GB239878A - Process for improving decamphorated oil of turpentine - Google Patents
Process for improving decamphorated oil of turpentineInfo
- Publication number
- GB239878A GB239878A GB22817/25A GB2281725A GB239878A GB 239878 A GB239878 A GB 239878A GB 22817/25 A GB22817/25 A GB 22817/25A GB 2281725 A GB2281725 A GB 2281725A GB 239878 A GB239878 A GB 239878A
- Authority
- GB
- United Kingdom
- Prior art keywords
- acid
- oil
- copper
- halogen
- oils
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 241000779819 Syncarpia glomulifera Species 0.000 title 1
- 239000001739 pinus spp. Substances 0.000 title 1
- 229940036248 turpentine Drugs 0.000 title 1
- 239000003921 oil Substances 0.000 abstract 8
- 235000019198 oils Nutrition 0.000 abstract 8
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 abstract 6
- 239000002253 acid Substances 0.000 abstract 6
- 239000003054 catalyst Substances 0.000 abstract 4
- 229910052736 halogen Inorganic materials 0.000 abstract 3
- 150000002367 halogens Chemical class 0.000 abstract 3
- XXZAOMJCZBZKPV-WEDXCCLWSA-N (1r,3s,4r)-3-chloro-4,7,7-trimethylbicyclo[2.2.1]heptane Chemical compound C1C[C@@]2(C)[C@@H](Cl)C[C@@H]1C2(C)C XXZAOMJCZBZKPV-WEDXCCLWSA-N 0.000 abstract 2
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 abstract 2
- 241000723346 Cinnamomum camphora Species 0.000 abstract 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract 2
- QPLDLSVMHZLSFG-UHFFFAOYSA-N Copper oxide Chemical compound [Cu]=O QPLDLSVMHZLSFG-UHFFFAOYSA-N 0.000 abstract 2
- 239000005751 Copper oxide Substances 0.000 abstract 2
- 239000003513 alkali Substances 0.000 abstract 2
- 230000015572 biosynthetic process Effects 0.000 abstract 2
- 238000009835 boiling Methods 0.000 abstract 2
- 229960000846 camphor Drugs 0.000 abstract 2
- 229930008380 camphor Natural products 0.000 abstract 2
- 229910052802 copper Inorganic materials 0.000 abstract 2
- 239000010949 copper Substances 0.000 abstract 2
- 229910000431 copper oxide Inorganic materials 0.000 abstract 2
- 238000001035 drying Methods 0.000 abstract 2
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 abstract 2
- 229910000464 lead oxide Inorganic materials 0.000 abstract 2
- 235000021388 linseed oil Nutrition 0.000 abstract 2
- 239000000944 linseed oil Substances 0.000 abstract 2
- 229960002523 mercuric chloride Drugs 0.000 abstract 2
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 abstract 2
- 229910052753 mercury Inorganic materials 0.000 abstract 2
- LWJROJCJINYWOX-UHFFFAOYSA-L mercury dichloride Chemical compound Cl[Hg]Cl LWJROJCJINYWOX-UHFFFAOYSA-L 0.000 abstract 2
- 239000007800 oxidant agent Substances 0.000 abstract 2
- YEXPOXQUZXUXJW-UHFFFAOYSA-N oxolead Chemical compound [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 abstract 2
- 235000011118 potassium hydroxide Nutrition 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- 238000003786 synthesis reaction Methods 0.000 abstract 2
- 150000003505 terpenes Chemical class 0.000 abstract 2
- 235000007586 terpenes Nutrition 0.000 abstract 2
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09F—NATURAL RESINS; FRENCH POLISH; DRYING-OILS; OIL DRYING AGENTS, i.e. SICCATIVES; TURPENTINE
- C09F3/00—Obtaining spirits of turpentine
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09F—NATURAL RESINS; FRENCH POLISH; DRYING-OILS; OIL DRYING AGENTS, i.e. SICCATIVES; TURPENTINE
- C09F5/00—Obtaining drying-oils
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Paints Or Removers (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
Abstract
The terpene oil remaining when the acid is removed from the pinene hydrochloride in the synthesis of camphor is treated with sulphuric or other acid, or an alkali, or a halogen, or air or other oxidizing agent, whereby there are produced sweet-smelling drying oils of higher boiling point. The oils obtained by the halogen treatment also serve as solvents. Catalysts may be present and raised temperatures and pressures may be used. In an example the oil is boiled with caustic potash lye in presence of mercury or copper. The mass is washed with dilute acid, dried, and fractionally distilled. The products are suitable substitutes for linseed oil. Other catalysts specified are p mercuric chloride, copper oxide, lead oxide, and iron chloride.ALSO:The terpene oil remaining when the acid is removed from the pinene hydrochloride in the synthesis of camphor, is treated with sulphuric or other acid, or an alkali, or a halogen, or air or other oxidizing agent, whereby there are produced sweet-smelling drying oils of higher boiling point. The oils also serve as solvents. The treatment may take place at atmospheric or higher temperatures and pressures and in presence of a catalyst. In an example the oil is boiled with about 1/10 its volume of caustic potash lye of 50 per cent cent strength in presence of mercury or copper. The mass is washed with dilute acid, dried, and fractionally distilled. The products are suitable substitutes for linseed oil. Other catalysts specified are mercuric chloride, copper oxide, lead oxide, and iron chloride.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE239878X | 1924-09-12 | ||
| DE255896X | 1925-07-25 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB239878A true GB239878A (en) | 1926-12-13 |
Family
ID=33030533
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB22817/25A Expired GB239878A (en) | 1924-09-12 | 1925-09-12 | Process for improving decamphorated oil of turpentine |
| GB18446/26A Expired GB255896A (en) | 1924-09-12 | 1926-07-23 | Process for treating decamphorated oil of turpentine |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB18446/26A Expired GB255896A (en) | 1924-09-12 | 1926-07-23 | Process for treating decamphorated oil of turpentine |
Country Status (1)
| Country | Link |
|---|---|
| GB (2) | GB239878A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106281041A (en) * | 2016-08-22 | 2017-01-04 | 怀化市双阳林化有限公司 | The deodorization of a kind of crude sulfate turpentine and the production method of sulfate turpentine |
-
1925
- 1925-09-12 GB GB22817/25A patent/GB239878A/en not_active Expired
-
1926
- 1926-07-23 GB GB18446/26A patent/GB255896A/en not_active Expired
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106281041A (en) * | 2016-08-22 | 2017-01-04 | 怀化市双阳林化有限公司 | The deodorization of a kind of crude sulfate turpentine and the production method of sulfate turpentine |
| CN106281041B (en) * | 2016-08-22 | 2019-01-04 | 湖南双阳高科化工有限公司 | A kind of deodorization of crude sulfate turpentine and the production method of sulfate turpentine |
Also Published As
| Publication number | Publication date |
|---|---|
| GB255896A (en) | 1927-10-24 |
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