GB941746A - Process for the concentration and desalting of dilute, saltcontaining sulphuric acid - Google Patents

Process for the concentration and desalting of dilute, saltcontaining sulphuric acid

Info

Publication number
GB941746A
GB941746A GB3581361A GB3581361A GB941746A GB 941746 A GB941746 A GB 941746A GB 3581361 A GB3581361 A GB 3581361A GB 3581361 A GB3581361 A GB 3581361A GB 941746 A GB941746 A GB 941746A
Authority
GB
United Kingdom
Prior art keywords
acid
concentrated
amount
dilute
evaporator
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB3581361A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer AG
Original Assignee
Bayer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer AG filed Critical Bayer AG
Publication of GB941746A publication Critical patent/GB941746A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/69Sulfur trioxide; Sulfuric acid
    • C01B17/88Concentration of sulfuric acid

Abstract

Sulphuric acid is concentrated and desalted by admission of dilute acid to an evaporator, continuous removal of the acidic suspension, and filtering off the salts from the concentrated acid and partial recycling of the concentrated acid to the dilute initial acid solution, characterized in that the amount of concentrated acid recycled to the dilute acid is such that the salt content of the suspension in the evaporator does not amount to more than about 1000 grams per litre. An acid containing 16-22% H2SO4 may be concentrated to 63-68% H2SO4, and the salt concentration in the evaporator preferably does not exceed 700-900 grams per litre. The amount of acid added to the salt solution is equal to the amount of salt suspension drawn off from the evaporator. Salts referred to are: ferrous sulphate and sulphates generally.ALSO:Sulphuric acid is concentrated and desalted by admission of dilute acid to an evaporator, continuous removal of the acidic suspension, and filtering off the salts from the concentrated acid and partial recycling of the concentrated acid to the dilute initial acid solution, characterized in that the amount of concentrated acid recycled to the dilute acid is such that the salt content of the suspension in the evaporation does not amount to more than about 1000 grams per litre. An acid containing 16-22% by weight H2SO4 may be concentrated to 63-68% H2SO4, and the amount of solid material in the evaporation should preferably not exceed 700-900 grams per litre. The amount of acid added to the salt solution is equal to the amount of salt suspension drawn off from the evaporator. Salts referred to are: ferrous sulphate and sulphates generally.
GB3581361A 1960-10-14 1961-10-04 Process for the concentration and desalting of dilute, saltcontaining sulphuric acid Expired GB941746A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEF32340A DE1131193B (en) 1960-10-14 1960-10-14 Process for concentrating and desalting dilute, salty sulfuric acid

Publications (1)

Publication Number Publication Date
GB941746A true GB941746A (en) 1963-11-13

Family

ID=7094591

Family Applications (1)

Application Number Title Priority Date Filing Date
GB3581361A Expired GB941746A (en) 1960-10-14 1961-10-04 Process for the concentration and desalting of dilute, saltcontaining sulphuric acid

Country Status (3)

Country Link
BE (1) BE608729A (en)
DE (1) DE1131193B (en)
GB (1) GB941746A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2618122A1 (en) * 1976-04-26 1977-11-10 Kronos Titan Gmbh Sulphuric acid mfr. by two stage concentration - and removal of pptd. metal salts
FR2403973A1 (en) * 1977-09-21 1979-04-20 Montedison Spa PROCESS FOR CONCENTRATION OF AQUEOUS SOLUTIONS OF SULFURIC ACID

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2618121A1 (en) * 1976-04-26 1977-11-10 Kronos Titan Gmbh Sulphuric acid demetallisation in titanium dioxide pigment mfr. - by continuous addn. to metal salt suspension in conc. acid and evapn.
DE2729756A1 (en) * 1977-07-01 1979-01-11 Kronos Titan Gmbh CONCN. AND PURIFICN. OF SULPHURIC ACID FROM TITANIUM DI:OXIDE MFR. - by boiling in presence of ferrous sulphate to remove chromium
CN108562107B (en) * 2018-03-30 2021-07-23 海尔智家股份有限公司 Refrigerator with a door

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2618122A1 (en) * 1976-04-26 1977-11-10 Kronos Titan Gmbh Sulphuric acid mfr. by two stage concentration - and removal of pptd. metal salts
FR2403973A1 (en) * 1977-09-21 1979-04-20 Montedison Spa PROCESS FOR CONCENTRATION OF AQUEOUS SOLUTIONS OF SULFURIC ACID

Also Published As

Publication number Publication date
BE608729A (en) 1962-02-01
DE1131193B (en) 1962-06-14

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