GB590750A - A method for the separation of components of starch - Google Patents
A method for the separation of components of starchInfo
- Publication number
- GB590750A GB590750A GB926845A GB926845A GB590750A GB 590750 A GB590750 A GB 590750A GB 926845 A GB926845 A GB 926845A GB 926845 A GB926845 A GB 926845A GB 590750 A GB590750 A GB 590750A
- Authority
- GB
- United Kingdom
- Prior art keywords
- starch
- separated
- amylose
- phenol
- precipitated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229920002472 Starch Polymers 0.000 title abstract 5
- 235000019698 starch Nutrition 0.000 title abstract 5
- 239000008107 starch Substances 0.000 title abstract 5
- 238000000926 separation method Methods 0.000 title 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Natural products OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract 5
- 229920000856 Amylose Polymers 0.000 abstract 3
- IWDCLRJOBJJRNH-UHFFFAOYSA-N P-Cresol Chemical compound CC1=CC=C(O)C=C1 IWDCLRJOBJJRNH-UHFFFAOYSA-N 0.000 abstract 2
- 239000007788 liquid Substances 0.000 abstract 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract 2
- CETWDUZRCINIHU-UHFFFAOYSA-N 2-Heptanol Chemical compound CCCCCC(C)O CETWDUZRCINIHU-UHFFFAOYSA-N 0.000 abstract 1
- IQUPABOKLQSFBK-UHFFFAOYSA-N 2-nitrophenol Chemical compound OC1=CC=CC=C1[N+]([O-])=O IQUPABOKLQSFBK-UHFFFAOYSA-N 0.000 abstract 1
- BTJIUGUIPKRLHP-UHFFFAOYSA-N 4-Nitrophenol Chemical compound OC1=CC=C([N+]([O-])=O)C=C1 BTJIUGUIPKRLHP-UHFFFAOYSA-N 0.000 abstract 1
- WXNZTHHGJRFXKQ-UHFFFAOYSA-N 4-chlorophenol Chemical compound OC1=CC=C(Cl)C=C1 WXNZTHHGJRFXKQ-UHFFFAOYSA-N 0.000 abstract 1
- 229920000945 Amylopectin Polymers 0.000 abstract 1
- WMGFVAGNIYUEEP-WUYNJSITSA-N Amylopectin Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)O[C@H](OC[C@@H]2[C@H]([C@H](O)[C@@H](O)[C@@H](O[C@@H]3[C@H](O[C@H](O)[C@H](O)[C@H]3O)CO)O2)O[C@@H]2[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O2)O)[C@H](O)[C@H]1O WMGFVAGNIYUEEP-WUYNJSITSA-N 0.000 abstract 1
- HPXRVTGHNJAIIH-UHFFFAOYSA-N Cyclohexanol Chemical compound OC1CCCCC1 HPXRVTGHNJAIIH-UHFFFAOYSA-N 0.000 abstract 1
- RLSSMJSEOOYNOY-UHFFFAOYSA-N M-Cresol Chemical compound CC1=CC=CC(O)=C1 RLSSMJSEOOYNOY-UHFFFAOYSA-N 0.000 abstract 1
- QWVGKYWNOKOFNN-UHFFFAOYSA-N O-Cresol Chemical compound CC1=CC=CC=C1O QWVGKYWNOKOFNN-UHFFFAOYSA-N 0.000 abstract 1
- WUOACPNHFRMFPN-UHFFFAOYSA-N Terpineol Chemical compound CC1=CCC(C(C)(C)O)CC1 WUOACPNHFRMFPN-UHFFFAOYSA-N 0.000 abstract 1
- MGSRCZKZVOBKFT-UHFFFAOYSA-N Thymol Chemical compound CC(C)C1=CC=C(C)C=C1O MGSRCZKZVOBKFT-UHFFFAOYSA-N 0.000 abstract 1
- 239000005844 Thymol Substances 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- -1 carvacol Chemical compound 0.000 abstract 1
- 125000004122 cyclic group Chemical group 0.000 abstract 1
- 239000006185 dispersion Substances 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 238000001704 evaporation Methods 0.000 abstract 1
- 150000002500 ions Chemical class 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 150000002989 phenols Chemical class 0.000 abstract 1
- 238000001556 precipitation Methods 0.000 abstract 1
- 239000011780 sodium chloride Substances 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 239000006228 supernatant Substances 0.000 abstract 1
- 239000000725 suspension Substances 0.000 abstract 1
- 229960000790 thymol Drugs 0.000 abstract 1
- 229930007823 thymol Natural products 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B30/00—Preparation of starch, degraded or non-chemically modified starch, amylose, or amylopectin
- C08B30/20—Amylose or amylopectin
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
The amylose component of starch is separated by a process which comprises the addition to an ion-containing aqueous dispersion of starch any of the group of phenols consisting of thymol, carvacol, o-, m- and p-cresol, o- and p-chlorophenol, o- and pbromophenol and o-and p-nitrophenol, and removing the precipitated amylose. The starch may be made into a paste with cold water and 0.1 per cent. of sodium chloride added in hot aqueous solution, the suspension being diluted till it contains 1-3 per cent. of starch. It is mechanically stirred while heated and after undispersed solid matter has been removed by centrifuging and the supernatant liquid brought to a pH of 8 and cooled to 20-30 DEG C, the amylose is precipitated by the phenol and separated. Amylopectin may be separated from the residual liquid by precipitation with methanol or by evaporation. The Provisional Specification describes also the use of any phenol, terpene alcohol or of a cyclic alcohol such as cyclohexanol or methyl hexanol.
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB590750A true GB590750A (en) | 1947-07-28 |
Family
ID=1629722
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB926845A Expired GB590750A (en) | 1945-04-13 | A method for the separation of components of starch |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB590750A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2822305A (en) * | 1951-12-15 | 1958-02-04 | Avebe Coop Verkoop Prod | Process for fractionating starch into components with branched and linear chains |
| US2829988A (en) * | 1953-05-15 | 1958-04-08 | Avebe Coop Verkoop Prod | Process for fractionating starch into components with branched and linear chains |
-
1945
- 1945-04-13 GB GB926845A patent/GB590750A/en not_active Expired
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2822305A (en) * | 1951-12-15 | 1958-02-04 | Avebe Coop Verkoop Prod | Process for fractionating starch into components with branched and linear chains |
| US2829990A (en) * | 1951-12-15 | 1958-04-08 | Avebe Coop Verkoop Prod | Process for fractionating starch into components with branched and linear chains |
| US2829989A (en) * | 1951-12-15 | 1958-04-08 | Avebe Coop Verkoop Prod | Process for fractionating starch into components with branched and linear chains |
| US2829988A (en) * | 1953-05-15 | 1958-04-08 | Avebe Coop Verkoop Prod | Process for fractionating starch into components with branched and linear chains |
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