GB801415A - Production of titanium tetraiodide - Google Patents

Production of titanium tetraiodide

Info

Publication number
GB801415A
GB801415A GB25934/56A GB2593456A GB801415A GB 801415 A GB801415 A GB 801415A GB 25934/56 A GB25934/56 A GB 25934/56A GB 2593456 A GB2593456 A GB 2593456A GB 801415 A GB801415 A GB 801415A
Authority
GB
United Kingdom
Prior art keywords
titanium tetrachloride
titanium
hydrogen iodide
iodide
tetraiodide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB25934/56A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Monsanto Chemicals Ltd
Monsanto Chemical Co
Original Assignee
Monsanto Chemicals Ltd
Monsanto Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Monsanto Chemicals Ltd, Monsanto Chemical Co filed Critical Monsanto Chemicals Ltd
Publication of GB801415A publication Critical patent/GB801415A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/02—Halides of titanium

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Titanium tetraiodide and by-product hydrogen chloride are prepared by treating liquid titanium tetrachloride with hydrogen iodide, the amount of hydrogen iodide being insufficient to utilize the whole of the titanium tetrachloride employed. The hydrogen iodide may be passed into liquid titanium tetrachloride such that the ratio of iodide to titanium does not reach 4, and preferably does not reach 3, or the hydrogen iodide and titanium tetrachloride may be added to a bath of titanium tetrachloride in mol. ratio of 4 : 1, or the titanium tetrachloride is passed downward in countercurrent to hydrogen iodide. The reaction temperature is preferably maintained between 10 DEG and 40 DEG C. and especially between 20 DEG and 30 DEG C. The titanium tetraiodide product may be separated by crystallization or by fractional distillation.
GB25934/56A 1955-08-24 1956-08-24 Production of titanium tetraiodide Expired GB801415A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US801415XA 1955-08-24 1955-08-24

Publications (1)

Publication Number Publication Date
GB801415A true GB801415A (en) 1958-09-10

Family

ID=22155514

Family Applications (1)

Application Number Title Priority Date Filing Date
GB25934/56A Expired GB801415A (en) 1955-08-24 1956-08-24 Production of titanium tetraiodide

Country Status (1)

Country Link
GB (1) GB801415A (en)

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