GB1449792A - Cyanide-free electrolyte for the electrodeposition of silver - Google Patents
Cyanide-free electrolyte for the electrodeposition of silverInfo
- Publication number
- GB1449792A GB1449792A GB874175A GB874175A GB1449792A GB 1449792 A GB1449792 A GB 1449792A GB 874175 A GB874175 A GB 874175A GB 874175 A GB874175 A GB 874175A GB 1449792 A GB1449792 A GB 1449792A
- Authority
- GB
- United Kingdom
- Prior art keywords
- silver
- compound
- compounds
- acid
- electro
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000003792 electrolyte Substances 0.000 title abstract 2
- 229910052709 silver Inorganic materials 0.000 title abstract 2
- 239000004332 silver Substances 0.000 title abstract 2
- 238000004070 electrodeposition Methods 0.000 title 1
- 150000001875 compounds Chemical class 0.000 abstract 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 4
- -1 oxide Chemical compound 0.000 abstract 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 abstract 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 abstract 2
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 abstract 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 abstract 2
- AEMRFAOFKBGASW-UHFFFAOYSA-N Glycolic acid Chemical compound OCC(O)=O AEMRFAOFKBGASW-UHFFFAOYSA-N 0.000 abstract 2
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 abstract 2
- 239000004698 Polyethylene Substances 0.000 abstract 2
- ZMZDMBWJUHKJPS-UHFFFAOYSA-M Thiocyanate anion Chemical compound [S-]C#N ZMZDMBWJUHKJPS-UHFFFAOYSA-M 0.000 abstract 2
- 239000000654 additive Substances 0.000 abstract 2
- 229910052783 alkali metal Inorganic materials 0.000 abstract 2
- 150000001412 amines Chemical class 0.000 abstract 2
- 229910021529 ammonia Inorganic materials 0.000 abstract 2
- 238000000151 deposition Methods 0.000 abstract 2
- ZMZDMBWJUHKJPS-UHFFFAOYSA-N hydrogen thiocyanate Natural products SC#N ZMZDMBWJUHKJPS-UHFFFAOYSA-N 0.000 abstract 2
- 229920000768 polyamine Polymers 0.000 abstract 2
- IIACRCGMVDHOTQ-UHFFFAOYSA-M sulfamate Chemical compound NS([O-])(=O)=O IIACRCGMVDHOTQ-UHFFFAOYSA-M 0.000 abstract 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical compound [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 abstract 2
- CWERGRDVMFNCDR-UHFFFAOYSA-N thioglycolic acid Chemical compound OC(=O)CS CWERGRDVMFNCDR-UHFFFAOYSA-N 0.000 abstract 2
- DHCDFWKWKRSZHF-UHFFFAOYSA-L thiosulfate(2-) Chemical compound [O-]S([S-])(=O)=O DHCDFWKWKRSZHF-UHFFFAOYSA-L 0.000 abstract 2
- DEWLEGDTCGBNGU-UHFFFAOYSA-N 1,3-dichloropropan-2-ol Chemical compound ClCC(O)CCl DEWLEGDTCGBNGU-UHFFFAOYSA-N 0.000 abstract 1
- QCRXMCYOAXNLAE-UHFFFAOYSA-N 1-(disulfanyl)butane Chemical compound CCCCSS QCRXMCYOAXNLAE-UHFFFAOYSA-N 0.000 abstract 1
- UHXXNUYGEDYXGD-UHFFFAOYSA-N 1-methylsulfanylselanylpropane Chemical compound CCC[Se]SC UHXXNUYGEDYXGD-UHFFFAOYSA-N 0.000 abstract 1
- BXVSAYBZSGIURM-UHFFFAOYSA-N 2-phenoxy-4h-1,3,2$l^{5}-benzodioxaphosphinine 2-oxide Chemical compound O1CC2=CC=CC=C2OP1(=O)OC1=CC=CC=C1 BXVSAYBZSGIURM-UHFFFAOYSA-N 0.000 abstract 1
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 abstract 1
- CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 abstract 1
- CETBSQOFQKLHHZ-UHFFFAOYSA-N Diethyl disulfide Chemical compound CCSSCC CETBSQOFQKLHHZ-UHFFFAOYSA-N 0.000 abstract 1
- YBARCVKHBGMMGC-UHFFFAOYSA-N N#C[SeH].O=S1(CCCC1)=O Chemical compound N#C[SeH].O=S1(CCCC1)=O YBARCVKHBGMMGC-UHFFFAOYSA-N 0.000 abstract 1
- 229910002651 NO3 Inorganic materials 0.000 abstract 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 abstract 1
- 229910019142 PO4 Inorganic materials 0.000 abstract 1
- 229920002873 Polyethylenimine Polymers 0.000 abstract 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 abstract 1
- JKNZUZCGFROMAZ-UHFFFAOYSA-L [Ag+2].[O-]S([O-])(=O)=O Chemical compound [Ag+2].[O-]S([O-])(=O)=O JKNZUZCGFROMAZ-UHFFFAOYSA-L 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 229910052936 alkali metal sulfate Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 229910052921 ammonium sulfate Inorganic materials 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- RMCHRYNDVIBPBP-UHFFFAOYSA-N benzyl-hydroxy-oxo-selanylidene-lambda6-sulfane Chemical compound [SeH]S(=O)(=O)CC1=CC=CC=C1 RMCHRYNDVIBPBP-UHFFFAOYSA-N 0.000 abstract 1
- 239000004305 biphenyl Substances 0.000 abstract 1
- 235000010290 biphenyl Nutrition 0.000 abstract 1
- 125000006267 biphenyl group Chemical group 0.000 abstract 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 abstract 1
- 239000004327 boric acid Substances 0.000 abstract 1
- 239000000919 ceramic Substances 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 235000011187 glycerol Nutrition 0.000 abstract 1
- 125000000623 heterocyclic group Chemical group 0.000 abstract 1
- 125000004433 nitrogen atom Chemical group N* 0.000 abstract 1
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 abstract 1
- 150000002894 organic compounds Chemical class 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 abstract 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 abstract 1
- 239000010452 phosphate Substances 0.000 abstract 1
- 239000004033 plastic Substances 0.000 abstract 1
- 229920003023 plastic Polymers 0.000 abstract 1
- 229920000333 poly(propyleneimine) Polymers 0.000 abstract 1
- 229920000573 polyethylene Polymers 0.000 abstract 1
- 229920000642 polymer Polymers 0.000 abstract 1
- 238000006116 polymerization reaction Methods 0.000 abstract 1
- 229910052700 potassium Inorganic materials 0.000 abstract 1
- KYEKHFSRAXRJBR-UHFFFAOYSA-M potassium;selenocyanate Chemical compound [K+].[Se-]C#N KYEKHFSRAXRJBR-UHFFFAOYSA-M 0.000 abstract 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 abstract 1
- UXAKYQHJRPCIOZ-UHFFFAOYSA-N propyl selenocyanate Chemical compound CCC[Se]C#N UXAKYQHJRPCIOZ-UHFFFAOYSA-N 0.000 abstract 1
- JUJWROOIHBZHMG-UHFFFAOYSA-N pyridine Substances C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 abstract 1
- WQGWDDDVZFFDIG-UHFFFAOYSA-N pyrogallol Chemical compound OC1=CC=CC(O)=C1O WQGWDDDVZFFDIG-UHFFFAOYSA-N 0.000 abstract 1
- 150000003335 secondary amines Chemical class 0.000 abstract 1
- 150000003378 silver Chemical class 0.000 abstract 1
- LFAGQMCIGQNPJG-UHFFFAOYSA-N silver cyanide Chemical compound [Ag+].N#[C-] LFAGQMCIGQNPJG-UHFFFAOYSA-N 0.000 abstract 1
- 229940098221 silver cyanide Drugs 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
- RWSOTUBLDIXVET-UHFFFAOYSA-O sulfonium Chemical compound [SH3+] RWSOTUBLDIXVET-UHFFFAOYSA-O 0.000 abstract 1
- KKHYGJFAHMJREW-UHFFFAOYSA-N triethylselanium Chemical compound CC[Se+](CC)CC KKHYGJFAHMJREW-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/46—Electroplating: Baths therefor from solutions of silver
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electroplating And Plating Baths Therefor (AREA)
- Conductive Materials (AREA)
- Manufacture And Refinement Of Metals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2410441A DE2410441C2 (de) | 1974-03-01 | 1974-03-01 | Cyanidfreies Bad und Verfahren zur galvanischen Abscheidung von Silber |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1449792A true GB1449792A (en) | 1976-09-15 |
Family
ID=5909129
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB874175A Expired GB1449792A (en) | 1974-03-01 | 1975-03-03 | Cyanide-free electrolyte for the electrodeposition of silver |
Country Status (22)
| Country | Link |
|---|---|
| US (1) | US3984292A (en, 2012) |
| JP (1) | JPS5413213B2 (en, 2012) |
| AR (1) | AR209761A1 (en, 2012) |
| AT (1) | AT332694B (en, 2012) |
| AU (1) | AU497419B2 (en, 2012) |
| CA (1) | CA1042836A (en, 2012) |
| CH (1) | CH606500A5 (en, 2012) |
| CS (1) | CS178182B2 (en, 2012) |
| DD (1) | DD114283A5 (en, 2012) |
| DE (1) | DE2410441C2 (en, 2012) |
| ES (1) | ES431700A1 (en, 2012) |
| FR (1) | FR2262705B1 (en, 2012) |
| GB (1) | GB1449792A (en, 2012) |
| HU (1) | HU171683B (en, 2012) |
| IE (1) | IE40688B1 (en, 2012) |
| IT (1) | IT1033325B (en, 2012) |
| NL (1) | NL7502446A (en, 2012) |
| RO (1) | RO68472A (en, 2012) |
| SE (1) | SE413038B (en, 2012) |
| SU (1) | SU612641A3 (en, 2012) |
| YU (1) | YU36764B (en, 2012) |
| ZA (1) | ZA751274B (en, 2012) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4376682A (en) * | 1980-04-07 | 1983-03-15 | Tdc Technology Development Corporation | Method for producing smooth coherent metal chalconide films |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4153519A (en) * | 1976-02-04 | 1979-05-08 | Hitachi, Ltd. | Silver-electroplating method using thiocyanic solution |
| US4067784A (en) * | 1976-06-09 | 1978-01-10 | Oxy Metal Industries Corporation | Non-cyanide acidic silver electroplating bath and additive therefore |
| CA1081651A (en) * | 1976-06-09 | 1980-07-15 | John M. Deuber | Non-cyanide electrodeposition of silver |
| US4121982A (en) * | 1978-02-03 | 1978-10-24 | American Chemical & Refining Company Incorporated | Gold alloy plating bath and method |
| US4155817A (en) * | 1978-08-11 | 1979-05-22 | American Chemical And Refining Company, Inc. | Low free cyanide high purity silver electroplating bath and method |
| BR8001854A (pt) * | 1979-04-04 | 1980-11-18 | Engelhard Min & Chem | Banho de revestimento de prata ou liga da mesma e respectivo processo de estabilizacao |
| JPS61195985A (ja) * | 1985-02-25 | 1986-08-30 | Nippon Engeruharudo Kk | 無光沢高速銀めつき液 |
| JPS61195986A (ja) * | 1985-02-25 | 1986-08-30 | Nippon Engeruharudo Kk | 無光沢高速銀めつき液 |
| US5302278A (en) * | 1993-02-19 | 1994-04-12 | Learonal, Inc. | Cyanide-free plating solutions for monovalent metals |
| GB0508188D0 (en) * | 2005-04-22 | 2005-06-01 | Eastman Kodak Co | Method of forming conductive tracks |
| DE102006004826B4 (de) * | 2006-01-31 | 2013-12-05 | Qimonda Ag | Metall- und Cyanid-Ionen-freie Ätzlösung zur nasschemischen Strukturierung von Metallschichten in der Halbleiterindustrie und deren Verwendung in einem Ätzverfahren |
| RU2323276C2 (ru) * | 2006-03-23 | 2008-04-27 | Закрытое акционерное общество "Драгцветмет" (ЗАО "Драгцветмет") | Электролит серебрения |
| US20130023166A1 (en) * | 2011-07-20 | 2013-01-24 | Tyco Electronics Corporation | Silver plated electrical contact |
| CN103866355A (zh) * | 2014-04-03 | 2014-06-18 | 苏州大学 | 无氰电镀银溶液及其电镀方法 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1857507A (en) * | 1929-10-22 | 1932-05-10 | Eastman Kodak Co | Process for the separation of silver by electrolysis |
-
1974
- 1974-03-01 DE DE2410441A patent/DE2410441C2/de not_active Expired
- 1974-09-12 CH CH1243074A patent/CH606500A5/xx not_active IP Right Cessation
- 1974-10-10 DD DD181617A patent/DD114283A5/xx unknown
- 1974-10-28 YU YU2873/74A patent/YU36764B/xx unknown
- 1974-10-30 SU SU742073760A patent/SU612641A3/ru active
- 1974-11-01 CS CS7481A patent/CS178182B2/cs unknown
- 1974-11-06 ES ES431700A patent/ES431700A1/es not_active Expired
- 1974-11-14 SE SE7414331A patent/SE413038B/xx unknown
- 1974-12-21 JP JP14750474A patent/JPS5413213B2/ja not_active Expired
-
1975
- 1975-01-23 US US05/543,206 patent/US3984292A/en not_active Expired - Lifetime
- 1975-02-25 IE IE383/75A patent/IE40688B1/xx unknown
- 1975-02-26 AU AU78605/75A patent/AU497419B2/en not_active Expired
- 1975-02-27 AT AT152075A patent/AT332694B/de not_active IP Right Cessation
- 1975-02-28 AR AR257813A patent/AR209761A1/es active
- 1975-02-28 IT IT20806/75A patent/IT1033325B/it active
- 1975-02-28 HU HU75SCHE511A patent/HU171683B/hu unknown
- 1975-02-28 RO RO7581527A patent/RO68472A/ro unknown
- 1975-02-28 ZA ZA00751274A patent/ZA751274B/xx unknown
- 1975-02-28 NL NL7502446A patent/NL7502446A/xx not_active Application Discontinuation
- 1975-03-03 CA CA222,175A patent/CA1042836A/en not_active Expired
- 1975-03-03 FR FR7506530A patent/FR2262705B1/fr not_active Expired
- 1975-03-03 GB GB874175A patent/GB1449792A/en not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4376682A (en) * | 1980-04-07 | 1983-03-15 | Tdc Technology Development Corporation | Method for producing smooth coherent metal chalconide films |
Also Published As
| Publication number | Publication date |
|---|---|
| YU36764B (en) | 1984-08-31 |
| JPS5413213B2 (en, 2012) | 1979-05-29 |
| AT332694B (de) | 1976-10-11 |
| FR2262705B1 (en, 2012) | 1978-04-21 |
| CS178182B2 (en, 2012) | 1977-08-31 |
| IE40688L (en) | 1975-09-01 |
| SE413038B (sv) | 1980-03-31 |
| JPS50120435A (en, 2012) | 1975-09-20 |
| HU171683B (hu) | 1978-02-28 |
| DD114283A5 (en, 2012) | 1975-07-20 |
| DE2410441A1 (de) | 1975-09-04 |
| NL7502446A (nl) | 1975-09-03 |
| AU7860575A (en) | 1976-08-26 |
| RO68472A (ro) | 1981-09-24 |
| ZA751274B (en) | 1976-01-28 |
| ATA152075A (de) | 1976-01-15 |
| IT1033325B (it) | 1979-07-10 |
| ES431700A1 (es) | 1976-09-16 |
| AU497419B2 (en) | 1978-12-14 |
| CH606500A5 (en, 2012) | 1978-10-31 |
| SU612641A3 (ru) | 1978-06-25 |
| FR2262705A1 (en, 2012) | 1975-09-26 |
| YU287374A (en) | 1982-06-18 |
| AR209761A1 (es) | 1977-05-31 |
| IE40688B1 (en) | 1979-08-01 |
| DE2410441C2 (de) | 1982-11-11 |
| CA1042836A (en) | 1978-11-21 |
| US3984292A (en) | 1976-10-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |