GB443285A - An improved method for the production of pure phenols from lignite tar, shale tar and low temperature tars - Google Patents
An improved method for the production of pure phenols from lignite tar, shale tar and low temperature tarsInfo
- Publication number
- GB443285A GB443285A GB1609434A GB1609434A GB443285A GB 443285 A GB443285 A GB 443285A GB 1609434 A GB1609434 A GB 1609434A GB 1609434 A GB1609434 A GB 1609434A GB 443285 A GB443285 A GB 443285A
- Authority
- GB
- United Kingdom
- Prior art keywords
- tar
- low temperature
- pure
- lignite
- shale
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/005—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by obtaining phenols from products, waste products or side-products of processes, not directed to the production of phenols, by conversion or working-up
- C07C37/007—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by obtaining phenols from products, waste products or side-products of processes, not directed to the production of phenols, by conversion or working-up from the tar industry
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Pure phenols are obtained from lignite tar, shale tar or low temperature tar by heating the tar oil to at least 300 DEG C. during or prior to fractionation so as to effect a mild cracking, treating the oils with soda lye, oxidizing the lye solution and then passing steam through it while the temperature of the liquid is increased to about 105--120 DEG C., so as to remove impurities, and finally recovering the pure phenols by acidifying the liquid. The oxidation may be effected by air or by sodium hypochlorite, and resinous byeproducts may be recovered. In examples, tar oil derived from low temperature tars is fractionated, the distillate treated with sulphuric acid, and a solution of the product in aqueous caustic soda is oxidized, steamed, and then acidified to yield pure cresols and an asphaltic residue. Specifications 355,445 and 363,330 are referred to.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1609434A GB443285A (en) | 1934-12-14 | 1934-12-14 | An improved method for the production of pure phenols from lignite tar, shale tar and low temperature tars |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1609434A GB443285A (en) | 1934-12-14 | 1934-12-14 | An improved method for the production of pure phenols from lignite tar, shale tar and low temperature tars |
Publications (1)
Publication Number | Publication Date |
---|---|
GB443285A true GB443285A (en) | 1936-02-26 |
Family
ID=10071080
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1609434A Expired GB443285A (en) | 1934-12-14 | 1934-12-14 | An improved method for the production of pure phenols from lignite tar, shale tar and low temperature tars |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB443285A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5248814A (en) * | 1991-09-13 | 1993-09-28 | Eniricerche S.P.A. | Process for producing regenerated humic acids from coal |
-
1934
- 1934-12-14 GB GB1609434A patent/GB443285A/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5248814A (en) * | 1991-09-13 | 1993-09-28 | Eniricerche S.P.A. | Process for producing regenerated humic acids from coal |
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