GB1430006A - Method of extracting lactams from acidic reaction mixtures - Google Patents
Method of extracting lactams from acidic reaction mixturesInfo
- Publication number
- GB1430006A GB1430006A GB3045773A GB3045773A GB1430006A GB 1430006 A GB1430006 A GB 1430006A GB 3045773 A GB3045773 A GB 3045773A GB 3045773 A GB3045773 A GB 3045773A GB 1430006 A GB1430006 A GB 1430006A
- Authority
- GB
- United Kingdom
- Prior art keywords
- amylphenol
- lactams
- sec
- phenol
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000003951 lactams Chemical class 0.000 title abstract 4
- 230000002378 acidificating effect Effects 0.000 title abstract 2
- 239000011541 reaction mixture Substances 0.000 title abstract 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 3
- CRBJBYGJVIBWIY-UHFFFAOYSA-N 2-isopropylphenol Chemical compound CC(C)C1=CC=CC=C1O CRBJBYGJVIBWIY-UHFFFAOYSA-N 0.000 abstract 2
- VLJSLTNSFSOYQR-UHFFFAOYSA-N 3-propan-2-ylphenol Chemical compound CC(C)C1=CC=CC(O)=C1 VLJSLTNSFSOYQR-UHFFFAOYSA-N 0.000 abstract 2
- YQUQWHNMBPIWGK-UHFFFAOYSA-N 4-isopropylphenol Chemical compound CC(C)C1=CC=C(O)C=C1 YQUQWHNMBPIWGK-UHFFFAOYSA-N 0.000 abstract 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 2
- 239000003929 acidic solution Substances 0.000 abstract 2
- -1 caprolactam Chemical class 0.000 abstract 2
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 abstract 2
- 239000000243 solution Substances 0.000 abstract 2
- 235000011149 sulphuric acid Nutrition 0.000 abstract 2
- 239000001117 sulphuric acid Substances 0.000 abstract 2
- YHOMKYYXCBXANK-UHFFFAOYSA-N 2,3-di(pentan-2-yl)phenol Chemical compound CCCC(C)C1=CC=CC(O)=C1C(C)CCC YHOMKYYXCBXANK-UHFFFAOYSA-N 0.000 abstract 1
- WMVJWKURWRGJCI-UHFFFAOYSA-N 2,4-bis(2-methylbutan-2-yl)phenol Chemical compound CCC(C)(C)C1=CC=C(O)C(C(C)(C)CC)=C1 WMVJWKURWRGJCI-UHFFFAOYSA-N 0.000 abstract 1
- BGRKGHSKCFAPCL-UHFFFAOYSA-N 2-(2-methylbutan-2-yl)phenol Chemical compound CCC(C)(C)C1=CC=CC=C1O BGRKGHSKCFAPCL-UHFFFAOYSA-N 0.000 abstract 1
- ROMXEVFSCNLHAB-UHFFFAOYSA-N 2-pentan-2-ylphenol Chemical compound CCCC(C)C1=CC=CC=C1O ROMXEVFSCNLHAB-UHFFFAOYSA-N 0.000 abstract 1
- WJQOZHYUIDYNHM-UHFFFAOYSA-N 2-tert-Butylphenol Chemical compound CC(C)(C)C1=CC=CC=C1O WJQOZHYUIDYNHM-UHFFFAOYSA-N 0.000 abstract 1
- JTHGIRIGZAGNOX-UHFFFAOYSA-N 4-pentan-2-ylphenol Chemical compound CCCC(C)C1=CC=C(O)C=C1 JTHGIRIGZAGNOX-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 125000004432 carbon atom Chemical group C* 0.000 abstract 1
- 230000000694 effects Effects 0.000 abstract 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 150000002989 phenols Chemical class 0.000 abstract 1
- 125000001424 substituent group Chemical group 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/16—Separation or purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Other In-Based Heterocyclic Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Hydrogenated Pyridines (AREA)
- Extraction Or Liquid Replacement (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Plant Substances (AREA)
- Separation By Low-Temperature Treatments (AREA)
- Polyamides (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Pyrrole Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT26384/72A IT956940B (it) | 1972-06-28 | 1972-06-28 | Procedimento per l estrazione di lattami da miscele acide di rea zione |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1430006A true GB1430006A (en) | 1976-03-31 |
Family
ID=11219370
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB3045773A Expired GB1430006A (en) | 1972-06-28 | 1973-06-27 | Method of extracting lactams from acidic reaction mixtures |
Country Status (23)
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1998041502A1 (en) * | 1997-03-17 | 1998-09-24 | Dsm N.V. | Process for purifying caprolactam |
| CN102335573A (zh) * | 2010-07-23 | 2012-02-01 | 中国石油化工股份有限公司 | 一种己内酰胺苛化装置 |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4013640A (en) * | 1974-04-11 | 1977-03-22 | Union Carbide Corporation | Process for the recovery of amides |
| DE2926279A1 (de) * | 1979-06-29 | 1981-01-08 | Basf Ag | Verfahren zur reinigung von caprolactam |
| US4328154A (en) * | 1980-11-03 | 1982-05-04 | Snia Viscosa Societa' Nazionale Industria Applicazioni Viscosa S.P.A. | Process for the purification of raw caprolactam |
| DE3834904A1 (de) * | 1988-10-13 | 1990-04-19 | Hoechst Ag | Verfahren zur extraktion von n-methyl-pyrrolidon-(2) |
| NL1000781C2 (nl) * | 1995-07-12 | 1997-01-14 | Dsm Nv | Werkwijze voor het winnen van caprolactam uit nylon-6 bevattende afval. |
| EP0826665A1 (en) * | 1996-09-02 | 1998-03-04 | Dsm N.V. | Recovery of epsilon-caprolactam from aqueous mixtures |
| TW420662B (en) * | 1996-02-17 | 2001-02-01 | Du Pont | Recovery of <epsilon>-caprolactam |
| TW201114740A (en) | 2009-10-30 | 2011-05-01 | China Petrochemical Dev Corp Taipei Taiwan | Method of separating amide from amino acid ionic solution |
| TWI414508B (zh) | 2011-01-17 | 2013-11-11 | China Petrochemical Dev Corp Taipei Taiwan | A catalyst composition and a method for preparing an amide using the composition |
| EP3055283A4 (en) * | 2013-10-07 | 2017-05-17 | GFBiochemicals Limited | Process to prepare levulinic acid |
| CN104262252A (zh) * | 2014-10-21 | 2015-01-07 | 湖南百利工程科技股份有限公司 | 一种从己内酰胺硫酸酯中分离己内酰胺和硫酸的方法 |
| CN104387322A (zh) * | 2014-10-21 | 2015-03-04 | 湖南百利工程科技股份有限公司 | 一种低副产硫酸铵的己内酰胺的制备方法 |
| CN104910071A (zh) * | 2015-05-08 | 2015-09-16 | 河北美邦工程科技股份有限公司 | 一种制备己内酰胺的方法 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH78A (de) * | 1889-01-18 | August Graemiger Anton | Apparat zum Färben, Waschen, Bleichen u. s. w., von Garn in aufgewickeltem Zustande | |
| CH446342A (de) * | 1963-11-29 | 1967-11-15 | Bayer Ag | Verfahren zum Herstellen reiner Lactame |
-
1972
- 1972-06-28 IT IT26384/72A patent/IT956940B/it active
-
1973
- 1973-06-25 NO NO2630/73A patent/NO143220C/no unknown
- 1973-06-26 US US373799A patent/US3912721A/en not_active Expired - Lifetime
- 1973-06-26 ZA ZA734342A patent/ZA734342B/xx unknown
- 1973-06-27 GB GB3045773A patent/GB1430006A/en not_active Expired
- 1973-06-27 DK DK356573*A patent/DK133150C/da active
- 1973-06-27 SU SU1937628A patent/SU557754A3/ru active
- 1973-06-27 CH CH940773A patent/CH602632A5/xx not_active IP Right Cessation
- 1973-06-27 IE IE1074/73A patent/IE37857B1/xx unknown
- 1973-06-28 AR AR248801A patent/AR197617A1/es active
- 1973-06-28 AU AU57449/73A patent/AU475133B2/en not_active Expired
- 1973-06-28 BE BE132858A patent/BE801610A/xx unknown
- 1973-06-28 JP JP7235473A patent/JPS5544067B2/ja not_active Expired
- 1973-06-28 TR TR17560A patent/TR17560A/xx unknown
- 1973-06-28 BR BR4800/73A patent/BR7304800D0/pt unknown
- 1973-06-28 AT AT569973A patent/AT326676B/de active
- 1973-06-28 NL NL7309031A patent/NL7309031A/xx not_active Application Discontinuation
- 1973-06-28 DE DE2332973A patent/DE2332973A1/de not_active Ceased
- 1973-06-28 IN IN1513/CAL/1973A patent/IN139738B/en unknown
- 1973-06-28 ES ES416415A patent/ES416415A1/es not_active Expired
- 1973-06-28 CA CA175,181A patent/CA1018524A/en not_active Expired
- 1973-06-28 FR FR7323688A patent/FR2190821B1/fr not_active Expired
- 1973-07-06 IL IL42677A patent/IL42677A/en unknown
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1998041502A1 (en) * | 1997-03-17 | 1998-09-24 | Dsm N.V. | Process for purifying caprolactam |
| US6448395B1 (en) | 1997-03-17 | 2002-09-10 | Dsm N.V. | Process for purifying caprolactam |
| CN102335573A (zh) * | 2010-07-23 | 2012-02-01 | 中国石油化工股份有限公司 | 一种己内酰胺苛化装置 |
Also Published As
| Publication number | Publication date |
|---|---|
| NO143220B (no) | 1980-09-22 |
| ATA569973A (de) | 1975-03-15 |
| TR17560A (tr) | 1975-07-23 |
| IL42677A (en) | 1976-06-30 |
| SU557754A3 (ru) | 1977-05-05 |
| AU5744973A (en) | 1975-01-09 |
| CH602632A5 (enrdf_load_html_response) | 1978-07-31 |
| US3912721A (en) | 1975-10-14 |
| NL7309031A (enrdf_load_html_response) | 1974-01-02 |
| CA1018524A (en) | 1977-10-04 |
| NO143220C (no) | 1981-01-02 |
| IT956940B (it) | 1973-10-10 |
| AR197617A1 (es) | 1974-04-23 |
| IN139738B (enrdf_load_html_response) | 1976-07-24 |
| IE37857B1 (en) | 1977-10-26 |
| JPS5544067B2 (enrdf_load_html_response) | 1980-11-10 |
| ZA734342B (en) | 1974-05-29 |
| BR7304800D0 (pt) | 1974-09-05 |
| BE801610A (fr) | 1973-12-28 |
| JPS4955683A (enrdf_load_html_response) | 1974-05-30 |
| DK133150C (da) | 1976-08-30 |
| ES416415A1 (es) | 1976-03-01 |
| IE37857L (en) | 1973-12-28 |
| DK133150B (da) | 1976-03-29 |
| FR2190821A1 (enrdf_load_html_response) | 1974-02-01 |
| DE2332973A1 (de) | 1974-01-10 |
| AT326676B (de) | 1975-12-29 |
| AU475133B2 (en) | 1976-08-12 |
| FR2190821B1 (enrdf_load_html_response) | 1978-12-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |