GB1065131A - The analysis of gases - Google Patents

The analysis of gases

Info

Publication number
GB1065131A
GB1065131A GB16411/65A GB1641165A GB1065131A GB 1065131 A GB1065131 A GB 1065131A GB 16411/65 A GB16411/65 A GB 16411/65A GB 1641165 A GB1641165 A GB 1641165A GB 1065131 A GB1065131 A GB 1065131A
Authority
GB
United Kingdom
Prior art keywords
gas
bodies
april
spectrometer
conduit
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB16411/65A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Pfizer Health AB
Original Assignee
LKB Produkter AB
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by LKB Produkter AB filed Critical LKB Produkter AB
Publication of GB1065131A publication Critical patent/GB1065131A/en
Expired legal-status Critical Current

Links

Classifications

    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J49/00—Particle spectrometers or separator tubes
    • H01J49/02—Details
    • H01J49/04—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components
    • H01J49/0422—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components for gaseous samples
    • H01J49/0427—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components for gaseous samples using a membrane permeable to gases
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/62—Detectors specially adapted therefor
    • G01N30/72—Mass spectrometers
    • G01N30/7206—Mass spectrometers interfaced to gas chromatograph
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/84—Preparation of the fraction to be distributed
    • G01N2030/8423—Preparation of the fraction to be distributed using permeable separator tubes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
  • Electron Tubes For Measurement (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

1,065,131. Gas chromatography. LKB-PRODUKTER A.B. April 15, 1965 [April 20, 1964; April 21, 1964; Sept. 24, 1964], No. 16411/65. Heading B1L. A separator is arranged between a gas chromatographic column and a mass spectrometer which by removing the lighter molecules, mainly the carrier gas, by diffusion through a permeable wall 9 increases the concentration of the sample substance in the carrier gas entering the spectrometer. Gas is fed from the chromatographic column through conduit 1 to a channel 12 formed by annual bodies 9 of porous material divided into the groups by a wall 6 and from each other by metal washers 10. Non-porous bodies 11 are placed at each end and a perforated stainless steel tube 7 surrounds the bodies. Chambers 4 and 5 in a cylindrical member 3 enclosing the bodies are connected by tubes 14 and 15 to vacuum pumps to quicken diffusion through the bodies 9. The gas stream may be expanded prior or after it is passed through the channel 12 by a nozzle. Gas flow control means 16 and 17 may be provided. The gas leaves the device through conduit 2 to the spectrometer.
GB16411/65A 1964-04-21 1965-04-15 The analysis of gases Expired GB1065131A (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
SE491164 1964-04-21
SE502564 1964-04-23
SE1149864 1964-09-25

Publications (1)

Publication Number Publication Date
GB1065131A true GB1065131A (en) 1967-04-12

Family

ID=27354371

Family Applications (1)

Application Number Title Priority Date Filing Date
GB16411/65A Expired GB1065131A (en) 1964-04-21 1965-04-15 The analysis of gases

Country Status (2)

Country Link
US (1) US3479798A (en)
GB (1) GB1065131A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2194742A (en) * 1986-08-06 1988-03-16 British American Tobacco Co Gas chromatography

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3712111A (en) * 1968-07-10 1973-01-23 Vanan Ass Flow control for gas analyzing apparatus
US3589171A (en) * 1969-08-25 1971-06-29 California Inst Of Techn Gas analysis system and palladium tube separator therefor
US4791292A (en) * 1986-04-24 1988-12-13 The Dow Chemical Company Capillary membrane interface for a mass spectrometer
US4951503A (en) * 1990-01-23 1990-08-28 Niagara Mohawk Power Corporation Method and apparatus for determining the heating value of a gaseous fuel
CN105372362A (en) * 2015-11-27 2016-03-02 大连理工大学 Vacuum keeper for a gas chromatography-mass spectrometer

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1174631A (en) * 1914-09-17 1916-03-07 Walter O Snelling Apparatus for separating gases.
US2627933A (en) * 1947-06-28 1953-02-10 Sinclair Refining Co Aerogel diffusion unit
BE539578A (en) * 1955-10-05
US2892508A (en) * 1957-04-17 1959-06-30 Bell Telephone Labor Inc Separation of gases by diffusion
US2924630A (en) * 1957-06-28 1960-02-09 Union Oil Co Fluid diffusion fractionation
US3246449A (en) * 1959-06-09 1966-04-19 Union Carbide Corp Recovery of helium
US3104960A (en) * 1960-05-24 1963-09-24 Eitel Mccullough Inc Gas flow apparatus
US3239996A (en) * 1963-03-18 1966-03-15 Humble Oil & Refining Company Method of separating helium from other constituents of natural gas
FR1366968A (en) * 1963-06-07 1964-07-17 Commissariat Energie Atomique Diffuser for gas separation

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2194742A (en) * 1986-08-06 1988-03-16 British American Tobacco Co Gas chromatography

Also Published As

Publication number Publication date
US3479798A (en) 1969-11-25

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