GB191329546A - Manufacture of Mononitro- and Dinitroaminobenzene-arsinic Acids or Substitution Derivatives thereof Substituted in the Amino-group. - Google Patents
Manufacture of Mononitro- and Dinitroaminobenzene-arsinic Acids or Substitution Derivatives thereof Substituted in the Amino-group.Info
- Publication number
- GB191329546A GB191329546A GB191329546DA GB191329546A GB 191329546 A GB191329546 A GB 191329546A GB 191329546D A GB191329546D A GB 191329546DA GB 191329546 A GB191329546 A GB 191329546A
- Authority
- GB
- United Kingdom
- Prior art keywords
- acid
- mononitro
- chlorbenzenearsonic
- derivatives
- dinitro
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000002253 acid Substances 0.000 title abstract 3
- 150000007513 acids Chemical class 0.000 title abstract 2
- 125000003277 amino group Chemical group 0.000 title 1
- 238000004519 manufacturing process Methods 0.000 title 1
- 238000006467 substitution reaction Methods 0.000 title 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 3
- 150000001875 compounds Chemical class 0.000 abstract 3
- OAKWMQGNBGGJGT-UHFFFAOYSA-N (4-chlorophenyl)arsonic acid Chemical compound O[As](O)(=O)C1=CC=C(Cl)C=C1 OAKWMQGNBGGJGT-UHFFFAOYSA-N 0.000 abstract 2
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 abstract 2
- NQRYJNQNLNOLGT-UHFFFAOYSA-N Piperidine Chemical compound C1CCNCC1 NQRYJNQNLNOLGT-UHFFFAOYSA-N 0.000 abstract 2
- 238000006396 nitration reaction Methods 0.000 abstract 2
- KCXLTLYNFDGRKZ-UHFFFAOYSA-N (4-chloro-3-nitrophenyl)arsonic acid Chemical compound O[As](O)(=O)C1=CC=C(Cl)C([N+]([O-])=O)=C1 KCXLTLYNFDGRKZ-UHFFFAOYSA-N 0.000 abstract 1
- KHBQMWCZKVMBLN-UHFFFAOYSA-N Benzenesulfonamide Chemical compound NS(=O)(=O)C1=CC=CC=C1 KHBQMWCZKVMBLN-UHFFFAOYSA-N 0.000 abstract 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 1
- JLPFBAOHWONVQL-UHFFFAOYSA-N [2-(dinitroamino)phenyl]arsonic acid Chemical class [N+](=O)([O-])N([N+](=O)[O-])C1=C(C=CC=C1)[As](O)(=O)O JLPFBAOHWONVQL-UHFFFAOYSA-N 0.000 abstract 1
- IXHDVZUOIRQHFE-UHFFFAOYSA-N [4-(methylamino)-3-nitrophenyl]arsonic acid Chemical compound CNC1=C(C=C(C=C1)[As](O)(=O)O)[N+](=O)[O-] IXHDVZUOIRQHFE-UHFFFAOYSA-N 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- -1 dinitro compound Chemical class 0.000 abstract 1
- 229960002449 glycine Drugs 0.000 abstract 1
- 235000013905 glycine and its sodium salt Nutrition 0.000 abstract 1
- 238000007689 inspection Methods 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 229910017604 nitric acid Inorganic materials 0.000 abstract 1
- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 abstract 1
- 150000003141 primary amines Chemical class 0.000 abstract 1
- 150000003335 secondary amines Chemical class 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/66—Arsenic compounds
- C07F9/70—Organo-arsenic compounds
- C07F9/74—Aromatic compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
29,546. Boehringer & Soehne, C. F. Dec. 24, 1912, [Convention date]. Mono- and di-nitroaminobenzenearsonic acids and derivatives thereof are prepared by treating 4-chlor-mono- or -di-nitrobenzenearsonic acids with ammonia or its derivatives, the product being further nitrated if a dinitro compound is desired and a mononitro compound is the parent substance. Ammonia derivatives include primary and secondary amines, and compounds of the type of aminoacetic acid, benzenesulphonamide, and piperidine. 3:5-Dinitro-4-chlorbenzenearsonic acid for use as a parent material is obtained by direct introduction of two nitro groups into 4-chlorbenzenearsonic acid, or by further nitration of the mononitro compound. 4-Chlor-3-nitrobenzenearsonic acid is prepared by nitration of 4-chlorbenzenearsonic acid. The Specification as open to inspection under Section 91 (3) (a) describes also the preparation of 3 : 5-dinitro-4-methylnitraminobenzene-1-arsonic acid by the action of concentrated nitric acid upon 4-methylamino-3-nitrobenzene-1-arsonic acid. This subject-matter does not appear in the Specification as accepted.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE285604T | 1912-12-24 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB191329546A true GB191329546A (en) | 1914-06-25 |
Family
ID=88978146
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB191329546D Expired GB191329546A (en) | 1912-12-24 | 1913-12-22 | Manufacture of Mononitro- and Dinitroaminobenzene-arsinic Acids or Substitution Derivatives thereof Substituted in the Amino-group. |
Country Status (3)
| Country | Link |
|---|---|
| DE (2) | DE285604C (en) |
| GB (1) | GB191329546A (en) |
| NL (1) | NL1367C (en) |
-
1912
- 1912-12-24 DE DE1912285604D patent/DE285604C/de not_active Expired
-
1913
- 1913-12-20 NL NL3840A patent/NL1367C/en active
- 1913-12-22 GB GB191329546D patent/GB191329546A/en not_active Expired
-
1915
- 1915-04-28 DE DE1915292546D patent/DE292546C/de not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DE292546C (en) | 1916-06-15 |
| DE285604C (en) | 1915-07-12 |
| NL1367C (en) | 1916-07-01 |
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