GB1155724A - Manufacture of Detergent Laundry Bars - Google Patents
Manufacture of Detergent Laundry BarsInfo
- Publication number
- GB1155724A GB1155724A GB28957/66A GB2895766A GB1155724A GB 1155724 A GB1155724 A GB 1155724A GB 28957/66 A GB28957/66 A GB 28957/66A GB 2895766 A GB2895766 A GB 2895766A GB 1155724 A GB1155724 A GB 1155724A
- Authority
- GB
- United Kingdom
- Prior art keywords
- detergent
- neutralizing agent
- solid
- shearing
- shearing zone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000003599 detergent Substances 0.000 title abstract 9
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 238000010008 shearing Methods 0.000 abstract 5
- 239000000203 mixture Substances 0.000 abstract 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 4
- 239000002253 acid Substances 0.000 abstract 3
- 239000003795 chemical substances by application Substances 0.000 abstract 3
- 238000000034 method Methods 0.000 abstract 3
- 230000003472 neutralizing effect Effects 0.000 abstract 3
- 150000003839 salts Chemical class 0.000 abstract 3
- 239000007787 solid Substances 0.000 abstract 3
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical class OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 abstract 1
- 229920000388 Polyphosphate Polymers 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 150000001642 boronic acid derivatives Chemical class 0.000 abstract 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 abstract 1
- 230000001427 coherent effect Effects 0.000 abstract 1
- 239000000470 constituent Substances 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 239000001205 polyphosphate Substances 0.000 abstract 1
- 235000011176 polyphosphates Nutrition 0.000 abstract 1
- 150000004760 silicates Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/04—Special methods for preparing compositions containing mixtures of detergents by chemical means, e.g. by sulfonating in the presence of other compounding ingredients followed by neutralising
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/30—Mixing; Kneading continuous, with mechanical mixing or kneading devices
- B29B7/34—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices
- B29B7/38—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary
- B29B7/46—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft
- B29B7/48—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft with intermeshing devices, e.g. screws
- B29B7/482—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft with intermeshing devices, e.g. screws provided with screw parts in addition to other mixing parts, e.g. paddles, gears, discs
- B29B7/483—Mixing; Kneading continuous, with mechanical mixing or kneading devices with movable mixing or kneading devices rotary with more than one shaft with intermeshing devices, e.g. screws provided with screw parts in addition to other mixing parts, e.g. paddles, gears, discs the other mixing parts being discs perpendicular to the screw axis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/25—Component parts, details or accessories; Auxiliary operations
- B29C48/36—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die
- B29C48/375—Plasticisers, homogenisers or feeders comprising two or more stages
- B29C48/39—Plasticisers, homogenisers or feeders comprising two or more stages a first extruder feeding the melt into an intermediate location of a second extruder
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/25—Component parts, details or accessories; Auxiliary operations
- B29C48/36—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die
- B29C48/395—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die using screws surrounded by a cooperating barrel, e.g. single screw extruders
- B29C48/40—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die using screws surrounded by a cooperating barrel, e.g. single screw extruders using two or more parallel screws or at least two parallel non-intermeshing screws, e.g. twin screw extruders
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/25—Component parts, details or accessories; Auxiliary operations
- B29C48/36—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die
- B29C48/395—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die using screws surrounded by a cooperating barrel, e.g. single screw extruders
- B29C48/40—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die using screws surrounded by a cooperating barrel, e.g. single screw extruders using two or more parallel screws or at least two parallel non-intermeshing screws, e.g. twin screw extruders
- B29C48/405—Intermeshing co-rotating screws
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/25—Component parts, details or accessories; Auxiliary operations
- B29C48/36—Means for plasticising or homogenising the moulding material or forcing it through the nozzle or die
- B29C48/50—Details of extruders
- B29C48/505—Screws
- B29C48/57—Screws provided with kneading disc-like elements, e.g. with oval-shaped elements
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0047—Detergents in the form of bars or tablets
- C11D17/0065—Solid detergents containing builders
- C11D17/0069—Laundry bars
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
1,155,724. Process for detergent laundry bars. COLGATE-PALMOLIVE CO. 28 June, 1966 [2 July, 1965; 26 Nov., 1965; 21 Feb.. 1966 (2)], No. 28957/66. Heading C5D. A process for the manufacture of a coherent, solid, built detergent composition containing a minor proportion of a synthetic water soluble, anionic detergent and a proportion of a water soluble, solid builder salt in excess of the amount of the detergent, and water in an amount sufficient to plasticize the composition, which comprises continuously intensively shearing the constituent materials together while advancing the same through a shearing zone to form an intricate plastic blend which is continuously discharged from the shearing zone. The detergent may be supplied to the shearing zone in already neutralized form or as a liquid detergent acid and an alkaline neutralizing agent, in which the alkaline neutralizing agent is brought into contact with the builder salt before contact with the acid, the first two being either in the form of a solution, or as a solid with a separate stream of water. Specified builder salts are alkali metal polyphosphates, silicates, borates, carbonates and bicarbonates, in the case of the last two the neutralizing agent is such that the detergent acid reacts with it preferentially. Any conventional synthetic anionic detergent may be used, many of which are specified. The residence time in the shearing zone is desirably less than ten minutes and the blend is continuously extruded in a heated plastic condition in the form of shapes which are surface hardened by cooling and thereafter compacted and extruded in the form of a bar. Suitable apparatus for the process is given in Specification 1,155,725.
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB30218/68A GB1155725A (en) | 1965-07-02 | 1966-06-28 | Mixing and Extrusion Apparatus |
GB60927/68A GB1155726A (en) | 1965-07-02 | 1966-06-28 | Detergent Laundry Bars |
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US46914465A | 1965-07-02 | 1965-07-02 | |
US50980365A | 1965-11-26 | 1965-11-26 | |
US52908766A | 1966-02-21 | 1966-02-21 | |
US52915166A | 1966-02-21 | 1966-02-21 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1155724A true GB1155724A (en) | 1969-06-18 |
Family
ID=27504131
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB28957/66A Expired GB1155724A (en) | 1965-07-02 | 1966-06-28 | Manufacture of Detergent Laundry Bars |
Country Status (7)
Country | Link |
---|---|
US (2) | US3497912A (en) |
AT (2) | AT289275B (en) |
BE (1) | BE683383A (en) |
ES (1) | ES328199A1 (en) |
GB (1) | GB1155724A (en) |
NL (1) | NL6609217A (en) |
SE (1) | SE345875B (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2455887A1 (en) * | 1979-05-11 | 1980-12-05 | Mann & Schroeder Kg | BATH SALT |
GB2213827A (en) * | 1988-01-14 | 1989-08-23 | Unilever Plc | Detergent laundry bars |
GB2257649A (en) * | 1991-07-18 | 1993-01-20 | Apv Corp Ltd | Converting fine particlulate material to block form,by extrusion |
Families Citing this family (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3639286A (en) * | 1968-05-28 | 1972-02-01 | Mario Ballestra | Synthetic detergent in bar or cake form and the method to manufacture same |
US4141947A (en) * | 1975-01-09 | 1979-02-27 | Colgate-Palmolive Company | Continuous process for making variegated soap |
EP0038100B1 (en) * | 1980-04-11 | 1984-04-11 | Unilever N.V. | Machine dishwashing composition |
US4515707A (en) * | 1983-06-27 | 1985-05-07 | The Chemithon Corporation | Intermediate product for use in producing a detergent bar and method for producing same |
US4543204A (en) * | 1983-08-17 | 1985-09-24 | Colgate-Palmolive Company | Sodium higher fatty alkyl sulfate detergent laundry bars and process for manufacture thereof |
GB8327616D0 (en) * | 1983-10-14 | 1983-11-16 | Unilever Plc | Multi-coloured detergent bars |
US4844928A (en) * | 1985-03-27 | 1989-07-04 | Lever Brothers Company | Process for the preparation of an edible fat-containing product |
US4840810A (en) * | 1985-03-27 | 1989-06-20 | Lever Brothers Company | Process for the preparation of an edible fat-containing product |
US4933100A (en) * | 1988-01-19 | 1990-06-12 | Colgate-Palmolive Co. | Built synthetic organic detergent composition patties and processes for washing laundry therewith |
US5045238A (en) * | 1989-06-09 | 1991-09-03 | The Procter & Gamble Company | High active detergent particles which are dispersible in cold water |
US5156794A (en) * | 1990-06-27 | 1992-10-20 | Kao Corporation | Pulverizing/kneading apparatus and method for manufacturing soap using the pulverizing/kneading apparatus |
DE4122912A1 (en) * | 1991-07-11 | 1993-01-14 | Theysohn Friedrich Fa | DOUBLE SCREW EXTRUDER |
GB9402837D0 (en) * | 1994-02-15 | 1994-04-06 | Unilever Plc | Extruder |
US5759982A (en) * | 1994-06-17 | 1998-06-02 | The Procter & Gamble Company | Laundry bars with polyethylene glycol as a processing aid |
WO1996035772A1 (en) * | 1995-05-12 | 1996-11-14 | The Procter & Gamble Company | Soap-based laundry bars with improved firmness |
US5573697A (en) * | 1995-05-31 | 1996-11-12 | Riddick; Eric F. | Process for making high active, high density detergent granules |
DE19718292A1 (en) * | 1997-04-30 | 1998-11-05 | Krupp Werner & Pfleiderer Gmbh | Multi-shaft screw machine, in particular two-shaft extruder |
JP4445478B2 (en) * | 2006-03-10 | 2010-04-07 | 株式会社日本製鋼所 | Plasticizing and kneading extruder for plastic raw materials |
ATE468958T1 (en) * | 2006-12-14 | 2010-06-15 | Sulzer Chemtech Ag | POROUS DOSING ELEMENT WITH COATING |
WO2023056550A1 (en) * | 2021-10-04 | 2023-04-13 | Magna International Inc. | Extrusion system and method of same |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2689962A (en) * | 1947-10-29 | 1954-09-28 | Earl H Hutcheson | Inner spring mattress |
US2584225A (en) * | 1949-10-01 | 1952-02-05 | Celanese Corp | Mixing apparatus |
FR1183960A (en) * | 1957-10-05 | 1959-07-16 | Belge Produits Chimiques Sa | Solid detergent compositions |
US3055837A (en) * | 1958-10-08 | 1962-09-25 | George G Wittwer | Synthetic detergent cake and process for making the same |
NL259594A (en) * | 1959-12-31 | |||
US3146493A (en) * | 1960-07-25 | 1964-09-01 | Bergwerksgesellschaft Hibernia | Process and apparatus for the production of polyolefine granulates |
US3089197A (en) * | 1960-07-25 | 1963-05-14 | Procter & Gamble | Method for preparing detergent compositions |
US3129187A (en) * | 1960-10-14 | 1964-04-14 | Atlantic Refining Co | Synthetic detergent toilet bar |
NL274845A (en) * | 1961-06-30 | 1900-01-01 | ||
BE634272A (en) * | 1963-02-27 |
-
1965
- 1965-11-26 US US509803A patent/US3497912A/en not_active Expired - Lifetime
-
1966
- 1966-02-21 US US529151A patent/US3434974A/en not_active Expired - Lifetime
- 1966-06-28 AT AT166370A patent/AT289275B/en active
- 1966-06-28 AT AT615266A patent/AT289273B/en not_active IP Right Cessation
- 1966-06-28 GB GB28957/66A patent/GB1155724A/en not_active Expired
- 1966-06-29 BE BE683383D patent/BE683383A/xx unknown
- 1966-07-01 SE SE9071/66A patent/SE345875B/xx unknown
- 1966-07-01 NL NL6609217A patent/NL6609217A/xx unknown
-
1967
- 1967-04-08 ES ES0328199A patent/ES328199A1/en not_active Expired
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2455887A1 (en) * | 1979-05-11 | 1980-12-05 | Mann & Schroeder Kg | BATH SALT |
GB2213827A (en) * | 1988-01-14 | 1989-08-23 | Unilever Plc | Detergent laundry bars |
GB2257649A (en) * | 1991-07-18 | 1993-01-20 | Apv Corp Ltd | Converting fine particlulate material to block form,by extrusion |
Also Published As
Publication number | Publication date |
---|---|
AT289273B (en) | 1971-04-13 |
BE683383A (en) | 1966-12-01 |
SE345875B (en) | 1972-06-12 |
AT289275B (en) | 1971-04-13 |
NL6609217A (en) | 1967-01-03 |
ES328199A1 (en) | 1967-08-16 |
US3434974A (en) | 1969-03-25 |
US3497912A (en) | 1970-03-03 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed [section 19, patents act 1949] | ||
PLNP | Patent lapsed through nonpayment of renewal fees |