GB573565A - Improvements in or relating to the concentration of aqueous acetic acid - Google Patents
Improvements in or relating to the concentration of aqueous acetic acidInfo
- Publication number
- GB573565A GB573565A GB309642A GB309642A GB573565A GB 573565 A GB573565 A GB 573565A GB 309642 A GB309642 A GB 309642A GB 309642 A GB309642 A GB 309642A GB 573565 A GB573565 A GB 573565A
- Authority
- GB
- United Kingdom
- Prior art keywords
- paraldehyde
- concentration
- acetic acid
- aqueous acetic
- relating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
- C07C51/46—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation by azeotropic distillation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The concentration of aqueous acetic acid is effected by azeotropic distillation with paraldehyde. Any remaining paraldehyde may be depolymerized and distilled off and then absorbed in paraldehyde containing a little sulphuric acid to convert it into paraldehyde. Preferably, the azeotropic distillation is effected under reduced pressure to bring the boiling-point below 80 DEG C. so as to avoid any depolymerization of the paraldehyde. The initial acid may be first extracted with paraldehyde, the extract being then treated as described above.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB309642A GB573565A (en) | 1941-06-17 | 1941-06-17 | Improvements in or relating to the concentration of aqueous acetic acid |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB309642A GB573565A (en) | 1941-06-17 | 1941-06-17 | Improvements in or relating to the concentration of aqueous acetic acid |
Publications (1)
Publication Number | Publication Date |
---|---|
GB573565A true GB573565A (en) | 1945-11-27 |
Family
ID=9751863
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB309642A Expired GB573565A (en) | 1941-06-17 | 1941-06-17 | Improvements in or relating to the concentration of aqueous acetic acid |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB573565A (en) |
-
1941
- 1941-06-17 GB GB309642A patent/GB573565A/en not_active Expired
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