GB1167554A - Sample Dividing Apparatus for use in Gas Analysis - Google Patents

Sample Dividing Apparatus for use in Gas Analysis

Info

Publication number
GB1167554A
GB1167554A GB32357/67A GB3235767A GB1167554A GB 1167554 A GB1167554 A GB 1167554A GB 32357/67 A GB32357/67 A GB 32357/67A GB 3235767 A GB3235767 A GB 3235767A GB 1167554 A GB1167554 A GB 1167554A
Authority
GB
United Kingdom
Prior art keywords
gas
flow
passes
nozzle
space
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB32357/67A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Scholven Chemie AG
Original Assignee
Scholven Chemie AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Scholven Chemie AG filed Critical Scholven Chemie AG
Publication of GB1167554A publication Critical patent/GB1167554A/en
Expired legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/38—Flow patterns
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/04—Preparation or injection of sample to be analysed
    • G01N30/06—Preparation
    • G01N30/10—Preparation using a splitter

Landscapes

  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)

Abstract

1,167,554. Gas chromatography. SCHOLVEN-CHEMIE A.G. 13 July, 1967 [16 July, 1966], No. 32357/67. Heading B1L. A specimen divider for gas chromatographs comprises a compensatory flow branch interposed between the main gas flow and one of the partial flow branches which is operable to vary the composition in the partial flow branches so as to compensate for the kinetic change in composition which occurs at the point of division of the main flow into the partial flow branches. Thus, sample is introduced at 4 into the carrier gas stream and the mixture is carried past mixing devices 6. 8 to nozzle 10 whence it passes down tube 14 and back up through annular space 18. A proportion of the gas stream is bled off at 16 and passes through capillary column 26 and thence to flame ionization detector 28. Of the gas which passes upwards through space 18. part is recycled through compensatory gap 12 under the suction effect created by the flow through nozzle 10; the remainder passes to expansion chamber 20, and through needle valve 22 to outlet 24. The dimensions of tube 14, nozzle 10, space 18 and gap 12 are determined empirically.
GB32357/67A 1966-07-16 1967-07-13 Sample Dividing Apparatus for use in Gas Analysis Expired GB1167554A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE1966SC039271 DE1673068B2 (en) 1966-07-16 1966-07-16 DEVICE FOR APPLYING A GAS ANALYZER, IN PARTICULAR A GAS CHROMATOGRAPH, WITH A PARTIAL QUANTITY OF A MAIN GAS FLOW

Publications (1)

Publication Number Publication Date
GB1167554A true GB1167554A (en) 1969-10-15

Family

ID=7435086

Family Applications (1)

Application Number Title Priority Date Filing Date
GB32357/67A Expired GB1167554A (en) 1966-07-16 1967-07-13 Sample Dividing Apparatus for use in Gas Analysis

Country Status (5)

Country Link
US (1) US3513636A (en)
CH (1) CH452934A (en)
DE (1) DE1673068B2 (en)
GB (1) GB1167554A (en)
NL (1) NL157718B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0624251A1 (en) * 1992-01-30 1994-11-17 Baker Hughes Incorporated Sample dispersing apparatus and method for use with pyrolysis furnace

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL6904800A (en) * 1969-03-28 1970-09-30
DE2620756C3 (en) * 1976-05-11 1979-03-22 Siemens Ag, 1000 Berlin Und 8000 Muenchen Sample injection device for process gas chromatography with capillary columns and operating methods for such a device
JPS5643557A (en) * 1979-09-19 1981-04-22 Hitachi Ltd Sample divider
DE3132638A1 (en) * 1981-08-18 1983-03-10 Vsesojuznyj naučno-issledovatel'skij i konstruktorskij institut chromatografii, Moskva Method for introducing samples into a gas chromatograph, and device for carrying out this method
DE3708504A1 (en) * 1987-03-16 1988-09-29 Siemens Ag DEVICE FOR DIVIDING THE GAS CHROMATOGRAPHIC ANALYSIS
US4766760A (en) * 1987-11-03 1988-08-30 Vsesojuzny Nauchno-Issledovatelsky I Konstruktorsky Istitute Khromatografii Method of chromatographic analysis of a mixture of liquid substances and a gas chromatograph for carrying out the method
US5047073A (en) * 1990-02-27 1991-09-10 Transducer Research, Inc. Sorption separation apparatus and methods
ITMI20012840A1 (en) * 2001-12-28 2003-06-28 Thermoquest Italia Spa METHOD AND APPARATUS FOR INJECTION BY VAPORIZATION OF HIGH VOLUMES IN GAS-CHROMATOGRAPHIC ANALYSIS
US6814785B2 (en) * 2002-07-24 2004-11-09 Perkinelmer Instruments Llc Analyte pre-concentrator for gas chromatography
JP2014228276A (en) 2013-05-17 2014-12-08 アズビル株式会社 Particle detection device and particle detection method
CN106168612B (en) * 2016-08-31 2017-09-12 许继集团有限公司 A kind of gas analysis sampling device

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2267354A (en) * 1940-02-02 1941-12-23 Northon Louis Irving Prevention of reverse flow in water supply systems
US3103942A (en) * 1961-09-22 1963-09-17 Du Pont Apparatus and process for distributing viscous liquids
US3357233A (en) * 1964-10-05 1967-12-12 Phillips Petroleum Co Fluid control system for analyzers

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0624251A1 (en) * 1992-01-30 1994-11-17 Baker Hughes Incorporated Sample dispersing apparatus and method for use with pyrolysis furnace
EP0624251A4 (en) * 1992-01-30 1995-01-18 Baker Hughes Inc Sample dispersing apparatus and method for use with pyrolysis furnace.

Also Published As

Publication number Publication date
DE1673068A1 (en) 1971-07-08
CH452934A (en) 1968-03-15
NL157718B (en) 1978-08-15
US3513636A (en) 1970-05-26
NL6708613A (en) 1968-01-17
DE1673068B2 (en) 1976-07-01

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Legal Events

Date Code Title Description
PS Patent sealed [section 19, patents act 1949]
PCNP Patent ceased through non-payment of renewal fee