技有限公司 | Seawater chemical dosing premixing device for marine ecological management |
| CN116586023A (en) * | 2023-07-19 | 2023-08-15 | 山东齐发化工有限公司 | Alkylation reaction device and method thereof |
| CN116586023B (en) * | 2023-07-19 | 2023-09-08 | 山东齐发化工有限公司 | Alkylation reaction device and method thereof |
| CN118122191A (en) * | 2024-05-06 | 2024-06-04 | 安徽理士新能源发展有限公司 | Lithium ion battery slurry processing and conveying integrated system and use method |
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