GB173540A - Improvements in the manufacture of phenyl glycine compounds - Google Patents
Improvements in the manufacture of phenyl glycine compoundsInfo
- Publication number
- GB173540A GB173540A GB1827820A GB1827820A GB173540A GB 173540 A GB173540 A GB 173540A GB 1827820 A GB1827820 A GB 1827820A GB 1827820 A GB1827820 A GB 1827820A GB 173540 A GB173540 A GB 173540A
- Authority
- GB
- United Kingdom
- Prior art keywords
- alkali
- phenyl glycine
- triphenyltriamine
- aniline
- ethylene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
In one method of production, tetrachlorethane or trichlorethylene and aniline in aqueous suspension are heated with an alkali such as milk of lime to 140-190 DEG C. until the conversion of the intermediate bodies such as ethylene-triphenyltriamine into phenyl glycine compounds is complete. An autoclave provided with an agitator may be used. After 24 hours' heating, the excess of aniline may be distilled off, and the residue cooled and filtered. The solid product may be converted into an alkali salt of phenylglycine, and the small quantity of the calcium salt remaining in the filtrate may be precipitated as the ferrous salt. In another method, ethylene-triphenyltriamine and a caustic alkali or alkaline earth are heated together. Specifications 678/06, 5013/07, 5014/07, and 13176/07 are referred to. According to the Provisional Specification, phenyl glycine anilide may be obtained as an intermediate product in the first method, also, alkali hydrates, carbonates, silicates, aluminates, and zincates are suitable alkalies.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1827820A GB173540A (en) | 1920-07-02 | 1920-07-02 | Improvements in the manufacture of phenyl glycine compounds |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1827820A GB173540A (en) | 1920-07-02 | 1920-07-02 | Improvements in the manufacture of phenyl glycine compounds |
Publications (1)
Publication Number | Publication Date |
---|---|
GB173540A true GB173540A (en) | 1922-01-03 |
Family
ID=10109703
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1827820A Expired GB173540A (en) | 1920-07-02 | 1920-07-02 | Improvements in the manufacture of phenyl glycine compounds |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB173540A (en) |
-
1920
- 1920-07-02 GB GB1827820A patent/GB173540A/en not_active Expired
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