GB1322701A - Apparatus for converting liquid fatty nitriles to amines - Google Patents
Apparatus for converting liquid fatty nitriles to aminesInfo
- Publication number
- GB1322701A GB1322701A GB1322701DA GB1322701A GB 1322701 A GB1322701 A GB 1322701A GB 1322701D A GB1322701D A GB 1322701DA GB 1322701 A GB1322701 A GB 1322701A
- Authority
- GB
- United Kingdom
- Prior art keywords
- coolant
- valve
- line
- reactants
- surge drum
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
- C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00083—Coils
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1322701 Temperature control of exothermic reactions N WADDLETON (ANDERSON LUEDEKA FITCH EVEN & TABIN) 29 June 1970 [1 April 1969] 16930/69 Heading B1X Exothermic reactions are controlled by means of indirect cooling fed from a constant level surge drum, wherein any coolant losses due to evaporation are replenished with fresh coolant. In the particular application of converting fatty nitriles to amines reactants are fed into a reactor 1 via an inlet 6, and stirrer 29 is started. The mixture is first heated by passing steam through coil 31 and any excessive condensate collecting in surge drum 32 is removed via lines 36, 50. Pressure control 66 opens valve 34 to atmosphere during this time. Pump 22 circulates the reactants via line 7, heater 2 and header 21 and when the reactants are at the required temperature the valve 34 is closed and the steam heating stopped by closing valve 55. Hydrogen is then introduced into the reactor via sparger 15 and NH 3 through line 16. Heat emitted is controlled by passing a coolant, e.g. H 2 O through the surge drum 32, line 36 and the coil 31. Any coolant vaporising is vented via pressure relief line 33 whereupon the level in drum 32 drops. The level controller 35 then causes valve 40 to open to admit make up coolant. Upon completion of the reaction valves 34, 51 are opened and valve 52 is closed so that the mixture may be further cooled.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1693069 | 1969-04-01 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1322701A true GB1322701A (en) | 1973-07-11 |
Family
ID=10086226
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1322701D Expired GB1322701A (en) | 1969-04-01 | 1969-04-01 | Apparatus for converting liquid fatty nitriles to amines |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB1322701A (en) |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0070797A2 (en) * | 1981-07-16 | 1983-01-26 | Buss Ag | Installation using a loop-type reactor and process by which a liquid educt is subjected to a chemical reaction in a circulatory manner |
FR2632718A1 (en) * | 1988-06-08 | 1989-12-15 | Chinoin Gyogyszer Es Vegyeszet | DEVICE FOR IMPLEMENTING THERMAL METHODS |
DE3826320A1 (en) * | 1988-08-03 | 1990-02-08 | Henkel Kgaa | Method for guiding a reaction proceeding at elevated temperature and apparatus for producing thermally sensitive products at elevated temperatures |
US5110508A (en) * | 1988-04-22 | 1992-05-05 | Henkel Kommanditgesellschaft Auf Aktien | Process and apparatus for making a heat-sensitive material |
CN108273452A (en) * | 2018-01-30 | 2018-07-13 | 浙江工业大学 | A kind of grease epoxidation reactor |
WO2018177400A1 (en) * | 2017-03-31 | 2018-10-04 | 北京中科诚毅科技发展有限公司 | Temperature and pressure control method for hydrogenation process, design method therefor and use thereof |
CN114917853A (en) * | 2022-05-11 | 2022-08-19 | 顶峰油脂化工(泰兴)有限公司 | Method for intermittent hydrogenation reaction |
-
1969
- 1969-04-01 GB GB1322701D patent/GB1322701A/en not_active Expired
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0070797A2 (en) * | 1981-07-16 | 1983-01-26 | Buss Ag | Installation using a loop-type reactor and process by which a liquid educt is subjected to a chemical reaction in a circulatory manner |
EP0070797A3 (en) * | 1981-07-16 | 1984-02-22 | Buss Ag | Installation using a loop-type reactor and process by which a liquid educt is subjected to a chemical reaction in a circulatory manner |
US5110508A (en) * | 1988-04-22 | 1992-05-05 | Henkel Kommanditgesellschaft Auf Aktien | Process and apparatus for making a heat-sensitive material |
FR2632718A1 (en) * | 1988-06-08 | 1989-12-15 | Chinoin Gyogyszer Es Vegyeszet | DEVICE FOR IMPLEMENTING THERMAL METHODS |
DE3826320A1 (en) * | 1988-08-03 | 1990-02-08 | Henkel Kgaa | Method for guiding a reaction proceeding at elevated temperature and apparatus for producing thermally sensitive products at elevated temperatures |
WO2018177400A1 (en) * | 2017-03-31 | 2018-10-04 | 北京中科诚毅科技发展有限公司 | Temperature and pressure control method for hydrogenation process, design method therefor and use thereof |
CN108273452A (en) * | 2018-01-30 | 2018-07-13 | 浙江工业大学 | A kind of grease epoxidation reactor |
CN108273452B (en) * | 2018-01-30 | 2023-09-26 | 浙江工业大学 | Grease epoxidation reactor |
CN114917853A (en) * | 2022-05-11 | 2022-08-19 | 顶峰油脂化工(泰兴)有限公司 | Method for intermittent hydrogenation reaction |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
PLNP | Patent lapsed through nonpayment of renewal fees |