GB443998A - Manufacture of solid stable sulphuric acid ester salts of leuco-vat-dyestuffs - Google Patents

Manufacture of solid stable sulphuric acid ester salts of leuco-vat-dyestuffs

Info

Publication number
GB443998A
GB443998A GB20803/35A GB2080335A GB443998A GB 443998 A GB443998 A GB 443998A GB 20803/35 A GB20803/35 A GB 20803/35A GB 2080335 A GB2080335 A GB 2080335A GB 443998 A GB443998 A GB 443998A
Authority
GB
United Kingdom
Prior art keywords
leuco
acid ester
sulphuric acid
salt
dyestuffs
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB20803/35A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Durand and Huguenin AG
Original Assignee
Durand and Huguenin AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Durand and Huguenin AG filed Critical Durand and Huguenin AG
Publication of GB443998A publication Critical patent/GB443998A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B9/00Esters or ester-salts of leuco compounds of vat dyestuffs
    • C09B9/02Esters or ester-salts of leuco compounds of vat dyestuffs of anthracene dyes
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J101/00Adhesives based on cellulose, modified cellulose, or cellulose derivatives
    • C09J101/08Cellulose derivatives
    • C09J101/16Esters of inorganic acids
    • C09J101/18Cellulose nitrate
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2666/00Composition of polymers characterized by a further compound in the blend, being organic macromolecular compounds, natural resins, waxes or and bituminous materials, non-macromolecular organic substances, inorganic substances or characterized by their function in the composition
    • C08L2666/02Organic macromolecular compounds, natural resins, waxes or and bituminous materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

Stable sulphuric acid ester salts of leuco vat dyestuffs are made in powder form by mixing together to form a paste, a moist alkali salt of the ester containing an excess of alkali and an agglutinant, and, if desired, urea and evaporating the paste to dryness, preferably under reduced pressure. Agglutinants mentioned are glucose, cane-sugar molasses, sulphite cellulose waste liquor, dextrin, gum, glue or mixtures thereof. In examples: (1) the potassium salt of the acid sulphuric acid ester of leuco - Bz. 2 : Bz 2<1> dimethoxy-dibenzanthrone and excess caustic soda solution are mixed with molasses syrup and urea and the mixture is evaporated to dryness in vacuo at about 60 DEG C.; (2) the same salt is mixed with an aqueous solution of dextrin and the mixture similarly dried; (3) the dyestuff in (1) is replaced by the sodium salt of the acid sulphuric acid ester of the leuco-compound of the dyestuff of Specification 24604/08, [Class 2].
GB20803/35A 1934-07-21 1935-07-22 Manufacture of solid stable sulphuric acid ester salts of leuco-vat-dyestuffs Expired GB443998A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE443998X 1934-07-21

Publications (1)

Publication Number Publication Date
GB443998A true GB443998A (en) 1936-03-11

Family

ID=6532855

Family Applications (1)

Application Number Title Priority Date Filing Date
GB20803/35A Expired GB443998A (en) 1934-07-21 1935-07-22 Manufacture of solid stable sulphuric acid ester salts of leuco-vat-dyestuffs

Country Status (2)

Country Link
FR (1) FR443998A (en)
GB (1) GB443998A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3086833A (en) * 1963-04-23 Diazonium salt compositions and method
US20190315967A1 (en) * 2018-04-13 2019-10-17 Nocopi Technologies, Inc. Leuco dye pastel marking device

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3086833A (en) * 1963-04-23 Diazonium salt compositions and method
US20190315967A1 (en) * 2018-04-13 2019-10-17 Nocopi Technologies, Inc. Leuco dye pastel marking device
US10597537B2 (en) * 2018-04-13 2020-03-24 Nocopi Technologies, Inc. Leuco dye pastel marking device

Also Published As

Publication number Publication date
FR443998A (en) 1912-10-07

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