GB874070A - Process for the production of n -sulphanilyl-n-butyl urea - Google Patents
Process for the production of n -sulphanilyl-n-butyl ureaInfo
- Publication number
- GB874070A GB874070A GB34362/59A GB3436259A GB874070A GB 874070 A GB874070 A GB 874070A GB 34362/59 A GB34362/59 A GB 34362/59A GB 3436259 A GB3436259 A GB 3436259A GB 874070 A GB874070 A GB 874070A
- Authority
- GB
- United Kingdom
- Prior art keywords
- sulphanilyl
- urea
- butylamine
- production
- boiling point
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/087—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
N-Sulphanilyl-N1-butyl urea is prepared by reacting N-sulphanilyl urea with butylamine in a molar ratio of 1:1.2 and in a ketone solvent having a boiling point within the range of 90 to 120 DEG C., the ammonia split off during the reaction being removed as quickly as possible from the reaction mixture by first stirring the reactants together until a salt is formed between the N-sulphanilyl urea and the butylamine, then rapidly heating the reaction mixture to the boiling point and continuing boiling until after complete solution has been obtained. The ketone solvent may be a mixture of ketones and is preferably insoluble or only slightly insoluble in water. The use of methyl isobutyl ketone is exemplified.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH874070X | 1959-04-07 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB874070A true GB874070A (en) | 1961-08-02 |
Family
ID=4544263
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB34362/59A Expired GB874070A (en) | 1959-04-07 | 1959-10-09 | Process for the production of n -sulphanilyl-n-butyl urea |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB874070A (en) |
-
1959
- 1959-10-09 GB GB34362/59A patent/GB874070A/en not_active Expired
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