GB801415A - Production of titanium tetraiodide - Google Patents
Production of titanium tetraiodideInfo
- Publication number
- GB801415A GB801415A GB25934/56A GB2593456A GB801415A GB 801415 A GB801415 A GB 801415A GB 25934/56 A GB25934/56 A GB 25934/56A GB 2593456 A GB2593456 A GB 2593456A GB 801415 A GB801415 A GB 801415A
- Authority
- GB
- United Kingdom
- Prior art keywords
- titanium tetrachloride
- titanium
- hydrogen iodide
- iodide
- tetraiodide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/02—Halides of titanium
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Titanium tetraiodide and by-product hydrogen chloride are prepared by treating liquid titanium tetrachloride with hydrogen iodide, the amount of hydrogen iodide being insufficient to utilize the whole of the titanium tetrachloride employed. The hydrogen iodide may be passed into liquid titanium tetrachloride such that the ratio of iodide to titanium does not reach 4, and preferably does not reach 3, or the hydrogen iodide and titanium tetrachloride may be added to a bath of titanium tetrachloride in mol. ratio of 4 : 1, or the titanium tetrachloride is passed downward in countercurrent to hydrogen iodide. The reaction temperature is preferably maintained between 10 DEG and 40 DEG C. and especially between 20 DEG and 30 DEG C. The titanium tetraiodide product may be separated by crystallization or by fractional distillation.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US801415XA | 1955-08-24 | 1955-08-24 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB801415A true GB801415A (en) | 1958-09-10 |
Family
ID=22155514
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB25934/56A Expired GB801415A (en) | 1955-08-24 | 1956-08-24 | Production of titanium tetraiodide |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB801415A (en) |
-
1956
- 1956-08-24 GB GB25934/56A patent/GB801415A/en not_active Expired
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