GB427526A - Improvements in the manufacture and production of magnesia and nitrogenous fertilisers from dolomite - Google Patents

Improvements in the manufacture and production of magnesia and nitrogenous fertilisers from dolomite

Info

Publication number
GB427526A
GB427526A GB26300/34A GB2630034A GB427526A GB 427526 A GB427526 A GB 427526A GB 26300/34 A GB26300/34 A GB 26300/34A GB 2630034 A GB2630034 A GB 2630034A GB 427526 A GB427526 A GB 427526A
Authority
GB
United Kingdom
Prior art keywords
ammonia
fertilizer
dolomite
evaporated
magnesia
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB26300/34A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kloeckner Werke AG
Original Assignee
Kloeckner Werke AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kloeckner Werke AG filed Critical Kloeckner Werke AG
Publication of GB427526A publication Critical patent/GB427526A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F5/00Compounds of magnesium
    • C01F5/14Magnesium hydroxide
    • C01F5/20Magnesium hydroxide by precipitation from solutions of magnesium salts with ammonia

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Fertilizers (AREA)

Abstract

Magnesia and nitrogenous fertilizers are obtained from dolomite by dissolving the dolomite in nitric acid, precipitating magnesium hydroxide from the solution with ammonia, separating the precipitate by filtration and converting it into magnesia and converting the filtrate into a fertilizer. The ammoniacal filtrate may be evaporated to obtain a fertilizer containing ammonium and calcium nitrates or may be treated with carbonic acid, say that obtained in the initial dissolution of the dolomite, to obtain calcium carbonate and ammonium nitrate which may be either separated or evaporated together to form a fertilizer. The amount of ammonia added may be restricted so that the fertilizer obtained contains magnesium nitrate. The ammonia may be added in the gaseous or aqueous form preferably with cooling to a temperature below 20 DEG C. The magnesia may be obtained free from iron by adding sufficient ammonia to precipitate ferric hydroxide which is filtered off before the further addition of ammonia. The ammoniacal filtrate may be evaporated at 140 DEG C., and solidified during cooling and stirring to form crystallinc granules. Specification 403,054 is referred to.ALSO:Nitrogenous fertilizers are obtained from dolomite by dissolving the dolomite in nitric acid, precipitating magnesium hydroxide from the solution with ammonia, separating the precipitate by filtration and converting it into magnesia and converting the filtrate into a fertilizer. The ammoniacal filtrate may be evaporated to obtain a fertilizer containing ammonium and calcium nitrates or may be treated with carbonic acid, say that obtained in the initial dissolution of the dolomite, to obtain calcium carbonate and ammonium nitrate which may be evaporated together to form a fertilizer. The amount of ammonia added may be restricted so that the fertilizer obtained contains magnesium nitrate. The ammonia may be added in the gaseous or aqueous form preferably with cooling to a temperature below 20 DEG C. The ammoniacal filtrate may be evaporated at 140 DEG C., and solidified during cooling and stirring to form crystalline granules. Specification 403,054, [Group III], is referred to.
GB26300/34A 1933-10-02 1934-09-13 Improvements in the manufacture and production of magnesia and nitrogenous fertilisers from dolomite Expired GB427526A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE427526X 1933-10-02

Publications (1)

Publication Number Publication Date
GB427526A true GB427526A (en) 1935-04-25

Family

ID=6477323

Family Applications (1)

Application Number Title Priority Date Filing Date
GB26300/34A Expired GB427526A (en) 1933-10-02 1934-09-13 Improvements in the manufacture and production of magnesia and nitrogenous fertilisers from dolomite

Country Status (1)

Country Link
GB (1) GB427526A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE966806C (en) * 1952-06-19 1957-09-12 Dr Otto Kippe Process for the production of nitrogenous fertilizers with simultaneous production of magnesia or magnesium hydroxide
CN111204779A (en) * 2020-03-10 2020-05-29 余荣华 Fused salt production method for co-producing high-purity magnesium hydroxide, magnesium carbonate and nitrogen-potassium fertilizer
CN113233480A (en) * 2021-06-29 2021-08-10 郭建文 Magnesium refining slag recovery equipment and recovery process thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE966806C (en) * 1952-06-19 1957-09-12 Dr Otto Kippe Process for the production of nitrogenous fertilizers with simultaneous production of magnesia or magnesium hydroxide
CN111204779A (en) * 2020-03-10 2020-05-29 余荣华 Fused salt production method for co-producing high-purity magnesium hydroxide, magnesium carbonate and nitrogen-potassium fertilizer
CN113233480A (en) * 2021-06-29 2021-08-10 郭建文 Magnesium refining slag recovery equipment and recovery process thereof

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