GB853919A - Method for controlling the thickness and crystalline grain structure of phosphate coatings formed upon metallic surfaces - Google Patents

Method for controlling the thickness and crystalline grain structure of phosphate coatings formed upon metallic surfaces

Info

Publication number
GB853919A
GB853919A GB670359A GB670359A GB853919A GB 853919 A GB853919 A GB 853919A GB 670359 A GB670359 A GB 670359A GB 670359 A GB670359 A GB 670359A GB 853919 A GB853919 A GB 853919A
Authority
GB
United Kingdom
Prior art keywords
chlorate
solution
unaccelerated
concentration
coating
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB670359A
Inventor
Ferdinand Philip Heller
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel Corp
Original Assignee
Amchem Products Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Amchem Products Inc filed Critical Amchem Products Inc
Priority to GB670359A priority Critical patent/GB853919A/en
Publication of GB853919A publication Critical patent/GB853919A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/73Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals characterised by the process
    • C23C22/77Controlling or regulating of the coating process

Landscapes

  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Chemical Treatment Of Metals (AREA)

Abstract

The thickness of coatings formed on metallic surfaces by chlorate-accelerated heavy-metal phosphate coating solutions under constant conditions of time and temperature is controlled by varying the concentration of chlorate present in the otherwise constant solution in inverse logarithmic proportion to the thickness of coating desired. The grain size of the coating is simultaneously controlled since the coarseness thereof similarly varies as an invere logarithmic function of the chlorate concentration. Where the coatings are formed by dipping, the chlorate concentration may be varied by injecting additional amounts of the chlorate or of the unaccelerated ingredients into the bath. Where the coatings are formed by spraying, the chlorate concentration may be varied by (a) injecting the required amount thereof into the pipeline feeding unaccelerated solution to the spray nozzles, (b) using separate spray nozzles for a solution of the accelerator and for the unaccelerated solution, or (c) using separate spray nozzles for the unaccelerated solution and for the same solution containing the maximum desired chlorate concentration. The example relates to the coating of steel panels using a sodium chlorate accelerated zinc phosphate solution.
GB670359A 1959-02-26 1959-02-26 Method for controlling the thickness and crystalline grain structure of phosphate coatings formed upon metallic surfaces Expired GB853919A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB670359A GB853919A (en) 1959-02-26 1959-02-26 Method for controlling the thickness and crystalline grain structure of phosphate coatings formed upon metallic surfaces

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB670359A GB853919A (en) 1959-02-26 1959-02-26 Method for controlling the thickness and crystalline grain structure of phosphate coatings formed upon metallic surfaces

Publications (1)

Publication Number Publication Date
GB853919A true GB853919A (en) 1960-11-09

Family

ID=9819242

Family Applications (1)

Application Number Title Priority Date Filing Date
GB670359A Expired GB853919A (en) 1959-02-26 1959-02-26 Method for controlling the thickness and crystalline grain structure of phosphate coatings formed upon metallic surfaces

Country Status (1)

Country Link
GB (1) GB853919A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113426600A (en) * 2021-07-09 2021-09-24 飞荣达科技(江苏)有限公司 Method for controlling flux coating amount of brazing liquid cold plate

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113426600A (en) * 2021-07-09 2021-09-24 飞荣达科技(江苏)有限公司 Method for controlling flux coating amount of brazing liquid cold plate
CN113426600B (en) * 2021-07-09 2024-03-19 飞荣达科技(江苏)有限公司 Control method for brazing flux coating amount of brazing liquid cooling plate

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