GB573702A - Preparation of alkali metal hydracrylates - Google Patents

Preparation of alkali metal hydracrylates

Info

Publication number
GB573702A
GB573702A GB15933/43A GB1593343A GB573702A GB 573702 A GB573702 A GB 573702A GB 15933/43 A GB15933/43 A GB 15933/43A GB 1593343 A GB1593343 A GB 1593343A GB 573702 A GB573702 A GB 573702A
Authority
GB
United Kingdom
Prior art keywords
alkali metal
sodium
hydracrylates
hydracrylate
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB15933/43A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wyeth Holdings LLC
Original Assignee
American Cyanamid Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by American Cyanamid Co filed Critical American Cyanamid Co
Publication of GB573702A publication Critical patent/GB573702A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/41Preparation of salts of carboxylic acids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Alkali metal hydracrylates are prepared by adding ethylene cyanohydrin to an aqueous solution of a strong base of an alkali metal which is maintained at a temperature of at least 70 DEG C. In an example, the strong base used is sodium hydroxide. During the addition of ethylene cyanohydrin, the solution of the base may be agitated mechanically and removal of ammonia facilitated by the introduction of a small stream of steam. On completion of the reaction, residual ammonia and water may be evaporated off and the product purified by, for example, recrystallization or solvent extraction. The sodium hydracrylate can be converted to another alkali metal hydracrylate by first forming the free acid by treatment with, for example, sulphuric acid. Other strong bases which can be used in the above process are potassium hydroxide and sodium and potassium carbonate. The process may be carried out also at reduced or elevated pressures. Specification 573,384 is referred to.
GB15933/43A 1942-10-07 1943-09-28 Preparation of alkali metal hydracrylates Expired GB573702A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US573702XA 1942-10-07 1942-10-07

Publications (1)

Publication Number Publication Date
GB573702A true GB573702A (en) 1945-12-03

Family

ID=22010155

Family Applications (1)

Application Number Title Priority Date Filing Date
GB15933/43A Expired GB573702A (en) 1942-10-07 1943-09-28 Preparation of alkali metal hydracrylates

Country Status (1)

Country Link
GB (1) GB573702A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2686797A (en) * 1949-05-18 1954-08-17 Bersworth Method of producing glycollic acid

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2686797A (en) * 1949-05-18 1954-08-17 Bersworth Method of producing glycollic acid

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